Patent US4016247A successfully refreshed from Google Patents.
US4016247A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Production of carbon shaped articles having high anisotropy
Assignee: Kureha Corp
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Filing: 1975-04-03
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Granted: 1977-04-05
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Expires: 1995-04-03
Abstract
Abstract In the production of carbon shaped articles such as fibers, films, etc. having high molecular orientation, anisotropy, strength, and modulus of elasticity through the steps of forming raw material pitch into desired shapes, infusibilization of the same followed by carbonization optionally graphitization, a raw material pitch having particular physical properties such as melt viscosity of 0.4 to 700 poises at a temperature range of 320° to 480° C, eminent structural anisotropy, and fluidity is used to produce such desired shaped product.
Inventors
- 👤 Sugio Otani
- 👤 Shoji Watanabe
- 👤 Tadashi Araki
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-27 17:54
CPC Classifications
D; D01; D01F; D01F9/00; D01F9/08; D01F9/12; D01F9/14; D01F9/145; C; C01; C01B; C01B32/00; C04; C04B; C04B35/00; C04B35/515; C04B35/52; C04B35/524; C10; C10C; C10C1/00; C10C1/19
Claims Analysis
Total Claims: 4
Claim 1
Independent Claim
163 words
In a method for producing carbon shaped articles having high molecular orientation, anisotropy, and modulus of elasticity from pitch as the raw material through the process steps of forming the pitch into the required shape, subjecting the same to infusibilization, carbonization, and optionally graphitization treatments, the improvement which comprises: forming said raw material pitch having specific properties of the carbon content in the range of from 95 to 96.5% by weight, a mean molecular weight of from 400 to 2,000, melt viscosity of from 0.4 to 700 poises at a temperature range of from 320° C to 480° C, said pitch possessing an anisotropic structure and excellent fluidity; and then carrying out said process steps of the infusibilization, carbonization, and optionally graphitization of said shaped articles, in sequence, without applying any tension whatsoever thereto during said treatments, said raw material pitch being obtained by subjecting tetrabenzophenazine to heat treatment at a temperature of from 450° to 600° C for 30 to 90 minutes.
Claim 2
Dependent Claim
163 words
In a method for producing carbon shaped articles having high molecular orientation, anisotropy, and modulus of elasticity from pitch as the raw material through the process steps of forming the pitch into the required shape, subjecting the same to infusibilization, carbonization, and optionally graphitization treatments, the improvement which comprises: forming said raw material pitch having specific properties of the carbon content in the range of from 95 to 96.5% by weight, a mean molecular weight of from 400 to 2,000, melt viscosity of from 0.4 to 700 poises at a temperature range of from 320° C to 480° C, said pitch possessing an anisotropic structure and excellent fluidity; and then carrying out said process steps of the infusibilization, carbonization, and optionally graphitization of said shaped articles, in sequence, without applying any tension whatsoever thereto during said treatments, said raw material pitch being obtained by subjecting tetrabenzophenazine to heat treatment at a temperature of from 450° to 600° C for 30 to 90 minutes.
Claim 3
Dependent Claim
25 words
A method as claimed in claim 1, in which said heat treatment of tetrabenzophenazine is effected at a temperature of from 580 to 590° C.
Claim 4
Dependent Claim
40 words
A method according to claim 1, in which the raw material pitch is obtained by subjecting the crystals of tetrabenzo (a,c,h,j)-phenazine having a melting point of 485° C to heat treatment at 580° C to 590° C for 1 hour.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-04-04 | 1980-10-04 | 1981-04-05 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-04-04 | 1984-10-04 | 1985-04-05 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-04-04 | 1988-10-04 | 1989-04-05 | $7700.00 | Window Closed / Lapsed |