Patent US4016247A successfully refreshed from Google Patents.
← Back to Patent Explorer
US4016247A Expired / Lapsed US ⏱️ 0.0 years remaining

Production of carbon shaped articles having high anisotropy

Assignee: Kureha Corp
•
Filing: 1975-04-03
•
Granted: 1977-04-05
•
Expires: 1995-04-03
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract In the production of carbon shaped articles such as fibers, films, etc. having high molecular orientation, anisotropy, strength, and modulus of elasticity through the steps of forming raw material pitch into desired shapes, infusibilization of the same followed by carbonization optionally graphitization, a raw material pitch having particular physical properties such as melt viscosity of 0.4 to 700 poises at a temperature range of 320° to 480° C, eminent structural anisotropy, and fluidity is used to produce such desired shaped product.

Inventors

  • 👤 Sugio Otani
  • 👤 Shoji Watanabe
  • 👤 Tadashi Araki

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 17:54
CPC Classifications
D; D01; D01F; D01F9/00; D01F9/08; D01F9/12; D01F9/14; D01F9/145; C; C01; C01B; C01B32/00; C04; C04B; C04B35/00; C04B35/515; C04B35/52; C04B35/524; C10; C10C; C10C1/00; C10C1/19

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 163 words
In a method for producing carbon shaped articles having high molecular orientation, anisotropy, and modulus of elasticity from pitch as the raw material through the process steps of forming the pitch into the required shape, subjecting the same to infusibilization, carbonization, and optionally graphitization treatments, the improvement which comprises: forming said raw material pitch having specific properties of the carbon content in the range of from 95 to 96.5% by weight, a mean molecular weight of from 400 to 2,000, melt viscosity of from 0.4 to 700 poises at a temperature range of from 320° C to 480° C, said pitch possessing an anisotropic structure and excellent fluidity; and then carrying out said process steps of the infusibilization, carbonization, and optionally graphitization of said shaped articles, in sequence, without applying any tension whatsoever thereto during said treatments, said raw material pitch being obtained by subjecting tetrabenzophenazine to heat treatment at a temperature of from 450° to 600° C for 30 to 90 minutes.
Claim 2
Dependent Claim 163 words
In a method for producing carbon shaped articles having high molecular orientation, anisotropy, and modulus of elasticity from pitch as the raw material through the process steps of forming the pitch into the required shape, subjecting the same to infusibilization, carbonization, and optionally graphitization treatments, the improvement which comprises: forming said raw material pitch having specific properties of the carbon content in the range of from 95 to 96.5% by weight, a mean molecular weight of from 400 to 2,000, melt viscosity of from 0.4 to 700 poises at a temperature range of from 320° C to 480° C, said pitch possessing an anisotropic structure and excellent fluidity; and then carrying out said process steps of the infusibilization, carbonization, and optionally graphitization of said shaped articles, in sequence, without applying any tension whatsoever thereto during said treatments, said raw material pitch being obtained by subjecting tetrabenzophenazine to heat treatment at a temperature of from 450° to 600° C for 30 to 90 minutes.
Claim 3
Dependent Claim 25 words
A method as claimed in claim 1, in which said heat treatment of tetrabenzophenazine is effected at a temperature of from 580 to 590° C.
Claim 4
Dependent Claim 40 words
A method according to claim 1, in which the raw material pitch is obtained by subjecting the crystals of tetrabenzo (a,c,h,j)-phenazine having a melting point of 485° C to heat treatment at 580° C to 590° C for 1 hour.

References Cited (Backward Citations)

US2915370A Cited
DE1151248B Cited
US3392216A Cited
US3558276A Cited
US3565980A Cited
US3629379A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-04-04 1980-10-04 1981-04-05 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-04-04 1984-10-04 1985-04-05 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-04-04 1988-10-04 1989-04-05 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag