Patent US4014647A successfully refreshed from Google Patents.
US4014647A
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Exhaust process for the dyeing of synthetic fibre materials
Assignee: Bayer AG
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Filing: 1975-02-14
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Granted: 1977-03-29
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Expires: 1995-02-14
Abstract
Abstract Exhaust process for the dyeing of synthetic fibre materials from organic water-immiscible solvents wherein are used as dyestuffs sulphonamide group containing disperse dyestuffs. There are obtained without originating waste waters dyeings with excellent fastness to washing, rubbing, light and sublimation.
Inventors
- 👤 Rutger Neeff
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-31 14:20
CPC Classifications
C; C09; C09B; C09B69/00; C09B1/00; C09B1/02; C09B1/06; C09B1/16; C09B1/20; C09B1/50; C09B1/56; C09B1/58; C09B25/00; C09B39/00; C09B5/00; C09B51/00; D; D06; D06P; D06P1/00; D06P1/90; D06P1/908
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
203 words
A process for dyeing synthetic fiber material by exhaustion comprising introducing synthetic fiber material into a dyebath which is a dispersion consisting essentially of A. organic solvent; B. nitro dyestuff containing 1 to 3 sulfonamide groups and largely insoluble in said dyebath; and C. up to 1% by weight of said organic solvent of water; said organic solvent consisting of water immiscible aliphatic halogenated hydrocarbon; and dyeing at a temperature of 60° to 170° C for 10-60 minutes until the dyebath is exhausted; said nitro dyestuff free of reactive groups, acid groups and carboxamide groups having the formula ##STR158## in which R 1 means hydrogen, a halogen atom, a trifluoro, cyano, hydroxy, C 1 -C 4 -alkyl or -alkoxy, a hydromethyl or -ethyl, a hydroxy-ethylene-oxy, acylamino, alkylsulphonylamino, alkylsulphone, carboxamido, aminosulphonylalkylene-amino or sulphonamide group; R 2 means hydrogen or a C 1 -C 4 -alkoxy group; R 3 means hydrogen, a halogen atom, a hydroxy, hydroxyethylene-oxy, carboxamido, aminosulphonyl-alkylene-oxy or sulphonamide group; X stands for the group --SO 2 -- or --CO; and Y stands for --NH-- or --O--, with the proviso that one of the radicals R 1 , R 3 or ##STR159## is a sulphonamide group or a radical containing a sulphonamide group.
Claim 2
Dependent Claim
203 words
A process for dyeing synthetic fiber material by exhaustion comprising introducing synthetic fiber material into a dyebath which is a dispersion consisting essentially of A. organic solvent; B. nitro dyestuff containing 1 to 3 sulfonamide groups and largely insoluble in said dyebath; and C. up to 1% by weight of said organic solvent of water; said organic solvent consisting of water immiscible aliphatic halogenated hydrocarbon; and dyeing at a temperature of 60° to 170° C for 10-60 minutes until the dyebath is exhausted; said nitro dyestuff free of reactive groups, acid groups and carboxamide groups having the formula ##STR158## in which R 1 means hydrogen, a halogen atom, a trifluoro, cyano, hydroxy, C 1 -C 4 -alkyl or -alkoxy, a hydromethyl or -ethyl, a hydroxy-ethylene-oxy, acylamino, alkylsulphonylamino, alkylsulphone, carboxamido, aminosulphonylalkylene-amino or sulphonamide group; R 2 means hydrogen or a C 1 -C 4 -alkoxy group; R 3 means hydrogen, a halogen atom, a hydroxy, hydroxyethylene-oxy, carboxamido, aminosulphonyl-alkylene-oxy or sulphonamide group; X stands for the group --SO 2 -- or --CO; and Y stands for --NH-- or --O--, with the proviso that one of the radicals R 1 , R 3 or ##STR159## is a sulphonamide group or a radical containing a sulphonamide group.
Claim 3
Dependent Claim
13 words
Process of claim 1 in which said nitro dyestuff has the formula ##STR160##
Claim 4
Dependent Claim
162 words
Process for dyeing synthetic fiber material by exhaustion comprising introducing synthetic fiber material into a dyebath which is a dispersion consisting essentially of A. organic solvent; B. nitro dyestuff containing 1 to 3 sulfonamide groups and largely insoluble in said dyebath; and C. up to 1% by weight of said organic solvent of water; said organic solvent consisting of water immiscible aliphatic halogenated hydrocarbon; and dyeing at a temperature of 60° C to 170° C for 10-60 minutes until the dyebath is exhausted; said nitro dyestuff free of reactive groups, acid groups and carboxamide groups having the formula ##STR161## in which R 1 means hydrogen, a C 1 -C 4 -alkyl or -alkoxy group, halogen, a trifluoromethyl, nitro, hydroxymethyl, hydroxyethyl, phenyl, phenoxy, phenylazo, benzyloxy, carboxy, C 1 -C 4 -alkoxycarbonyl, C 1 -C 4 -acylamino, C 1 -C 4 -alkylsulphonyl or sulphonamide group; R 2 means hydrogen, halogen or a C 1 -C 4 -alkoxy group; and D means a sulphonamide group.
Claim 5
Dependent Claim
162 words
Process for dyeing synthetic fiber material by exhaustion comprising introducing synthetic fiber material into a dyebath which is a dispersion consisting essentially of A. organic solvent; B. nitro dyestuff containing 1 to 3 sulfonamide groups and largely insoluble in said dyebath; and C. up to 1% by weight of said organic solvent of water; said organic solvent consisting of water immiscible aliphatic halogenated hydrocarbon; and dyeing at a temperature of 60° C to 170° C for 10-60 minutes until the dyebath is exhausted; said nitro dyestuff free of reactive groups, acid groups and carboxamide groups having the formula ##STR161## in which R 1 means hydrogen, a C 1 -C 4 -alkyl or -alkoxy group, halogen, a trifluoromethyl, nitro, hydroxymethyl, hydroxyethyl, phenyl, phenoxy, phenylazo, benzyloxy, carboxy, C 1 -C 4 -alkoxycarbonyl, C 1 -C 4 -acylamino, C 1 -C 4 -alkylsulphonyl or sulphonamide group; R 2 means hydrogen, halogen or a C 1 -C 4 -alkoxy group; and D means a sulphonamide group.
Claim 6
Dependent Claim
22 words
The process of claim 1 in which said synthetic fiber material is polyester, polyamide, cellulose, triacetate, cellulose 21/2 acetate, polyacrylonitrile, or polyurethane.
Claim 7
Dependent Claim
13 words
The process of claim 1 in which said synthetic fiber material is polyester.
Claim 8
Dependent Claim
13 words
The process of claim 1 in which said synthetic fiber material is polyamide.
Claim 9
Dependent Claim
28 words
The process of claim 1 in which said dyebath contains 0.05 to 2% by weight of non-ionic dyeing auxiliary based on the weight of said aliphatic halogenated hydrocarbon.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-03-28 | 1980-09-27 | 1981-03-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-03-28 | 1984-09-27 | 1985-03-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-03-28 | 1988-09-27 | 1989-03-29 | $7700.00 | Window Closed / Lapsed |