Patent US4002176A successfully refreshed from Google Patents.
US4002176A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Tobacco based smoking material
Assignee: Imperial Group PLC
•
Filing: 1974-08-13
•
Granted: 1977-01-11
•
Expires: 1994-08-13
Abstract
Abstract Thermal degradation of tobacco by heating at above 100 DEG , suitably 100 DEG -300 DEG C in presence of a catalyst until the weight of the residue is less than 90% of the weight of the original tobacco improves the smoke-flavor, although similar heating in absence of catalyst fails to produce this effect. The degraded tobacco material is an improved material suitable for smoking mixtures wherein the degraded tobacco material possesses an enhanced tobacco flavor as compared to untreated tobacco.
Inventors
- 👤 Robert Craig Anderson
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 12:44
CPC Classifications
A; A24; A24B; A24B3/00; A24B3/12; A24B15/00; A24B15/10; A24B15/12; A24B15/14; A24B15/16; A24B15/165
Claims Analysis
Total Claims: 20
Claim 1
Independent Claim
120 words
A process for the manufacture of an improved material suitable for smoking mixtures, comprising subjecting tobacco to a catalyzed degradation process at a temperature between about 100° to about 300° C until the weight of degraded material is less than 90% but not less than about 70% of the weight of the original tobacco, wherein said catalyzed degradation is carried out in the presence of a catalyst which accelerates the thermal degradation of said tobacco or lowers the thermal degradation temperature, said catalyst selected from the group consisting of strong acids, salts of strong acids with weak bases, alkali salts of weak acids and alkali hydroxides whereby the degraded tobacco material possesses enhanced tobacco flavour as compared to untreated tobacco.
Claim 2
Dependent Claim
120 words
A process for the manufacture of an improved material suitable for smoking mixtures, comprising subjecting tobacco to a catalyzed degradation process at a temperature between about 100° to about 300° C until the weight of degraded material is less than 90% but not less than about 70% of the weight of the original tobacco, wherein said catalyzed degradation is carried out in the presence of a catalyst which accelerates the thermal degradation of said tobacco or lowers the thermal degradation temperature, said catalyst selected from the group consisting of strong acids, salts of strong acids with weak bases, alkali salts of weak acids and alkali hydroxides whereby the degraded tobacco material possesses enhanced tobacco flavour as compared to untreated tobacco.
Claim 3
Dependent Claim
13 words
Process according to claim 1 wherein the temperature is 100° to 250° C.
Claim 4
Dependent Claim
13 words
Process according to claim 1 wherein the temperature is 160° to 250° C.
Claim 5
Dependent Claim
19 words
Process according to claim 3 wherein acidity from the use of a strong acid is neutralised by adding ammonia.
Claim 6
Dependent Claim
13 words
Process according to claim 1 wherein the catalyst used is an acidic substance.
Claim 7
Dependent Claim
23 words
Process according to claim 5 wherein the catalyst is a strong acid or a salt of a strong acid with a weak base.
Claim 8
Dependent Claim
11 words
Process according to claim 6 wherein the catalyst is sulphuric acid.
Claim 9
Dependent Claim
11 words
Process according to claim 6 wherein the catalyst is ammonium sulphamate.
Claim 10
Dependent Claim
20 words
Process according to claim 1 wherein the amount of catalyst is from 1 to 20% by weight of the tobacco.
Claim 11
Dependent Claim
20 words
Process according to claim 1 wherein the amount of catalyst is from 3 to 8% by weight of the tobacco.
Claim 12
Dependent Claim
14 words
Process according to claim 1 applied to tobacco stalks or finely powdered tobacco material.
Claim 13
Dependent Claim
10 words
Thermally degraded tobacco made by the process of claim 1.
Claim 14
Dependent Claim
11 words
Thermally degraded tobacco according to claim 12 formulated into a sheet.
Claim 15
Dependent Claim
33 words
Thermally degraded tobacco according to claim 13 formulated into a sheet which contains another smoke-producing material, a glow-promoting catalyst, a material to improve ash coherence or colour, nicotine, flavourant, humectant, medicament or filler.
Claim 16
Dependent Claim
34 words
Thermally degraded tobacco formulated into a sheet according to claim 13, containing at least 40% of filler in which ions accelerating combustion are balanced against ions retarding combustion to provide an acceptable combustion rate.
Claim 17
Dependent Claim
18 words
Thermally degraded tobacco according to claim 12 formulated into a sheet with the aid of a binding agent.
Claim 18
Dependent Claim
94 words
A process for the manufacture of an improved material suitable for smoking mixtures, comprising subjecting tobacco to a catalyzed degradation process at a temperature in excess of 100° C until the weight of the degraded material is less than 90% but not less than about 70% of the weight of the original tobacco, wherein said catalyzed degradation is carried out in the presence of a catalyst which accelerates the thermal degradation of said tobacco or lowers the thermal degradation temperature whereby the degraded tobacco material possesses enhanced tobacco flavour as compared to untreated tobacco.
Claim 19
Dependent Claim
94 words
A process for the manufacture of an improved material suitable for smoking mixtures, comprising subjecting tobacco to a catalyzed degradation process at a temperature in excess of 100° C until the weight of the degraded material is less than 90% but not less than about 70% of the weight of the original tobacco, wherein said catalyzed degradation is carried out in the presence of a catalyst which accelerates the thermal degradation of said tobacco or lowers the thermal degradation temperature whereby the degraded tobacco material possesses enhanced tobacco flavour as compared to untreated tobacco.
Claim 20
Dependent Claim
17 words
Process according to claim 17 wherein the temperature is between about 100° C to about 300° C.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-01-11 | 1980-07-12 | 1981-01-11 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-01-11 | 1984-07-12 | 1985-01-11 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-01-11 | 1988-07-12 | 1989-01-11 | $7700.00 | Window Closed / Lapsed |