Patent US4001024A successfully refreshed from Google Patents.
← Back to Patent Explorer
US4001024A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of multi-layer coating

Assignee: Eastman Kodak Co
•
Filing: 1976-03-22
•
Granted: 1977-01-04
•
Expires: 1996-03-22
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract The simultaneous high speed application of a plurality of liquid coating compositions to a moving web by the method of multi-layer bead coating is improved by coating the lowermost layer as a thin layer formed from a low viscosity coating composition and coating the layer immediately above the lowermost layer as a thicker layer of higher viscosity such that vortical action of the coating bead is confined to the lowermost layer and the layer immediately above it. By this means, intermixing of the coating composition forming the lowermost layer with the coating composition forming the layer immediately above it occurs, but all other layers are coated in discrete form. The method is especially useful in the manufacture of multi-layer photographic films and papers.

Inventors

  • 👤 Donald Allen Dittman
  • 👤 Francis Armand Rozzi

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 20:58
CPC Classifications
G; G03; G03C; G03C1/00; G03C1/74; B; B05; B05C; B05C5/00; B05C5/007; B05C9/00; B05C9/06; G03C2001/7481; G03C2200/00; G03C2200/11; G03C2200/20

Claims Analysis

Total Claims: 17
Claim 1
Independent Claim 184 words
In a method of simultaneously applying a plurality of layers of liquid coating compositions to a moving web in which each of said compositions is fed into a coating bead which is maintained in bridging relationship between the surface of said web and a coating device spaced therefrom and the surface of said web is continuously moved across and in contact with said coating bead to simultaneously pick up all of said layers, the improvement wherein the speed of the web is at least 100 centimeters per second, the lowermost layer is thin and formed of a coating composition of low viscosity, and the layer immediately above the lowermost layer is thicker than the lowermost layer and formed of a coating composition of higher viscosity; the thickness and viscosity of the lowermost layer and of the layer immediately above it being such that vortical of said coating bead is confined within the lowermost layer and the layer immediately above it, whereby interlayer mixing occurs between the lowermost layer and the layer immediately above it but all other layers are coated in distinct layer relationship.
Claim 2
Dependent Claim 184 words
In a method of simultaneously applying a plurality of layers of liquid coating compositions to a moving web in which each of said compositions is fed into a coating bead which is maintained in bridging relationship between the surface of said web and a coating device spaced therefrom and the surface of said web is continuously moved across and in contact with said coating bead to simultaneously pick up all of said layers, the improvement wherein the speed of the web is at least 100 centimeters per second, the lowermost layer is thin and formed of a coating composition of low viscosity, and the layer immediately above the lowermost layer is thicker than the lowermost layer and formed of a coating composition of higher viscosity; the thickness and viscosity of the lowermost layer and of the layer immediately above it being such that vortical of said coating bead is confined within the lowermost layer and the layer immediately above it, whereby interlayer mixing occurs between the lowermost layer and the layer immediately above it but all other layers are coated in distinct layer relationship.
Claim 3
Dependent Claim 195 words
In a method of manufacturing a photographic element by simultaneously applying a plurality of layers of liquid photographic coating compositions to a moving web of photographic support material in which each of said compositions is fed into a coating bead which is maintained in bridging relationship between the surface of said web and a coating device spaced therefrom and the surface of said web is continuously moved across and in contact with said coating bead to simultaneously pick up all of said layers, the improvement wherein the speed of the web is at least 100 centimeters per second, the lowermost layer is thin and formed of a coating composition of low viscosity, and the layer immediately above the lowermost layer is thicker than the lowermost layer and formed of a coating composition of higher viscosity; the thickness and viscosity of the lowermost layer and of the layer immediately above it being such that vortical action of said coating bead is confined within the lowermost layer and the layer immediately above it, whereby interlayer mixing occurs between the lowermost layer and the layer immediately above it but all other layers are coated in distinct layer relationship.
Claim 4
Dependent Claim 195 words
In a method of manufacturing a photographic element by simultaneously applying a plurality of layers of liquid photographic coating compositions to a moving web of photographic support material in which each of said compositions is fed into a coating bead which is maintained in bridging relationship between the surface of said web and a coating device spaced therefrom and the surface of said web is continuously moved across and in contact with said coating bead to simultaneously pick up all of said layers, the improvement wherein the speed of the web is at least 100 centimeters per second, the lowermost layer is thin and formed of a coating composition of low viscosity, and the layer immediately above the lowermost layer is thicker than the lowermost layer and formed of a coating composition of higher viscosity; the thickness and viscosity of the lowermost layer and of the layer immediately above it being such that vortical action of said coating bead is confined within the lowermost layer and the layer immediately above it, whereby interlayer mixing occurs between the lowermost layer and the layer immediately above it but all other layers are coated in distinct layer relationship.
Claim 5
Dependent Claim 57 words
The method of claim 2 wherein the wet coverage of the lowermost layer is in the range from about 2 to about 12 cubic centimeters of coating composition per square meter of web surface and the lowermost layer is formed from a coating composition with a viscosity in the range from about 1 to about 8 centipoises.
Claim 6
Dependent Claim 65 words
The method of claim 3 wherein the wet coverage of the layer immediately above the lowermost layer is in the range from about 15 to about 50 cubic centimeters of coating composition per square meter of web surface and the layer immediately above the lowermost layer is formed from a coating composition with a viscosity in the range from about 10 to about 100 centipoises.
Claim 7
Dependent Claim 115 words
The method of claim 2 wherein the wet coverage of the lowermost layer is in the range from about 5 to about 10 cubic centimeters of coating composition per square meter of web surface, the lowermost layer is formed from a coating composition with a viscosity in the range from about 3 to about 5 centipoises, the wet coverage of the layer immediately above the lowermost layer is in the range from about 20 to about 35 cubic centimeters of coating composition per square meter of web surface, and the layer immediately above the lowermost layer is formed from a coating composition with a viscosity in the range from about 30 to about 70 centipoises.
Claim 8
Dependent Claim 21 words
The method of claim 2 wherein the coating composition from which the lowermost layer is formed in a dilute gelatin solution.
Claim 9
Dependent Claim 27 words
The method of claim 2 wherein the coating composition from which the lowermost layer is formed is a dispersion of a coupler solvent in a hydrophilic colloid.
Claim 10
Dependent Claim 24 words
The method of claim 2 wherein the coating composition used to form the layer immediately above the lowermost layer is a gelatino/silver halide emulsion.
Claim 11
Dependent Claim 48 words
The method of claim 2 wherein the coating compositions used to form the lowermost layer and the layer immediately above it are each gelatino/silver halide emulsion but the composition used to form the lowermost layer is more dilute than that used to form the layer immediately above it.
Claim 12
Dependent Claim 13 words
The method of claim 2 wherein said support is a cellulose acetate support.
Claim 13
Dependent Claim 12 words
The method of claim 2 wherein said support is a polyester support.
Claim 14
Dependent Claim 13 words
The method of claim 2 wherein said support is a polymer-coated paper support.
Claim 15
Dependent Claim 13 words
The method of claim 2 wherein said support is a polyethylene-coated paper support.
Claim 16
Dependent Claim 16 words
The method of claim 2 wherein the coating composition forming the lowermost layer contains a surfactant.
Claim 17
Dependent Claim 103 words
The method of claim 2 wherein the lowermost layer is formed from a dilute gelatin solution having a viscosity in the range of from about 3 to about 5 centipoises coated at a wet coverage in the range from about 5 to about 10 cubic centimeters per square meter of web surface and the layer immediately above the lowermost layer is formed from a gelantino/silver halide emulsion having a viscosity in the range of from about 30 to about 70 centipoises coated at a wet coverage in the range from about 20 to about 35 cubic centimeters per square meter of web surface.

References Cited (Backward Citations)

US2761791A Cited
US2975754A Cited
US2932855A Cited
GB929905A Cited
US3206323A Cited
US3573965A Cited
US3508947A Cited
US3749053A Cited
GB1417765A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-01-04 1980-07-05 1981-01-04 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-01-04 1984-07-05 1985-01-04 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-01-04 1988-07-05 1989-01-04 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag