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US4000975A
Expired / Lapsed
US
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Method of measuring damage to grain
Assignee: Iowa State University Research Foundation Inc
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Filing: 1976-01-12
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Granted: 1977-01-04
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Expires: 1996-01-12
Abstract
Abstract A method of measuring mechanical damage to a grain, such as corn, includes applying a reacting solution to a sample of corn. The solution contains a material, such as 8-anilino-1-naphthalene sulfonic acid, that reacts selectively with the damaged portion of the corn kernels, i.e., the internal protein that is exposed when the outer shell is penetrated or breached. Excess solution is washed off; and the kernels are dried for convenience of handling. The dried corn is ground to a uniform fineness and then spread over a predetermined area. What is inherently a three-dimensional or volume phenomena (damage) is converted to a two-dimensional or area measurement. The sample is exposed to ultraviolet light; and induced fluorescence is measured. The output of the measuring system is linearly related to, and thus a measure of the mechanical damage of the sample.
Inventors
- 👤 Gerald Davis Christenbury
- 👤 Wesley Fisher Buchele
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-27 17:56
CPC Classifications
G; G01; G01N; G01N21/00; G01N21/62; G01N21/63; G01N21/64; G01N21/6428; G01N33/00; G01N33/02; G01N33/10
Claims Analysis
Total Claims: 12
Claim 1
Independent Claim
112 words
A method of measuring mechanical damage to grain comprising: applying a solution to a sample of the damaged grain for a predetermined time, said solution containing a material which selectively chemically bonds to interior protein of said grain, said interior protein having been exposed by said mechanical damage, and which does not bond to other portions of the grain to an appreciable extent, wherein the resulting products fluoresce when irradiated; grinding said sample grains to which said solution has been applied; exposing said ground sample to a source of radiation which induces said fluorescence; and measuring the induced fluorescence of the ground sample, which measurement defines the mechanical damage of said grain.
Claim 2
Independent Claim
112 words
A method of measuring mechanical damage to grain comprising: applying a solution to a sample of the damaged grain for a predetermined time, said solution containing a material which selectively chemically bonds to interior protein of said grain, said interior protein having been exposed by said mechanical damage, and which does not bond to other portions of the grain to an appreciable extent, wherein the resulting products fluoresce when irradiated; grinding said sample grains to which said solution has been applied; exposing said ground sample to a source of radiation which induces said fluorescence; and measuring the induced fluorescence of the ground sample, which measurement defines the mechanical damage of said grain.
Claim 3
Dependent Claim
11 words
The method of claim 1 wherein said grain is kernel corn.
Claim 4
Dependent Claim
19 words
The method of claim 1 wherein said step of grinding comprises grinding said sample to substantially uniform particle size.
Claim 5
Dependent Claim
24 words
The method of claim 1 further comprising the step of spreading the ground sample over a predetermined area before exposing it to ultraviolet light.
Claim 6
Dependent Claim
43 words
The method of claim 1 further comprising the step of detecting induced fluorescence of said sample with a fiber optic conduit having a known conical acceptance window and spreading said sample out beneath said fiber optic conduit throughout the conical acceptance window thereof.
Claim 7
Dependent Claim
28 words
The method of claim 1 further comprising the step of washing said solution from said sample prior to grinding and drying said washed samples for convenience of handling.
Claim 8
Dependent Claim
20 words
The method of claim 1 wherein said solution contains ANS and said predetermined time is less than about 30 minutes.
Claim 9
Dependent Claim
16 words
The method of claim 1 wherein said application time is in the range of 1-2 minutes.
Claim 10
Dependent Claim
15 words
The method of claim 1 wherein said solution is a 0.05 percent solution of ANS.
Claim 11
Independent Claim
112 words
A method of measuring the mechanical damage sustained by corn kernels comprising: selecting a sample of the damaged corn kernels; applying an aqueous solution of a reacting agent to said sample, said agent selectively bonding to the exposed fluory endosperm of said grain to form reaction products which fluoresce when irradiated; removing said solution after a predetermined time; washing excess solution from said sample; grinding said sample to substantially uniform particle size; spreading said ground sample over a known area; exposing the ground sample to a source of radiation which induces said fluorescence; and measuring the induced fluorescence of said sample, which measurement defines the mechanical damage sustained by the corn kernels.
Claim 12
Independent Claim
112 words
A method of measuring the mechanical damage sustained by corn kernels comprising: selecting a sample of the damaged corn kernels; applying an aqueous solution of a reacting agent to said sample, said agent selectively bonding to the exposed fluory endosperm of said grain to form reaction products which fluoresce when irradiated; removing said solution after a predetermined time; washing excess solution from said sample; grinding said sample to substantially uniform particle size; spreading said ground sample over a known area; exposing the ground sample to a source of radiation which induces said fluorescence; and measuring the induced fluorescence of said sample, which measurement defines the mechanical damage sustained by the corn kernels.
References Cited (Backward Citations)
US3773827A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-01-04 | 1980-07-05 | 1981-01-04 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-01-04 | 1984-07-05 | 1985-01-04 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-01-04 | 1988-07-05 | 1989-01-04 | $7700.00 | Window Closed / Lapsed |