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US4000239A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for spinning naphthalate polyester fibers

Assignee: Teijin Ltd
•
Filing: 1973-11-30
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Granted: 1976-12-28
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Expires: 1993-11-30
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Abstract

Abstract A filament, fiber or yarn consisting of a naphthalate polyester containing at least 85 mol % of ethylene-2,6-naphthalate units and having an intrinsic viscosity of 0.45 to 1.0, said filament, fiber or yarn having a diffrection intensity ratio (R) between a bragg refection angle 2θ = 187.7° and 2θ = 15.6°, as determined by the X-ray diffraction method, being in the range of more than 1.73 and up to 5.00. Electrically insulating material can be produced by heat-treating a fabric consisting mainly of the above naphthalate polyester fibers and with a sleeve consisting mainly of the above naphthalate polyester fibers.

Inventors

  • 👤 Isao Hamana
  • 👤 Yoshio Fuziwara
  • 👤 Shiro Kumakawa

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 02:46
CPC Classifications
D; D01; D01F; D01F6/00; D01F6/58; D01F6/62; H; H01; H01B; H01B3/00; H01B3/18; H01B3/30; H01B3/42; H01B3/48; H01B3/50

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 212 words
A process for producing a naphthalate polyester filament, fiber or yarn having a diffraction intensity ratio (R) between a Bragg reflection angle 2θ = 18.7° and 2θ = 15.6° , as determined by the X-ray diffraction method, being in the range of more than 1.73 and up to 5.00, which comprises melt-spinning a naphthalate polyester containing at least 85 mol % of ethylene-2,6-naphthalate units and having an intrinsic viscosity of 0.45 to 1.0, using a spinning nozzle having a cross sectional area of 0.049 to 3.14 mm 2 per hole at a spinning temperature expressed by the following equation: 28.6 [η] + 301.4 ≧ T ≧ 35.7 [η] + 279.3 wherein T is the spinning temperature in ° C. and [η] is the intrinsic viscosity of the polyester, said spinning being at a draft ratio of 50-20,000 and the draft ratio satisfying the following equation: -7.43 × 10.sup.-.sup.5 W + 2.37 ≦log D ≧2.27 √A + 1.98 wherein W is the take-up speed in meters per minute, D is the draft ratio, and A is the cross-sectional area in square millimeter per hole of the spinning nozzle, and then cooling the extruded filaments, and taking up the extruded filaments by Godet rollers at a speed of 3,000 to 8,000 meters per minute.
Claim 2
Dependent Claim 212 words
A process for producing a naphthalate polyester filament, fiber or yarn having a diffraction intensity ratio (R) between a Bragg reflection angle 2θ = 18.7° and 2θ = 15.6° , as determined by the X-ray diffraction method, being in the range of more than 1.73 and up to 5.00, which comprises melt-spinning a naphthalate polyester containing at least 85 mol % of ethylene-2,6-naphthalate units and having an intrinsic viscosity of 0.45 to 1.0, using a spinning nozzle having a cross sectional area of 0.049 to 3.14 mm 2 per hole at a spinning temperature expressed by the following equation: 28.6 [η] + 301.4 ≧ T ≧ 35.7 [η] + 279.3 wherein T is the spinning temperature in ° C. and [η] is the intrinsic viscosity of the polyester, said spinning being at a draft ratio of 50-20,000 and the draft ratio satisfying the following equation: -7.43 × 10.sup.-.sup.5 W + 2.37 ≦log D ≧2.27 √A + 1.98 wherein W is the take-up speed in meters per minute, D is the draft ratio, and A is the cross-sectional area in square millimeter per hole of the spinning nozzle, and then cooling the extruded filaments, and taking up the extruded filaments by Godet rollers at a speed of 3,000 to 8,000 meters per minute.
Claim 3
Dependent Claim 63 words
The process of claim 1 wherein the spinning temperature is defined by the following equations 28.6 [≧]+ 301.4 ≧T≧35.7 [η] + 279.3 T ≧(73.8 [≧]- 88.6) √ A + 331.6 wherein T is the spinning temperature in ° C., [η] is the intrinsic viscosity of the polyester, and A is the cross sectional area in square millimeter per hole of the spinning nozzle.

References Cited (Backward Citations)

US2604667A Cited
US3361859A Cited
US3486318A Cited
JPS451932Y1 Cited
US3452132A Cited
JPS4311824Y1 Cited
US3616832A Cited
US3549597A Cited
US3707593A Cited
US3875119A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-12-28 1980-06-28 1980-12-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-12-28 1984-06-28 1984-12-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-12-28 1988-06-28 1988-12-28 $7700.00 Window Closed / Lapsed

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