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US3973440A Expired / Lapsed US ⏱️ 0.0 years remaining

Catalyst sampling method

Assignee: Universal Oil Products Co
•
Filing: 1975-04-28
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Granted: 1976-08-10
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Expires: 1995-04-28
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Abstract

Abstract Small representative samples of catalyst are removed from a fixed bed reactor through a withdrawal conduit and transferred into a sample receiver held at a lower pressure by quickly unsealing the withdrawal conduit and causing a small and sudden gas flow which fluidizes catalyst and lifts it into the withdrawal conduit, through which it falls by the action of gravity.

Inventors

  • 👤 John E. Vande Ven
  • 👤 Steven M. Fischer

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 06:51
CPC Classifications
G; G01; G01N; G01N1/00; G01N1/02; G01N1/10; G01N1/20; B; B01; B01J; B01J8/00; B01J8/0015; B01J8/002

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 142 words
A method of transferring a catalyst sample from a sampling point within a vessel containing a bed of catalyst into a withdrawal conduit having a downward-facing catalyst entrance port, and of transferring the catalyst sample into a sample receiver located outside of the vessel which comprises the steps of: a. sealing the withdrawal conduit to gas flow at a point intermediate the sampling point and the sample receiver; b. evacuating the sample receiver and creating a pressure therein lower than that maintained in the vessel; and, c. rapidly unsealing the withdrawal conduit and passing a short and rapid gas flow through the withdrawal conduit, which equalizes the pressures within the vessel and the sample receiver, and effecting a fluidization of catalyst into the entrance port of the withdrawal conduit and the transfer of catalyst through the withdrawal conduit to the sample receiver.
Claim 2
Independent Claim 142 words
A method of transferring a catalyst sample from a sampling point within a vessel containing a bed of catalyst into a withdrawal conduit having a downward-facing catalyst entrance port, and of transferring the catalyst sample into a sample receiver located outside of the vessel which comprises the steps of: a. sealing the withdrawal conduit to gas flow at a point intermediate the sampling point and the sample receiver; b. evacuating the sample receiver and creating a pressure therein lower than that maintained in the vessel; and, c. rapidly unsealing the withdrawal conduit and passing a short and rapid gas flow through the withdrawal conduit, which equalizes the pressures within the vessel and the sample receiver, and effecting a fluidization of catalyst into the entrance port of the withdrawal conduit and the transfer of catalyst through the withdrawal conduit to the sample receiver.
Claim 3
Dependent Claim 21 words
The method of claim 1 further characterized in that the pressure within the sample receiver is lowered to a subatmospheric pressure.
Claim 4
Dependent Claim 17 words
The method of claim 2 further characterized in that a portion of the withdrawal conduit is evacuated.

References Cited (Backward Citations)

US3129590A Cited
US3348419A Cited
US3442138A Cited
US3487695A Cited
US3653265A Cited
US3786682A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-08-10 1980-02-09 1980-08-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-08-10 1984-02-09 1984-08-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-08-10 1988-02-09 1988-08-10 $7700.00 Window Closed / Lapsed

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