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US3958933A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the manufacture of fast dyeings on synthetic hydrophobic textile material

Assignee: Novartis Corp
•
Filing: 1974-05-13
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Granted: 1976-06-01
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Expires: 1994-05-13
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Abstract

Abstract The invention describes a process for the discontinuous aftertreatment of synthetic hydrophobic textile material, especially polyamide or polyester textile material, which is dyed preferably from an organic liquor with disperse dyestuffs containing hydroxyl and/or amino groups, with chemical fixing agents such as isocyanates, masked isocyanates, acid halides or acid anhydrides, from chlorinated aliphatic hydrocarbons, especially perchloroethylene, at temperatures above 80°C, and subsequently rinsing and drying this material on which dyeings are obtained that are fast to water, solvents, light and are also very fast to sublimation.

Inventors

  • 👤 Gustaf Graff
  • 👤 Hans-Jorg Angliker
  • 👤 Richard Peter
  • 👤 Branimir Milicevic
  • 👤 Hansruedi Hoster
  • 👤 Raymond DeFago

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 23:30
CPC Classifications
D; D06; D06P; D06P1/00; D06P1/90; D06P1/92; D06P1/922; D06P1/924; C; C09; C09B; C09B43/00; C09B43/12; C09B43/18; C09B43/26; D06P5/00; D06P5/02; D06P5/04; Y; Y10; Y10S; Y10S8/00; Y10S8/11

Claims Analysis

Total Claims: 20
Claim 1
Independent Claim 109 words
A process for dyeing synthetic hydrophobic textile material, which comprises dyeing the textile material with a disperse dyestuff containing a hydroxyl and/or a primary or secondary amino group and thereafter treating, at a temperature above 80°C, the dyed textile with a solution of a fixing agent in a chlorinated aliphatic hydrocarbon boiling above about 100°C, the fixing agent consisting essentially of an acylating agent selected from the group consisting of organic isocyanates, masked organic isocyanates, aliphatic monocarboxylic acid halides of at least 8 carbon atoms, aromatic carboxylic acid halides, heterocyclic carboxylic acid halides, aliphatic dicarboxylic acid halides, aliphatic polycarboxylic acid halides, and aliphatic and aromatic cyclic dicarboxylic acid anhydrides.
Claim 2
Dependent Claim 109 words
A process for dyeing synthetic hydrophobic textile material, which comprises dyeing the textile material with a disperse dyestuff containing a hydroxyl and/or a primary or secondary amino group and thereafter treating, at a temperature above 80°C, the dyed textile with a solution of a fixing agent in a chlorinated aliphatic hydrocarbon boiling above about 100°C, the fixing agent consisting essentially of an acylating agent selected from the group consisting of organic isocyanates, masked organic isocyanates, aliphatic monocarboxylic acid halides of at least 8 carbon atoms, aromatic carboxylic acid halides, heterocyclic carboxylic acid halides, aliphatic dicarboxylic acid halides, aliphatic polycarboxylic acid halides, and aliphatic and aromatic cyclic dicarboxylic acid anhydrides.
Claim 3
Dependent Claim 13 words
A process according to claim 1, wherein the chlorinated aliphatic hydrocarbon is perchloroethylene.
Claim 4
Dependent Claim 24 words
A process according to claim 1, wherein textile materials are treated which are dyed with disperse dyestuffs containing a primary or secondary amino group.
Claim 5
Dependent Claim 32 words
A process according to claim 1, wherein textile materials are treated which are dyed with disperse dyestuffs containing at least a primary or secondary amino group and at least one hydroxyl group.
Claim 6
Dependent Claim 24 words
A process according to claim 1, wherein textile materials are treated which are dyed with disperse dyestuffs containing at least one aliphatic hydroxyl group.
Claim 7
Dependent Claim 18 words
A process according to claim 1, wherein an isocyanate or masked isocyanate is used as the fixing agent.
Claim 8
Dependent Claim 32 words
A process according to claim 6, wherein the fixing agent is selected from the group consisting of OCN(CH 2 ) 4 NCO, NaO 3 SCONH(CH 2 ) 6 NHCOSO 3 Na, ##SPC20##
Claim 9
Dependent Claim 16 words
A process according to claim 1, wherein 1,6-hexamethylenediisocyanate or toluylene-diisocyanates are used as the fixing agent.
Claim 10
Dependent Claim 25 words
A process according to claim 1, wherein the masked isocyanate is an addition product of hexamethylene-diisocyanate or toluylene-diisocyanate with malonic acid diethyl ester or pentachlorophenol.
Claim 11
Dependent Claim 15 words
A process according to claim 1, wherein the acylating agent is a poly acid chloride.
Claim 12
Dependent Claim 15 words
A process according to claim 1, wherein the acylating agent is a dicarboxylic acid anhydride.
Claim 13
Dependent Claim 15 words
A process according to claim 1 wherein textile materials from polyester or polyamide are treated.
Claim 14
Dependent Claim 15 words
A process according to claim 1, wherein treated textile material is subsequently rinsed and dried.
Claim 15
Dependent Claim 10 words
The treated dyed textile material obtained according to claim 13.
Claim 16
Dependent Claim 55 words
A process for dyeing polyamide or polyester textile material which comprises duyeing aid material with a disperse dyestuff containing at least one hyd roxyl or primary or secondary acylatable amino group and thereafter treating the dyed textile at a temperature above 80°C with a solution comprising an organic isocyanate or masked organic isocyanate in perchloretylene.
Claim 17
Dependent Claim 55 words
A process for dyeing polyamide or polyester textile material which comprises duyeing aid material with a disperse dyestuff containing at least one hyd roxyl or primary or secondary acylatable amino group and thereafter treating the dyed textile at a temperature above 80°C with a solution comprising an organic isocyanate or masked organic isocyanate in perchloretylene.
Claim 18
Dependent Claim 57 words
A process according to claim 15 wherein the isocyanate or masked isocyanate is selected from the group consisting of hexamethylene-diisocyanate, toluylene-diisocyanate, the reaction product of hexamethylene-diisocyanate with malonic acid diethyl ester, the reaction product of hexamethylenediisocyanate with pentachlorophenol, the reaction product of toluylene-dissocyanate with malonic acid diethyl ester, the reaction product of toluylene-diisocyanate with pentachlorophenol, tetramethylene-diisocyanate, ##SPC21##
Claim 19
Dependent Claim 24 words
The process of claim 1, wherein the textile material is dyed with a disperse dyestuff in a chlorinated aliphatic hydrocarbon boiling above about 100°C.
Claim 20
Dependent Claim 22 words
A process according to claim 17, wherein the dyeing and the aftertreatment are carried out in the same bath without intermediate rinsing.

References Cited (Backward Citations)

US3232692A Cited
FR1079766A Cited
GB729656A Cited
GB729643A Cited
US3066005A Cited
FR1250832A Cited
FR1277887A Cited
US3078138A Cited
US3265461A Cited
US3537808A Cited
GB1078894A Cited
US3782896A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-06-01 1979-12-01 1980-06-01 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-06-01 1983-12-01 1984-06-01 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-06-01 1987-12-01 1988-06-01 $7700.00 Window Closed / Lapsed

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