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US3957676A Expired / Lapsed US ⏱️ 0.0 years remaining

Chemical digestion of low level nuclear solid waste material

Assignee: Energy Research and Development Administration ERDA
•
Filing: 1972-09-22
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Granted: 1976-05-18
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Expires: 1992-09-22
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Abstract

Abstract A chemical digestion for treatment of low level combustible nuclear solid waste material is provided and comprises reacting the solid waste material with concentrated sulfuric acid at a temperature within the range of 230°-300°C and simultaneously and/or thereafter contacting the reacting mixture with concentrated nitric acid or nitrogen dioxide. In a special embodiment spent ion exchange resins are converted by this chemical digestion to noncombustible gases and a low volume noncombustible residue.

Inventors

  • 👤 Carl R. Cooley
  • 👤 Ronald E. Lerch

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 11:10
CPC Classifications
G; G21; G21F; G21F9/00; G21F9/28; G21F9/30

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 65 words
A method for processing low level light weight, bulky combustible nuclear solid waste material comprising the steps of reacting said solid waste material with concentrated sulfuric acid at a temperature within the range of 230° - 300°C and simultaneously and/or thereafter contacting said reacted waste with concentrated nitric acid or nitrogen oxides whereby carbonaceous material is oxidized to gaseous byproducts and a low volume residue.
Claim 2
Independent Claim 65 words
A method for processing low level light weight, bulky combustible nuclear solid waste material comprising the steps of reacting said solid waste material with concentrated sulfuric acid at a temperature within the range of 230° - 300°C and simultaneously and/or thereafter contacting said reacted waste with concentrated nitric acid or nitrogen oxides whereby carbonaceous material is oxidized to gaseous byproducts and a low volume residue.
Claim 3
Dependent Claim 19 words
The method of claim 1 wherein said solid waste material comprises a heterogeneous mixture of organic and inorganic materials.
Claim 4
Dependent Claim 15 words
The method of claim 1 wherein said solid waste material comprises spent ion exchange resins.
Claim 5
Dependent Claim 38 words
The method of claim 1 wherein said reaction step is conducted by incremental additions of solid waste material and said contacting step is conducted by incremental additions of nitric acid or nitrogen oxides to said solid waste material.
Claim 6
Dependent Claim 27 words
The method of claim 1 including the additional steps of separating said low volume residue from the resulting aqueous solution, neutralizing said residue and drying the residue.
Claim 7
Dependent Claim 20 words
The method of claim 1 wherein said low level solid waste material includes uranium - and plutonium - bearing material.

References Cited (Backward Citations)

US2733126A Cited
US2741541A Cited
US2849278A Cited
US2955019A Cited
US3557013A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-05-18 1979-11-17 1980-05-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-05-18 1983-11-17 1984-05-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-05-18 1987-11-17 1988-05-18 $7700.00 Window Closed / Lapsed

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