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US3956009A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for drying fructose solutions

Assignee: WR Grace and Co
•
Filing: 1975-05-14
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Granted: 1976-05-11
•
Expires: 1995-05-14
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Abstract

Abstract A process for preparing dried, solid, particulate fructose products from fructose solutions by drying the solution in a current of heated air and in the presence of separately introduced recycled dried product solids.

Inventors

  • 👤 Joseph Theodore Lundquist, Jr.
  • 👤 Preston Leonard Veltman
  • 👤 Edward Theodore Woodruff

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 22:30
CPC Classifications
B; B01; B01D; B01D1/00; B01D1/16; B01D1/18; C; C13; C13K; C13K11/00

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 86 words
A process for preparing dried solid fructose particulate free-flowing products from fructose solutions comprising: a. Drying dispersed fructose solution in a current of heated gas and in the presence of 1 to 10 parts by weight of separately introduced recycled product solids per part by weight of solids in the solution to be dried; and b. Supplying the hot drying gas at an outlet temperature of 60° to 120° C while maintaining average product residence time in the drying zone at about 30 seconds or less.
Claim 2
Dependent Claim 86 words
A process for preparing dried solid fructose particulate free-flowing products from fructose solutions comprising: a. Drying dispersed fructose solution in a current of heated gas and in the presence of 1 to 10 parts by weight of separately introduced recycled product solids per part by weight of solids in the solution to be dried; and b. Supplying the hot drying gas at an outlet temperature of 60° to 120° C while maintaining average product residence time in the drying zone at about 30 seconds or less.
Claim 3
Dependent Claim 22 words
The process of claim 1 in which the hot drying gas inlet temperature is in the range of from 100 to 300°C.
Claim 4
Dependent Claim 20 words
The process of claim 2 in which the average product residence time is maintained between 4 seconds and 30 seconds.
Claim 5
Dependent Claim 122 words
A process for preparing dry fructose products comprising: a. dispersing fructose particles having a particle size of less than about 500 microns in a current of heated air having an inlet temperature of at least 100°C; b. separately dispersing in the heated gas from about 1 to about 0.1 parts by weight, dry solids basis, of a fructose solution, per part by weight of said particles; c. evaporating the water from the solution; d. separating the resulting dry product from the hot gas stream having a temperature of 60 to 120°C; e. recycling the necessary amounts of dry product material from step (d) to provide the particles used in the dispersion step (a); and f. recovering the remainder of the dry product.
Claim 6
Dependent Claim 122 words
A process for preparing dry fructose products comprising: a. dispersing fructose particles having a particle size of less than about 500 microns in a current of heated air having an inlet temperature of at least 100°C; b. separately dispersing in the heated gas from about 1 to about 0.1 parts by weight, dry solids basis, of a fructose solution, per part by weight of said particles; c. evaporating the water from the solution; d. separating the resulting dry product from the hot gas stream having a temperature of 60 to 120°C; e. recycling the necessary amounts of dry product material from step (d) to provide the particles used in the dispersion step (a); and f. recovering the remainder of the dry product.
Claim 7
Dependent Claim 32 words
The process of claim 4 wherein the product recycled in step (e) is reduced to an average particle size of about 200 microns or less before introduction to the dispersion step (a).
Claim 8
Dependent Claim 28 words
The process of claim 5 wherein the size reduction is sufficient to provide an average particle size within the range of from about 50 to about 200 microns.
Claim 9
Dependent Claim 20 words
The process of claim 4 wherein the product obtained at step (d) is conditioned until the product is free flowing.
Claim 10
Dependent Claim 18 words
The process of claim 4 wherein the fructose solution contains 30 to 100 percent by weight fructose solids.
Claim 11
Dependent Claim 18 words
The process of claim 8 wherein the solution contains less than 58 percent by weight non-fructose sugar solids.

References Cited (Backward Citations)

US3477874A Cited
US3513023A Cited
US3600222A Cited
US3684573A Cited
US3674557A Cited
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US3704169A Cited
US3706599A Cited
US3883365A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-05-11 1979-11-10 1980-05-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-05-11 1983-11-10 1984-05-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-05-11 1987-11-10 1988-05-11 $7700.00 Window Closed / Lapsed

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