Patent US3948799A successfully refreshed from Google Patents.
US3948799A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for preparing silica organosols
Assignee: ChampionX LLC
•
Filing: 1973-09-28
•
Granted: 1976-04-06
•
Expires: 1993-09-28
Abstract
Abstract Silica organosols are described which comprise hydroxy free organic solvents as the continuous phase and as the discontinuous phase which is uniformly dispersed throughout the hydroxy free organic liquid, discrete dense particles of colloidal silica having a particle size within the range of 3 - 100 mu. Also described is a method for preparing these silica sols which comprise adding hydroxy free organic solvents to commercially available aqueous silica sols and then removing the water from the mixture by distillation.
Inventors
- 👤 David P. Schaefer
- 👤 Linda J. Pluta
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 18:08
CPC Classifications
C; C01; C01B; C01B33/00; C01B33/113; C01B33/12; C01B33/14; C01B33/145
Claims Analysis
Total Claims: 3
Claim 1
Independent Claim
141 words
A process for preparing a silica organosol which comprises the steps of: A. adding a hydroxy free organic liquid having a dipole moment in Debye Units greater than 3 to an aqueous colloidal silica sol said silica sol composed of discrete silica particles having an average particle size diameter of 3-300 mμ, said sol further characterized as having a silica concentration of from 10-60% by weight silica expressed as SiO 2 ; while, B. simultaneously removing water from the aqueous colloidal silica sol until the water content has been reduced to not more than 5% by weight and the amount of hydroxy free organic liquid added is an amount sufficient to produce a product of not greater than 60% SiO 2 ; and then, C. recovering a silica organosol comprised of silica particles uniformly dispersed in the hydroxy free organic liquid.
Claim 2
Dependent Claim
141 words
A process for preparing a silica organosol which comprises the steps of: A. adding a hydroxy free organic liquid having a dipole moment in Debye Units greater than 3 to an aqueous colloidal silica sol said silica sol composed of discrete silica particles having an average particle size diameter of 3-300 mμ, said sol further characterized as having a silica concentration of from 10-60% by weight silica expressed as SiO 2 ; while, B. simultaneously removing water from the aqueous colloidal silica sol until the water content has been reduced to not more than 5% by weight and the amount of hydroxy free organic liquid added is an amount sufficient to produce a product of not greater than 60% SiO 2 ; and then, C. recovering a silica organosol comprised of silica particles uniformly dispersed in the hydroxy free organic liquid.
Claim 3
Dependent Claim
13 words
The process of claim 1 where the hydroxy free organic liquid is dimethylformamide.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-04-06 | 1979-10-06 | 1980-04-06 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-04-06 | 1983-10-06 | 1984-04-06 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-04-06 | 1987-10-06 | 1988-04-06 | $7700.00 | Window Closed / Lapsed |