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US3941584A Expired / Lapsed US ⏱️ 0.0 years remaining

Production of reflective metal flake pigments

Assignee: Huntington Alloys Corp
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Filing: 1974-06-19
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Granted: 1976-03-02
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Expires: 1994-06-19
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Abstract

Abstract Directed to a metal flake powder of a stain-resistant metal or alloy and a process for producing the same wherein a metal powder of -100 mesh size is ball milled in a mobile liquid medium wherein the ratio of mobile liquid to powder being milled is at least about 10 to 1, e.g., about 25:1 to about 50:1.

Inventors

  • 👤 John Hayes Tundermann
  • 👤 John Herbert Harrington

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 20:05
CPC Classifications
B; B22; B22F; B22F9/00; B22F9/02; B22F9/04; B22F1/00; B22F1/06; B22F1/068; C; C09; C09C; C09C1/00; C09C1/62; C09C1/622; C09C1/66; B22F2009/041; B22F2009/043; B22F2998/00; C01; C01P; C01P2004/00; C01P2004/01; C01P2004/03; C01P2004/20; C01P2004/60; C01P2004/61; C01P2004/62; C01P2006/00; C01P2006/10; C01P2006/12; C01P2006/32; C01P2006/33; C01P2006/34; C01P2006/60; Y; Y10; Y10T; Y10T428/00; Y10T428/29; Y10T428/2982

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 181 words
A metal flake powder consisting essentially of solid opaque flakes of metal each flake having a thickness of less than one micron; said flakes having essentially smooth, defect free, mechanically formed faces with major dimensions of about 10 to 40 microns; said powder being capable of being formed as a water floated layer and exhibiting, when formed as a water floated layer of minus 325 mesh particles a high specular reflectance of at least 30 percent as measured by aiming a beam of parallel light rays generated by a tungsten filament light source at an angle of 30° from the vertical and detecting the specularly reflected light, as affected by the absorption characteristics of the material tested, by a photo cell sensitive in the range of 300 to 700 millimicrons wavelength; and said metal flakes being coated with a thin lubricant film adapted to provide leafing characteristics to said flakes when said lubricant film is not wetted by a coating composition vehicle and to provide non-leafing characteristics to said flakes when said lubricant film is wetted by a coating composition vehicle.
Claim 2
Dependent Claim 181 words
A metal flake powder consisting essentially of solid opaque flakes of metal each flake having a thickness of less than one micron; said flakes having essentially smooth, defect free, mechanically formed faces with major dimensions of about 10 to 40 microns; said powder being capable of being formed as a water floated layer and exhibiting, when formed as a water floated layer of minus 325 mesh particles a high specular reflectance of at least 30 percent as measured by aiming a beam of parallel light rays generated by a tungsten filament light source at an angle of 30° from the vertical and detecting the specularly reflected light, as affected by the absorption characteristics of the material tested, by a photo cell sensitive in the range of 300 to 700 millimicrons wavelength; and said metal flakes being coated with a thin lubricant film adapted to provide leafing characteristics to said flakes when said lubricant film is not wetted by a coating composition vehicle and to provide non-leafing characteristics to said flakes when said lubricant film is wetted by a coating composition vehicle.
Claim 3
Dependent Claim 23 words
A metal flake powder in accordance with claim 1 wherein the average flake thickness is in the range of 0.27 to 0.94 micron.
Claim 4
Dependent Claim 18 words
A metal flake powder as in claim 1 wherein each flake is characterized by generally rounded smooth edges.
Claim 5
Dependent Claim 64 words
A metal flake powder in accordance with claim 1 having a composition containing, by weight, up to about 90% copper, up to about 10% maganese, up to about 3% molybdenum, up to about 70% zinc, up to about 70% tin, up to about 10% silver, and the balance essentially a metal from the group consisting of nickel, iron, cobalt, chromium and the platinum-group metals.
Claim 6
Dependent Claim 44 words
A metal flake powder in accordance with claim 1 made of a metal from the group consisting of nickel; cobalt; alloys of nickel, iron and cobalt with each other and with, optionally, chromium; stainless steels; nickel-copper alloys; nickel-chromium alloys; nickel-chromium-iron alloys and nickel-silver alloys.
Claim 7
Dependent Claim 22 words
A metal flake powder in accordance with claim 1 having a thickness of less than 1 micron and made of carbonyl nickel.
Claim 8
Dependent Claim 23 words
A metal flake powder in accordance with claim 1 having a thickness of less than 1 micron and made of a stainless steel.
Claim 9
Dependent Claim 20 words
A metal flake powder in accordance with claim 1 wherein said metal has a melting point of at least 1100°C.
Claim 10
Dependent Claim 19 words
A metal flake powder in accordance with claim 1 wherein said metal has a density of at least 7.5.

References Cited (Backward Citations)

US2666714A Cited
US2839378A Cited
US3234038A Cited
US3389105A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-03-02 1979-09-01 1980-03-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-03-02 1983-09-01 1984-03-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-03-02 1987-09-01 1988-03-02 $7700.00 Window Closed / Lapsed

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