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US3940545A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for binding siliceous fibers

Assignee: Individual
•
Filing: 1974-05-23
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Granted: 1976-02-24
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Expires: 1994-05-23
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Abstract

Abstract A process for reducing the static charge and binding glass fibers is disclosed, wherein the glass fibers are contacted with a composition comprising an alkylene polyol, such as an alkylene glycol, a lower alkanol, a polybasic acid, and a siliconate compound. The composition is applied to siliceous fibers, especially glass fibers, in either loose or blanket form, to reduce the static charge thereon and to function as a binder for the fibers. Glass fibers treated by the composition of the present invention are useful in various applications such as for blown insulation.

Inventors

  • 👤 A. Carey Williams

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-10 01:26
CPC Classifications
C; C03; C03C; C03C25/00; C03C25/10; C03C25/24; C03C25/40; C03C25/25; Y; Y10; Y10S; Y10S428/00; Y10S428/92; Y10S428/921; Y10T; Y10T428/00; Y10T428/29; Y10T428/2913; Y10T428/2933; Y10T428/2964

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 191 words
Process for reducing the static charge and binding siliceous fibers, said process comprising first forming an aqueous composition comprising about 30 to about 70 percent by weight of water, 1 part of at least 1 lower alkanol of 1 to 4 carbon atoms, about 0.8-4 parts of at least 1 polybasic water-soluble acid having 2 or 3 acidic groups per molecule and a molecular weight of less than about 250, about 1-5 parts by weight of a lower alkylene polyol or poly(lower alkylene glycol), and about 0.1-1 parts of at least 1 water-soluble siliconate which reduces the surface tension of pure distilled water by at least 50 percent when used in an amount of 0.4 weight percent therein, wherein said lower alkanol and said lower alkylene polyol or poly(lower alkylene glycol) are mixed together prior to the addition thereto of said polybasic acid, applying the resulting composition to siliceous fibers at a temperature from about 35° to about 100°F in an amount corresponding to at least 1 oz. of said composition per 30 lbs. of siliceous fibers, and then drying said fibers to form a dried coating of said composition thereon.
Claim 2
Dependent Claim 191 words
Process for reducing the static charge and binding siliceous fibers, said process comprising first forming an aqueous composition comprising about 30 to about 70 percent by weight of water, 1 part of at least 1 lower alkanol of 1 to 4 carbon atoms, about 0.8-4 parts of at least 1 polybasic water-soluble acid having 2 or 3 acidic groups per molecule and a molecular weight of less than about 250, about 1-5 parts by weight of a lower alkylene polyol or poly(lower alkylene glycol), and about 0.1-1 parts of at least 1 water-soluble siliconate which reduces the surface tension of pure distilled water by at least 50 percent when used in an amount of 0.4 weight percent therein, wherein said lower alkanol and said lower alkylene polyol or poly(lower alkylene glycol) are mixed together prior to the addition thereto of said polybasic acid, applying the resulting composition to siliceous fibers at a temperature from about 35° to about 100°F in an amount corresponding to at least 1 oz. of said composition per 30 lbs. of siliceous fibers, and then drying said fibers to form a dried coating of said composition thereon.
Claim 3
Dependent Claim 21 words
Process as claimed in claim 1, wherein said composition additionally contains a coupling amount of at least 1 silane coupling agent.
Claim 4
Dependent Claim 13 words
Process as claimed in claim 1, wherein said alkylene glycol is ethylene glycol.
Claim 5
Dependent Claim 12 words
Process as claimed in claim 3, wherein said lower alkanol is ethanol.
Claim 6
Dependent Claim 14 words
Process as claimed in claim 4, wherein said polybasic water-soluble acid is citric acid.
Claim 7
Dependent Claim 14 words
Process as claimed in claim 5, wherein said water-soluble siliconate is methyl sodium siliconate.
Claim 8
Dependent Claim 15 words
Process as claimed in claim 1, wherein said composition is applied to chopped glass fibers.
Claim 9
Dependent Claim 21 words
Process as claimed in claim 7, wherein said chopped glass fibers are entrained in an airstream when contacted by said composition.
Claim 10
Dependent Claim 12 words
Blown glass fiber insulation when produced by the process of claim 8.

References Cited (Backward Citations)

US2393863A Cited
US2556045A Cited
US2990307A Cited
US3405001A Cited
US3287096A Cited
US3567570A Cited
US3702783A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-02-23 1979-08-25 1980-02-24 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-02-23 1983-08-25 1984-02-24 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-02-23 1987-08-25 1988-02-24 $7700.00 Window Closed / Lapsed

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