US3940545A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for binding siliceous fibers
Assignee: Individual
•
Filing: 1974-05-23
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Granted: 1976-02-24
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Expires: 1994-05-23
Abstract
Abstract A process for reducing the static charge and binding glass fibers is disclosed, wherein the glass fibers are contacted with a composition comprising an alkylene polyol, such as an alkylene glycol, a lower alkanol, a polybasic acid, and a siliconate compound. The composition is applied to siliceous fibers, especially glass fibers, in either loose or blanket form, to reduce the static charge thereon and to function as a binder for the fibers. Glass fibers treated by the composition of the present invention are useful in various applications such as for blown insulation.
Inventors
- 👤 A. Carey Williams
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-10 01:17
CPC Classifications
C; C03; C03C; C03C25/00; C03C25/10; C03C25/24; C03C25/40; C03C25/25; Y; Y10; Y10S; Y10S428/00; Y10S428/92; Y10S428/921; Y10T; Y10T428/00; Y10T428/29; Y10T428/2913; Y10T428/2933; Y10T428/2964
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
191 words
Process for reducing the static charge and binding siliceous fibers, said process comprising first forming an aqueous composition comprising about 30 to about 70 percent by weight of water, 1 part of at least 1 lower alkanol of 1 to 4 carbon atoms, about 0.8-4 parts of at least 1 polybasic water-soluble acid having 2 or 3 acidic groups per molecule and a molecular weight of less than about 250, about 1-5 parts by weight of a lower alkylene polyol or poly(lower alkylene glycol), and about 0.1-1 parts of at least 1 water-soluble siliconate which reduces the surface tension of pure distilled water by at least 50 percent when used in an amount of 0.4 weight percent therein, wherein said lower alkanol and said lower alkylene polyol or poly(lower alkylene glycol) are mixed together prior to the addition thereto of said polybasic acid, applying the resulting composition to siliceous fibers at a temperature from about 35° to about 100°F in an amount corresponding to at least 1 oz. of said composition per 30 lbs. of siliceous fibers, and then drying said fibers to form a dried coating of said composition thereon.
Claim 2
Dependent Claim
191 words
Process for reducing the static charge and binding siliceous fibers, said process comprising first forming an aqueous composition comprising about 30 to about 70 percent by weight of water, 1 part of at least 1 lower alkanol of 1 to 4 carbon atoms, about 0.8-4 parts of at least 1 polybasic water-soluble acid having 2 or 3 acidic groups per molecule and a molecular weight of less than about 250, about 1-5 parts by weight of a lower alkylene polyol or poly(lower alkylene glycol), and about 0.1-1 parts of at least 1 water-soluble siliconate which reduces the surface tension of pure distilled water by at least 50 percent when used in an amount of 0.4 weight percent therein, wherein said lower alkanol and said lower alkylene polyol or poly(lower alkylene glycol) are mixed together prior to the addition thereto of said polybasic acid, applying the resulting composition to siliceous fibers at a temperature from about 35° to about 100°F in an amount corresponding to at least 1 oz. of said composition per 30 lbs. of siliceous fibers, and then drying said fibers to form a dried coating of said composition thereon.
Claim 3
Dependent Claim
21 words
Process as claimed in claim 1, wherein said composition additionally contains a coupling amount of at least 1 silane coupling agent.
Claim 4
Dependent Claim
13 words
Process as claimed in claim 1, wherein said alkylene glycol is ethylene glycol.
Claim 5
Dependent Claim
12 words
Process as claimed in claim 3, wherein said lower alkanol is ethanol.
Claim 6
Dependent Claim
14 words
Process as claimed in claim 4, wherein said polybasic water-soluble acid is citric acid.
Claim 7
Dependent Claim
14 words
Process as claimed in claim 5, wherein said water-soluble siliconate is methyl sodium siliconate.
Claim 8
Dependent Claim
15 words
Process as claimed in claim 1, wherein said composition is applied to chopped glass fibers.
Claim 9
Dependent Claim
21 words
Process as claimed in claim 7, wherein said chopped glass fibers are entrained in an airstream when contacted by said composition.
Claim 10
Dependent Claim
12 words
Blown glass fiber insulation when produced by the process of claim 8.
References Cited (Backward Citations)
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-02-23 | 1979-08-25 | 1980-02-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-02-23 | 1983-08-25 | 1984-02-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-02-23 | 1987-08-25 | 1988-02-24 | $7700.00 | Window Closed / Lapsed |