Process of manufacturing a porous, stainless steel filter element and sealing it in a tubular fitting, and resulting filter

Claim 2

A process for manufacturing a sintered, porous stainless steel filter for use in medical injection and infusion equipment and the like; said filter being manufactured from stainless steel particles having an irregular or dendritic shape with arm-like projections extending outwardly therefrom; said process comprising the steps of: screening dendritic stainless steel particles to obtain particles of a predetermined size; mixing the screened particles with a lubricant; loading the particle-lubricant mixture into a mold of desired shape; compacting the particle-lubricant mixture in the mold at a predetermined compaction pressure to cause the arm-like projections on the particles to engage and interlock with one another and form a self-supporting, porous, green filter; heating the green filter at a predetermined temperature to burn off the lubricant; and sintering the filter to form a sintered, porous, stainless steel filter.

Claim 3

A process of manufacturing a filter according to claim 1, wherein said screening step comprises screening stainless steel particles to obtain particles having mean diameters of between about 44 and 74 micrometers.

Claim 4

A process of manufacturing a filter according to claim 2, wherein the mixture is compacted to a density of about 5.6 gm/cm 3 .

Claim 5

The product of the process of claim 3.

Claim 6

The product of the process of claim 2.

Claim 7

A process of manufacturing a filter according to claim 1, wherein said screening step comprises screening stainless steel particles to obtain particles having mean diameters of between about 125 and 149 micrometers.

Claim 8

A process of manufacturing a filter according to claim 6, wherein the mixture is compacted to a density of about 5.4 gm/cm 3 .

Claim 9

The product of the process of claim 7.

Claim 10

The product of the process of claim 6.

Claim 11

A process of manufacturing a filter according to claim 1, wherein said step of mixing the screened particles with a lubricant comprises mixing the screened particles with a synthetic wax of general fatty acid origin.

Claim 12

The product of the process of claim 10.

Claim 13

A process of manufacturing a filter according to claim 1, wherein said step of sintering said filter comprises heating said filter at a temperature of between about 2000°F, and about 2400°F, for about 30 minutes.

Claim 14

The product of the process of claim 12.

Claim 15

The product of the process of claim 1.

Claim 16

A process for manufacturing a porous filter fir use in medical injection and infusion equipment and the like, said filter being manufactured from metal particles having an irregular or dendritic shape with arm-like projections extending outwardly therefrom; said process comprising the steps of: screening dendritic metal particles to obtain dendritic particles of a predetermined size; mixing the screened dendritic particles with a lubricant; loading the particle-lubricant mixture into a mold; compacting the particle-lubricant mixture in the mold at a predetermined compaction pressure to cause the arm-like projections on the particles to engage and interlock with one another and form a self-supporting green article; heating the green article at a predetermined temperature to burn off the lubricant; and sintering the filter to form a sintered, porous metal filter.

Claim 17

A process for manufacturing a porous filter fir use in medical injection and infusion equipment and the like, said filter being manufactured from metal particles having an irregular or dendritic shape with arm-like projections extending outwardly therefrom; said process comprising the steps of: screening dendritic metal particles to obtain dendritic particles of a predetermined size; mixing the screened dendritic particles with a lubricant; loading the particle-lubricant mixture into a mold; compacting the particle-lubricant mixture in the mold at a predetermined compaction pressure to cause the arm-like projections on the particles to engage and interlock with one another and form a self-supporting green article; heating the green article at a predetermined temperature to burn off the lubricant; and sintering the filter to form a sintered, porous metal filter.

Claim 18

The product of the process of claim 15.

Claim 19

A process for making a filter device of metal particles for medical injection and infusion equipment and the like, said filter of said filter device being manufactured from metal particles having an irregular or dendritic shape with arm-like projections extending outwardly therefrom; said process comprising the steps of: screening the metal particles to obtain particles of a predetermined size; mixing the screened particles with a lubricant; loading the particle-lubricant mixture into a mold; compacting the particle-lubricant mixture in the mold at a predetermined compaction pressure to cause the arm-like projections on the particles to engage and interlock with one another and, form a self-supporting green filter article having a porous, axially-extending outer peripheral wall; heating the green filter article at a predetermined temperature to burn off the lubricant; sintering the filter to form a sintered, porous metal filter; and inserting the filter into the interior peripheral wall of an at least partially plastic peripheral member having an axially-extending interior peripheral wall so that at least a continuous peripheral portion of said interior peripheral wall is in contact with said axially-extending outer peripheral surface of said filter; and heating said filter to a temperature sufficient to cause at least a portion of the interior peripheral wall of said peripheral member to flow into the pores of said filter.

Claim 20

A process for making a filter device of metal particles for medical injection and infusion equipment and the like, said filter of said filter device being manufactured from metal particles having an irregular or dendritic shape with arm-like projections extending outwardly therefrom; said process comprising the steps of: screening the metal particles to obtain particles of a predetermined size; mixing the screened particles with a lubricant; loading the particle-lubricant mixture into a mold; compacting the particle-lubricant mixture in the mold at a predetermined compaction pressure to cause the arm-like projections on the particles to engage and interlock with one another and, form a self-supporting green filter article having a porous, axially-extending outer peripheral wall; heating the green filter article at a predetermined temperature to burn off the lubricant; sintering the filter to form a sintered, porous metal filter; and inserting the filter into the interior peripheral wall of an at least partially plastic peripheral member having an axially-extending interior peripheral wall so that at least a continuous peripheral portion of said interior peripheral wall is in contact with said axially-extending outer peripheral surface of said filter; and heating said filter to a temperature sufficient to cause at least a portion of the interior peripheral wall of said peripheral member to flow into the pores of said filter.

Claim 21

The product of the process of claim 17.

Claim 22

A process of making a filter device for medical injection and infusion equipment and the like, said filter of said filter device being manufactured from metal particles having an irregular or dendritic shape with arm-like projections extending outwardly therefrom; said process comprising the steps of: compacting the metal particles in a mold in the substantial absence of a binder to cause the arm-like projections on adjacent particles to interlock with one another and form a self-supporting, porous, green article; and sintering said green article to produce a sintered, porous metal filter; inserting the filter into the interior peripheral wall of an at least partially plastic peripheral member, and heating said filter to a temperature sufficient to cause at least a portion of the interior peripheral wall of said peripheral member to flow into the pores of said filter.

Claim 23

A process of making a filter device for medical injection and infusion equipment and the like, said filter of said filter device being manufactured from metal particles having an irregular or dendritic shape with arm-like projections extending outwardly therefrom; said process comprising the steps of: compacting the metal particles in a mold in the substantial absence of a binder to cause the arm-like projections on adjacent particles to interlock with one another and form a self-supporting, porous, green article; and sintering said green article to produce a sintered, porous metal filter; inserting the filter into the interior peripheral wall of an at least partially plastic peripheral member, and heating said filter to a temperature sufficient to cause at least a portion of the interior peripheral wall of said peripheral member to flow into the pores of said filter.

Claim 24

The product of the process of claim 19.

Claim 25

A process for manufacturing a filter device for medical injection and infusion equipment and the like, said filter of said filter device being manufactured from metal particles having an irregular or dendritic shape with arm-like projections extending outwardly therefrom; said process comprising the steps of: screening the metal particles to obtain particles of a predetermined size; mixing the screened particles with a lubricant; loading the particle-lubricant mixture into a mold; compacting the particle-lubricant mixture in the mold at a predetermined compaction pressure to cause the arm-like projections on the particles to engage and interlock with one another and form a selfsupporting green article; heating the green filter article at a predetermined temperature to burn off the lubricant; sintering the filter article to form a sintered, porous metal filter; force-fitting said filter into a plastic annular projection within the interior peripheral wall of a tubular member; and heating said filter to a temperature sufficient to cause a peripheral portion of the interior peripheral wall of said plastic annulus to soften and flow into pores in such filter to form a continuous peripheral seal between said tubular member and said filter.

Claim 26

A process for manufacturing a filter device for medical injection and infusion equipment and the like, said filter of said filter device being manufactured from metal particles having an irregular or dendritic shape with arm-like projections extending outwardly therefrom; said process comprising the steps of: screening the metal particles to obtain particles of a predetermined size; mixing the screened particles with a lubricant; loading the particle-lubricant mixture into a mold; compacting the particle-lubricant mixture in the mold at a predetermined compaction pressure to cause the arm-like projections on the particles to engage and interlock with one another and form a selfsupporting green article; heating the green filter article at a predetermined temperature to burn off the lubricant; sintering the filter article to form a sintered, porous metal filter; force-fitting said filter into a plastic annular projection within the interior peripheral wall of a tubular member; and heating said filter to a temperature sufficient to cause a peripheral portion of the interior peripheral wall of said plastic annulus to soften and flow into pores in such filter to form a continuous peripheral seal between said tubular member and said filter.

Claim 27

The product of the process of claim 21.