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US3933473A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for recovering a usable alloy from titanium scrap

Assignee: Airco Inc
•
Filing: 1973-10-19
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Granted: 1976-01-20
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Expires: 1993-10-19
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Abstract

Abstract A method for recovering a usable alloy consisting of 2.5 - 3.5% aluminum, 1.7 - 2.50% tin and balance titanium from titanium scrap is disclosed. The method comprises cleaning the scrap, charging the cleaned scrap into an electron beam furnace and refining the charge under a hard vacuum so as to attain a predetermined composition.

Inventors

  • 👤 James Dickson

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 16:12
CPC Classifications
C; C22; C22B; C22B7/00; C22B7/001; C22B7/003; C22B9/00; C22B9/16; C22B9/22; C22B9/228; C22C; C22C14/00; Y; Y02; Y02P; Y02P10/00; Y02P10/20

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 248 words
The method of obtaining a weldable, forgeable, ductile, corrosion resistant product alloy from scrap metal alloy of a major component of titanium having additives including at least in excess of 2 per cent of aluminum, and comprising not in excess of about 2 per cent interstitial impurities including one or more of the elements nitrogen, carbon, hydrogen and oxygen, which comprises the steps of: cleansing the said scrap metal to remove scale comprising oxides and nitrides and hydrocarbons, charging said cleansed scrap metal into a furnace in a vacuum-tight housing evacuated to a pressure not exceeding about 5 × 10.sup. -4 torr, said furnace comprising an open-faced hearth section having an inlet end and a casting station spaced apart from and disposed downstream from said inlet end, melting the said scrap metal charge in said furnace by electron beam bombardment at the inlet end of said hearth section thereby causing said molten charge to drip down onto said open-faced hearth section to form a stream flowing along said hearth section in the direction of said casting station, exposing said molten scrap stream flowing along said hearth section to further electron beam bombardment at one or more points spaced apart from said inlet end causing the higher vapor pressure elements thereof including at least a portion of said aluminum to become volatilized and distilled off, and collecting the remaining portion of said molten scrap stream in said casting station permitting it to flow into and solidify in a mold.
Claim 2
Independent Claim 248 words
The method of obtaining a weldable, forgeable, ductile, corrosion resistant product alloy from scrap metal alloy of a major component of titanium having additives including at least in excess of 2 per cent of aluminum, and comprising not in excess of about 2 per cent interstitial impurities including one or more of the elements nitrogen, carbon, hydrogen and oxygen, which comprises the steps of: cleansing the said scrap metal to remove scale comprising oxides and nitrides and hydrocarbons, charging said cleansed scrap metal into a furnace in a vacuum-tight housing evacuated to a pressure not exceeding about 5 × 10.sup. -4 torr, said furnace comprising an open-faced hearth section having an inlet end and a casting station spaced apart from and disposed downstream from said inlet end, melting the said scrap metal charge in said furnace by electron beam bombardment at the inlet end of said hearth section thereby causing said molten charge to drip down onto said open-faced hearth section to form a stream flowing along said hearth section in the direction of said casting station, exposing said molten scrap stream flowing along said hearth section to further electron beam bombardment at one or more points spaced apart from said inlet end causing the higher vapor pressure elements thereof including at least a portion of said aluminum to become volatilized and distilled off, and collecting the remaining portion of said molten scrap stream in said casting station permitting it to flow into and solidify in a mold.
Claim 3
Dependent Claim 26 words
The method as defined in claim 1 wherein said scrap metal is cleansed in a detergent maintained at a temperature of between 80° and 90° centigrade.
Claim 4
Dependent Claim 23 words
The method as defined in claim 1 wherein said furnace is evacuated to a pressure not exceeding about 2 × 10.sup. -4 torr.
Claim 5
Dependent Claim 8 words
The product of the process of claim 1.
Claim 6
Dependent Claim 27 words
A method as defined in claim 1 in which the scrap metal alloy comprises a blend of titanium alloys having substantially the formulation Ti--5Al--2 1/2Sn and Ti--6Al--4V.
Claim 7
Dependent Claim 19 words
A method as defined in claim 1 wherein said scrap metal alloy consists essentially of the alloy Ti--5Al--2 1/2Sn.
Claim 8
Dependent Claim 18 words
A method as defined in claim 1 wherein said scrap metal alloy consists essentially of the alloy Ti--6Al--4V.
Claim 9
Dependent Claim 18 words
A method as defined in claim 1 wherein said scrap metal alloy comprises primarily machine turnings and chips.
Claim 10
Dependent Claim 47 words
A method as defined in claim 1 wherein said scrap metal alloy contains between about 4 and 6 percent by weight of aluminum, between about 2 and 3 percent by weight of tin, between about 0.18 and 0.40 percent by weight of oxygen and the balance titanium.
Claim 11
Dependent Claim 33 words
A method as defined in claim 1 in which the composition of said product alloy falls essentially by weight percent within the limits 1-3.5% Al, 1.3-2.5% Sn, 0.23-0.32% oxygen and the balance Ti.

References Cited (Backward Citations)

US2734244A Cited
US2548897A Cited
US2866700A Cited
US2813921A Cited
US3005246A Cited
US3342250A Cited
US3660074A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-01-19 1979-07-21 1980-01-20 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-01-19 1983-07-21 1984-01-20 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-01-19 1987-07-21 1988-01-20 $7700.00 Window Closed / Lapsed

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