Patent US3931036A successfully refreshed from Google Patents.
US3931036A
Expired / Lapsed
US
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Compacted alkali metal silicate
Assignee: PQ Corp
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Filing: 1974-05-13
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Granted: 1976-01-06
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Expires: 1994-05-13
Abstract
Abstract This invention generally relates to the production of alkali metal silicates. More particularly the invention relates to the production of compressed alkali metal silicate granules of desirable density and particle properties.
Inventors
- 👤 Richard H. Pierce
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 06:28
CPC Classifications
B; B01; B01J; B01J2/00; B01J2/22; C; C01; C01B; C01B33/00; C01B33/20; C01B33/32; C01B33/325
Claims Analysis
Total Claims: 14
Claim 1
Independent Claim
199 words
In the known process of preparing product granules of hydrated alkali metal silicate with a particle size larger than 100 mesh, a mol ratio of SiO 2 /M 2 O between 1.6/1.0 and 4.0/1.0 wherein M stands for an alkali metal, a bulk density of 35 to 75 lbs/ft 3 and a moisture content of 12 to 26%, the improvement comprising: a. preparing a damp, uniform mixture of 90 to 97% alkali metal silicate powder and 3 to 10% alkali metal silicate solution by: 1. maintaining said alkali metal silicate powder with a moisture content of 10 to 20% and a particle size of less than 100 mesh in motion while adding to said powder the alkali metal silicate solution containing 25 to 45% silicate solids in 1 to 4 minutes, and 2. blending said mixture for 1 to 4 minutes by maintaining it in motion; b. subjecting said mixture to a pressure between 500 and 2500 psi, thereby forming a compacted sheet of 1/32 to 1/8 inch thickness; c. aging the compacted material for 5 to 15 minutes; and d. granulating said sheet and recovering 50 to 75% of the resulting granules that are larger than 100 mesh.
Claim 2
Dependent Claim
199 words
In the known process of preparing product granules of hydrated alkali metal silicate with a particle size larger than 100 mesh, a mol ratio of SiO 2 /M 2 O between 1.6/1.0 and 4.0/1.0 wherein M stands for an alkali metal, a bulk density of 35 to 75 lbs/ft 3 and a moisture content of 12 to 26%, the improvement comprising: a. preparing a damp, uniform mixture of 90 to 97% alkali metal silicate powder and 3 to 10% alkali metal silicate solution by: 1. maintaining said alkali metal silicate powder with a moisture content of 10 to 20% and a particle size of less than 100 mesh in motion while adding to said powder the alkali metal silicate solution containing 25 to 45% silicate solids in 1 to 4 minutes, and 2. blending said mixture for 1 to 4 minutes by maintaining it in motion; b. subjecting said mixture to a pressure between 500 and 2500 psi, thereby forming a compacted sheet of 1/32 to 1/8 inch thickness; c. aging the compacted material for 5 to 15 minutes; and d. granulating said sheet and recovering 50 to 75% of the resulting granules that are larger than 100 mesh.
Claim 3
Dependent Claim
32 words
The process of claim 1 wherein the alkali metal silicate powder has a SiO 2 /M 2 O mol ratio between 2.0/1.0 and 2.6/1.0 with a moisture content of 15 to 19%.
Claim 4
Dependent Claim
34 words
The process of claim 1 wherein the addition of the alkali metal silicate solution is completed in 1 to 2 minutes and the blending after the addition is completed in 1 to 2 minutes.
Claim 5
Dependent Claim
30 words
The process of claim 1 wherein said damp, uniform mixture of alkali metal silicate powder and alkali metal silicate solution is subjected to a pressure of 900 to 1600 psi.
Claim 6
Dependent Claim
33 words
The process of claim 1 wherein the alkali metal silicate powder of step (a) (1) includes 75 to 90% hydrated alkali metal silicate powder and 10 to 50% anhydrous alkali metal silicate glass.
Claim 7
Dependent Claim
132 words
In the known process of preparing product granules of hydrated alkali metal silicate with a particle size larger than 100 mesh, a mol ratio of SiO 2 /M 2 O between 1.6/1.0 and 4.0/1.0 wherein M stands for an alkali metal, a bulk density of 35 to 75 lbs/ft 3 and a moisture content of 12 to 26%, the improvement comprising: a. preparing a damp, uniform mixture of 90 to 97% alkali metal silicate powder and 3 to 10% alkali metal silicate solution, by: 1. maintaining said alkali metal silicate powder with a moisture content of 10 to 20% and a particle size of less than 100 mesh in motion while adding to said powder the alkali metal silicate solution containing 25 to 45% silicate solids in 1 to 4 minutes, and
Claim 8
Dependent Claim
132 words
In the known process of preparing product granules of hydrated alkali metal silicate with a particle size larger than 100 mesh, a mol ratio of SiO 2 /M 2 O between 1.6/1.0 and 4.0/1.0 wherein M stands for an alkali metal, a bulk density of 35 to 75 lbs/ft 3 and a moisture content of 12 to 26%, the improvement comprising: a. preparing a damp, uniform mixture of 90 to 97% alkali metal silicate powder and 3 to 10% alkali metal silicate solution, by: 1. maintaining said alkali metal silicate powder with a moisture content of 10 to 20% and a particle size of less than 100 mesh in motion while adding to said powder the alkali metal silicate solution containing 25 to 45% silicate solids in 1 to 4 minutes, and
Claim 9
Dependent Claim
87 words
blending said mixture for 1 to 4 minutes by maintaining it in motion. b. subjecting said mixture to a pressure between 500 and 2500 psi, thereby forming a compacted sheet of 1/32 to 1/8 inch thickness; c. heating the compacted material to a temperature of 65° to 200°C for 3 to 8 minutes; d. cooling the compacted material to below 21°C in 1 to 10 minutes; and e. granulating said compacted material and recovering 50 to 75% of the resulting granules that are larger than 100 mesh.
Claim 10
Dependent Claim
87 words
blending said mixture for 1 to 4 minutes by maintaining it in motion. b. subjecting said mixture to a pressure between 500 and 2500 psi, thereby forming a compacted sheet of 1/32 to 1/8 inch thickness; c. heating the compacted material to a temperature of 65° to 200°C for 3 to 8 minutes; d. cooling the compacted material to below 21°C in 1 to 10 minutes; and e. granulating said compacted material and recovering 50 to 75% of the resulting granules that are larger than 100 mesh.
Claim 11
Dependent Claim
32 words
The process of claim 6 wherein the alkali metal silicate powder has a SiO 2 /M 2 O mol ratio between 2.0/1.0 and 2.6/1.0 with a moisture content of 15 to 19%.
Claim 12
Dependent Claim
34 words
The process of claim 6 wherein the addition of the alkali metal silicate solution is completed in 1 to 2 minutes and the blending after the addition is completed in 1 to 2 minutes.
Claim 13
Dependent Claim
30 words
The process of claim 6 wherein said damp, uniform mixture of alkali metal silicate powder and alkali metal silicate solution is subjected to a pressure of 900 to 1600 psi.
Claim 14
Dependent Claim
33 words
The process of claim 6 wherein the alkali metal silicate powder of step (a) (1) includes 75 to 90% hydrated alkali metal silicate powder and 10 to 50% anhydrous alkali metal silicate glass.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-01-05 | 1979-07-07 | 1980-01-06 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-01-05 | 1983-07-07 | 1984-01-06 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-01-05 | 1987-07-07 | 1988-01-06 | $7700.00 | Window Closed / Lapsed |