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US3929535A Expired / Lapsed US ⏱️ 0.0 years remaining

Color reversible, mirror surface glassy materials from plumbite-treated cellulosics

Assignee: United States Department of Agriculture
•
Filing: 1974-08-22
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Granted: 1975-12-30
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Expires: 1994-08-22
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Abstract

Abstract Colored glasslike materials have been produced from an uncolored transparent or translucent glassy intermediate which was made by heating plumbite-treated cellulosics in a limited oxygen atmosphere while in contact with a glass or ceramic surface. The uncolored intermediate can be caused to become either gold, silver or purplish black and mirrorlike by exposing it to the direct flame of a bunsen-type burner. The color may be removed by reheating the glassy material in an oven or by heating the back side with a bunsen-type burner when the glassy material is bound to a glass or ceramic holder. The color formation color removal may be repeated.

Inventors

  • 👤 Truman L Ward
  • 👤 Ruth R Benerito

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 21:52
CPC Classifications
B; B44; B44F; B44F1/00; B44F1/08; B44F1/10

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 203 words
A PROCESS FOR IMPARTING TO SILICA GLASS OR CERAMICS REVERSIBLE SURFACE COLORATIONS WHICH ARE VISABLE FROM THE ONE SIDE IN A MIRROR-LIKE FINISH, WHEN VIEWED FROM THE SAME SIDE AS THE LIGHT SOURCE, AND ARE SEMI-TRANSPARENT OR CLEAR WHEN VIEWED FROM THE OPPOSITE SIDE, THE SAID PROCESS COMPRISING: A. CONTACTING A PLUMBITE-TREATED CELLULOSIC SHEET FLATLY AGAINST A SILICA GLASS OR CERAMIC SURFACE, THE SAID CELLULOSIC SHEET CONTAINING ABOUT FROM 8% TO 15% LEAD, B. HEATING THE CONTACTED MATERIAL IN A CLOSED OVEN, OR OTHER LIMITED OXYGEN ENVIRONMENT, AT A TEMPERATURE OF BELOW 200*C. AND ELEVATING SAID TEMPERATURE TO ABOUT FROM 600* TO 800*C. AND MAINTAINING THE ELEVATED TEMPERATURE FOR A PERIOD OF ABOUT 60 MINUTES TO OBTAIN A CHEMICALLY BOUND UNIT OF ASSEMBLED COMPONENTS WITH HARD SURFACES, C. COOLING THE SAID UNIT SLOWLY TO AVOID FRACTIONATION OF THE COMPONENT PARTS, AND D. REHEATING THE PLUMBITE-TREATED SIDE OF THE SAID UNIT WITH A GAS-AIR FLAME OF ABOUT FROM 1,000* TO 1,500*C. TO OBTAIN COLORATIONS IN THE GOLD, SILVER, AND PURPLE RANGE UPON HEATING FOR PERIODS OF ABOUT FROM 1 TO 5 MINUTES, THE LESSER QUANTITIES OF HEAT YIELDING THE GOLDEN TONES, THE MEDIUM QUANTITIES THE SILVER TONES, AND THE HIGHER QUANTITIES THE PURPLISH TONES.
Claim 2
Dependent Claim 203 words
A PROCESS FOR IMPARTING TO SILICA GLASS OR CERAMICS REVERSIBLE SURFACE COLORATIONS WHICH ARE VISABLE FROM THE ONE SIDE IN A MIRROR-LIKE FINISH, WHEN VIEWED FROM THE SAME SIDE AS THE LIGHT SOURCE, AND ARE SEMI-TRANSPARENT OR CLEAR WHEN VIEWED FROM THE OPPOSITE SIDE, THE SAID PROCESS COMPRISING: A. CONTACTING A PLUMBITE-TREATED CELLULOSIC SHEET FLATLY AGAINST A SILICA GLASS OR CERAMIC SURFACE, THE SAID CELLULOSIC SHEET CONTAINING ABOUT FROM 8% TO 15% LEAD, B. HEATING THE CONTACTED MATERIAL IN A CLOSED OVEN, OR OTHER LIMITED OXYGEN ENVIRONMENT, AT A TEMPERATURE OF BELOW 200*C. AND ELEVATING SAID TEMPERATURE TO ABOUT FROM 600* TO 800*C. AND MAINTAINING THE ELEVATED TEMPERATURE FOR A PERIOD OF ABOUT 60 MINUTES TO OBTAIN A CHEMICALLY BOUND UNIT OF ASSEMBLED COMPONENTS WITH HARD SURFACES, C. COOLING THE SAID UNIT SLOWLY TO AVOID FRACTIONATION OF THE COMPONENT PARTS, AND D. REHEATING THE PLUMBITE-TREATED SIDE OF THE SAID UNIT WITH A GAS-AIR FLAME OF ABOUT FROM 1,000* TO 1,500*C. TO OBTAIN COLORATIONS IN THE GOLD, SILVER, AND PURPLE RANGE UPON HEATING FOR PERIODS OF ABOUT FROM 1 TO 5 MINUTES, THE LESSER QUANTITIES OF HEAT YIELDING THE GOLDEN TONES, THE MEDIUM QUANTITIES THE SILVER TONES, AND THE HIGHER QUANTITIES THE PURPLISH TONES.
Claim 3
Dependent Claim 34 words
A process for removing the coloration imparted by the process of claim 1 comprising heating the colored material in a closed oven at temperatures of about from 600* to 700*C., for about 30 minutes.
Claim 4
Dependent Claim 48 words
A process for removing the coloration imparted by the process of claim 1 comprising applying the said gas-air flame directly to the side of the assembled components opposite the plumbite-cellulosic film side, and maintaining the heating for a period of time long enough to cause the coloration removal.

References Cited (Backward Citations)

US123247A Cited
US2190210A Cited
US2595800A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-12-29 1979-06-30 1979-12-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-12-29 1983-06-30 1983-12-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-12-29 1987-06-30 1987-12-30 $7700.00 Window Closed / Lapsed

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