US3929535A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Color reversible, mirror surface glassy materials from plumbite-treated cellulosics
Assignee: United States Department of Agriculture
•
Filing: 1974-08-22
•
Granted: 1975-12-30
•
Expires: 1994-08-22
Abstract
Abstract Colored glasslike materials have been produced from an uncolored transparent or translucent glassy intermediate which was made by heating plumbite-treated cellulosics in a limited oxygen atmosphere while in contact with a glass or ceramic surface. The uncolored intermediate can be caused to become either gold, silver or purplish black and mirrorlike by exposing it to the direct flame of a bunsen-type burner. The color may be removed by reheating the glassy material in an oven or by heating the back side with a bunsen-type burner when the glassy material is bound to a glass or ceramic holder. The color formation color removal may be repeated.
Inventors
- 👤 Truman L Ward
- 👤 Ruth R Benerito
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-31 19:06
CPC Classifications
B; B44; B44F; B44F1/00; B44F1/08; B44F1/10
Claims Analysis
Total Claims: 4
Claim 1
Independent Claim
203 words
A PROCESS FOR IMPARTING TO SILICA GLASS OR CERAMICS REVERSIBLE SURFACE COLORATIONS WHICH ARE VISABLE FROM THE ONE SIDE IN A MIRROR-LIKE FINISH, WHEN VIEWED FROM THE SAME SIDE AS THE LIGHT SOURCE, AND ARE SEMI-TRANSPARENT OR CLEAR WHEN VIEWED FROM THE OPPOSITE SIDE, THE SAID PROCESS COMPRISING: A. CONTACTING A PLUMBITE-TREATED CELLULOSIC SHEET FLATLY AGAINST A SILICA GLASS OR CERAMIC SURFACE, THE SAID CELLULOSIC SHEET CONTAINING ABOUT FROM 8% TO 15% LEAD, B. HEATING THE CONTACTED MATERIAL IN A CLOSED OVEN, OR OTHER LIMITED OXYGEN ENVIRONMENT, AT A TEMPERATURE OF BELOW 200*C. AND ELEVATING SAID TEMPERATURE TO ABOUT FROM 600* TO 800*C. AND MAINTAINING THE ELEVATED TEMPERATURE FOR A PERIOD OF ABOUT 60 MINUTES TO OBTAIN A CHEMICALLY BOUND UNIT OF ASSEMBLED COMPONENTS WITH HARD SURFACES, C. COOLING THE SAID UNIT SLOWLY TO AVOID FRACTIONATION OF THE COMPONENT PARTS, AND D. REHEATING THE PLUMBITE-TREATED SIDE OF THE SAID UNIT WITH A GAS-AIR FLAME OF ABOUT FROM 1,000* TO 1,500*C. TO OBTAIN COLORATIONS IN THE GOLD, SILVER, AND PURPLE RANGE UPON HEATING FOR PERIODS OF ABOUT FROM 1 TO 5 MINUTES, THE LESSER QUANTITIES OF HEAT YIELDING THE GOLDEN TONES, THE MEDIUM QUANTITIES THE SILVER TONES, AND THE HIGHER QUANTITIES THE PURPLISH TONES.
Claim 2
Dependent Claim
203 words
A PROCESS FOR IMPARTING TO SILICA GLASS OR CERAMICS REVERSIBLE SURFACE COLORATIONS WHICH ARE VISABLE FROM THE ONE SIDE IN A MIRROR-LIKE FINISH, WHEN VIEWED FROM THE SAME SIDE AS THE LIGHT SOURCE, AND ARE SEMI-TRANSPARENT OR CLEAR WHEN VIEWED FROM THE OPPOSITE SIDE, THE SAID PROCESS COMPRISING: A. CONTACTING A PLUMBITE-TREATED CELLULOSIC SHEET FLATLY AGAINST A SILICA GLASS OR CERAMIC SURFACE, THE SAID CELLULOSIC SHEET CONTAINING ABOUT FROM 8% TO 15% LEAD, B. HEATING THE CONTACTED MATERIAL IN A CLOSED OVEN, OR OTHER LIMITED OXYGEN ENVIRONMENT, AT A TEMPERATURE OF BELOW 200*C. AND ELEVATING SAID TEMPERATURE TO ABOUT FROM 600* TO 800*C. AND MAINTAINING THE ELEVATED TEMPERATURE FOR A PERIOD OF ABOUT 60 MINUTES TO OBTAIN A CHEMICALLY BOUND UNIT OF ASSEMBLED COMPONENTS WITH HARD SURFACES, C. COOLING THE SAID UNIT SLOWLY TO AVOID FRACTIONATION OF THE COMPONENT PARTS, AND D. REHEATING THE PLUMBITE-TREATED SIDE OF THE SAID UNIT WITH A GAS-AIR FLAME OF ABOUT FROM 1,000* TO 1,500*C. TO OBTAIN COLORATIONS IN THE GOLD, SILVER, AND PURPLE RANGE UPON HEATING FOR PERIODS OF ABOUT FROM 1 TO 5 MINUTES, THE LESSER QUANTITIES OF HEAT YIELDING THE GOLDEN TONES, THE MEDIUM QUANTITIES THE SILVER TONES, AND THE HIGHER QUANTITIES THE PURPLISH TONES.
Claim 3
Dependent Claim
34 words
A process for removing the coloration imparted by the process of claim 1 comprising heating the colored material in a closed oven at temperatures of about from 600* to 700*C., for about 30 minutes.
Claim 4
Dependent Claim
48 words
A process for removing the coloration imparted by the process of claim 1 comprising applying the said gas-air flame directly to the side of the assembled components opposite the plumbite-cellulosic film side, and maintaining the heating for a period of time long enough to cause the coloration removal.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1978-12-29 | 1979-06-30 | 1979-12-30 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1982-12-29 | 1983-06-30 | 1983-12-30 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1986-12-29 | 1987-06-30 | 1987-12-30 | $7700.00 | Window Closed / Lapsed |