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US3929432A Expired / Lapsed US ⏱️ 0.0 years remaining

Diamond particle having a composite coating of titanium and a metal layer

Assignee: De Beers Industrial Diamond Division Pty Ltd
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Filing: 1973-09-18
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Granted: 1975-12-30
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Expires: 1993-09-18
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Abstract

Abstract A diamond particle of the MD or the SD type having a composite coating comprising a thin continuous layer of titanium adjacent the diamond surface and a metal layer on the titanium layer, the metal of the metal layer being capable of forming an alloy with titanium under the influence of heat and the titanium/diamond interface being essentially free of chemical bond formation. The invention further provides a method of making a metal bonded abrasive device which includes the steps mixing the above described particles with a suitable metal matrix, heating the mixture to a temperature exceeding 500*C, maintaining the mixture at the elevated temperature for a period of from 10 to 30 minutes, and allowing the mixture to return to ambient conditions.

Inventors

  • 👤 Robert John Caveney

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 18:30
CPC Classifications
C; C09; C09K; C09K3/00; C09K3/14; C09K3/1436; C09K3/1445; B; B24; B24D; B24D18/00

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 135 words
A DIAMON PARTICLE OF THE MD OR SD TYPE HAVING A COMPOSITE COATING COMPRISING A THIN CONTINUOUS LAYER OF TITANIUM ADJACENT THE DIAMOND SURFACE, THE TITANIUM BEING PRESENT IN AN EFFECTIVE AMOUNT LESS THAN 3% BY WEIGHT OF THE UNCOATED PARTICLE, SAID AMOUNT BEING EFFECTIVE TO PROVIDE A CONTINUOUS LAYER AROUND THE DIAMOND PARTICLE, AND A METAL LAYER ON THE TITANIUM LAYER, THE METAL OF THE METAL LAYER BEING SELECTED FROM THE GOUP CONSISTING OF IRON, NICKEL, COBALT, COPPER AND ALLOYS CONTAINING ONE OR MORE OF THESE METALS AND BEING CAPABLE OF FORMING AN ALLOY WITH TITANIUM UNDER THE INFLUENCE OF HEAT AND BEING PRESENT IN AN AMOUNT OF FROM 10 TO 100% BY WEIGHT OF THE UNCOATED PARTICLE, AND THE INTERFACE BETWEEN THE DIAMOND AND THE TITANIUM BEING ESSENTIALLY FREE OF CHEMICAL BOND FORMATION.
Claim 2
Dependent Claim 135 words
A DIAMON PARTICLE OF THE MD OR SD TYPE HAVING A COMPOSITE COATING COMPRISING A THIN CONTINUOUS LAYER OF TITANIUM ADJACENT THE DIAMOND SURFACE, THE TITANIUM BEING PRESENT IN AN EFFECTIVE AMOUNT LESS THAN 3% BY WEIGHT OF THE UNCOATED PARTICLE, SAID AMOUNT BEING EFFECTIVE TO PROVIDE A CONTINUOUS LAYER AROUND THE DIAMOND PARTICLE, AND A METAL LAYER ON THE TITANIUM LAYER, THE METAL OF THE METAL LAYER BEING SELECTED FROM THE GOUP CONSISTING OF IRON, NICKEL, COBALT, COPPER AND ALLOYS CONTAINING ONE OR MORE OF THESE METALS AND BEING CAPABLE OF FORMING AN ALLOY WITH TITANIUM UNDER THE INFLUENCE OF HEAT AND BEING PRESENT IN AN AMOUNT OF FROM 10 TO 100% BY WEIGHT OF THE UNCOATED PARTICLE, AND THE INTERFACE BETWEEN THE DIAMOND AND THE TITANIUM BEING ESSENTIALLY FREE OF CHEMICAL BOND FORMATION.
Claim 3
Dependent Claim 16 words
A diamond particle according to claim 1 wherein the metal of the metal layer is nickel.
Claim 4
Dependent Claim 96 words
A diamond particle of the MD or SD type having a composite coating comprising a thin continuous layer of titanium adjacent the diamond surface and a layer of nickel on the titanium layer, the interface between the diamond and the titanium being essentially free of chemical bond formation, the titanium being present in an effective amount of less than 3% by weight of the uncoated particle, said amount being effective to provide a continuous layer around the diamond particle, and the nickel being present in an amount of from 10-100% by weight of the uncoated particle.
Claim 5
Dependent Claim 96 words
A diamond particle of the MD or SD type having a composite coating comprising a thin continuous layer of titanium adjacent the diamond surface and a layer of nickel on the titanium layer, the interface between the diamond and the titanium being essentially free of chemical bond formation, the titanium being present in an effective amount of less than 3% by weight of the uncoated particle, said amount being effective to provide a continuous layer around the diamond particle, and the nickel being present in an amount of from 10-100% by weight of the uncoated particle.
Claim 6
Independent Claim 196 words
A method of manufacturing a metal bonded abrasive device including the steps of: a. forming an effective mixture of a solid metal matrix material and diamond particles of the MD or SD type having a composite coating comprising a thin continuous layer of titanium adjacent the diamond surface, the titanium being present in an effective amount less than 3% by weight of the uncoated particle, said amount being effective to provide a continuous layer around the diamond particle, and a metal layer on the titanium layer, the metal of the metal layer being selected from the group consisting of iron, nickel, cobalt, copper and alloys containing one or more of these metals and being capable of forming an alloy with titanium under the influence of heat and being present in an amount of from 10 to 100% by weight of the uncoated particle, and the interface between the diamond and the titanium being essentially free of chemical bond formation; b. heating the mixture to a temperature exceeding 500*C; c. maintaining the mixture at a temperature exceeding 500*C for a period of from 10 to 30 minutes; and d. allowing the mixture to return to ambient conditions.
Claim 7
Independent Claim 196 words
A method of manufacturing a metal bonded abrasive device including the steps of: a. forming an effective mixture of a solid metal matrix material and diamond particles of the MD or SD type having a composite coating comprising a thin continuous layer of titanium adjacent the diamond surface, the titanium being present in an effective amount less than 3% by weight of the uncoated particle, said amount being effective to provide a continuous layer around the diamond particle, and a metal layer on the titanium layer, the metal of the metal layer being selected from the group consisting of iron, nickel, cobalt, copper and alloys containing one or more of these metals and being capable of forming an alloy with titanium under the influence of heat and being present in an amount of from 10 to 100% by weight of the uncoated particle, and the interface between the diamond and the titanium being essentially free of chemical bond formation; b. heating the mixture to a temperature exceeding 500*C; c. maintaining the mixture at a temperature exceeding 500*C for a period of from 10 to 30 minutes; and d. allowing the mixture to return to ambient conditions.
Claim 8
Dependent Claim 25 words
A method according to claim 4 wherein the mixture is maintained at a temperature exceeding 500*C for a period of from 10 to 20 minutes.
Claim 9
Dependent Claim 24 words
A method according to claim 4 wherein the metal matrix material is capable of forming an alloy with the metal of the metal layer.
Claim 10
Dependent Claim 13 words
A method according to claim 6 wherein the metal matrix material is bronze.
Claim 11
Dependent Claim 22 words
A method according to claim 7 wherein the mixture is heated to a temperature of from 700* to 850*C in step (b).
Claim 12
Dependent Claim 28 words
A method according to claim 7 wherein the mixture is heated to a temperature of about 720*C in step (b) and maintained at this temperature during step (c).
Claim 13
Dependent Claim 15 words
A method according to claim 4 wherein the device is a segment of a saw.
Claim 14
Dependent Claim 14 words
A method according to claim 4 wherein the device is a metal bond wheel.

References Cited (Backward Citations)

US3293012A Cited
US3356473A Cited
US3528788A Cited
US3650714A Cited
US3879901A Cited
US3663191A Cited
US3841852A Cited
US3871840A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-12-29 1979-06-30 1979-12-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-12-29 1983-06-30 1983-12-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-12-29 1987-06-30 1987-12-30 $7700.00 Window Closed / Lapsed

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