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US3928089A Expired / Lapsed US ⏱️ 0.0 years remaining

Rare earth intermetallic compounds produced by a reduction-diffusion process

Assignee: General Electric Co
•
Filing: 1974-07-24
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Granted: 1975-12-23
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Expires: 1994-07-24
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Abstract

Abstract A reduction-diffusion process for producing novel rare earth intermetallic compounds, for example, cobalt-rare earth intermetallic compounds, especially compounds useful in preparing permanent magnets. A particulate mixture of rare earth metal halide, cobalt and calcium hydride is heated to effect reduction of the rare earth metal halide and to diffuse the resulting rare earth metal into the cobalt to form the intermetallic compound.

Inventors

  • 👤 Robert E Cech

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 22:42
CPC Classifications
C; C22; C22C; C22C19/00; C22C19/07; H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/032; H01F1/04; H01F1/047; H01F1/053; H01F1/055; H01F1/0553

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 155 words
A PROCESS FOR PREPARING A MAGNETIC MATERIAL COMPRISED OF A PARTICULATE RATE EARTH INTERMETALLIC COMPOUND COMPRISING PROVIDING A HALIDE OF A RATE EARTH METAL EXCEPT SAMARIUM, EUROPIUM AND YTTERBIUM, ADMIXING IN AT LEAST SUBSTANTIALLY STOICHIOMETRIC AMOUNTS PARTICLES OF SAID RARE EARTH METAL HALIDE, CALCIUM HYDRIDE AND A SOLID METAL SELECTED FROM THE GROUP CONSISTING OF COBALT, COBALT-MANGANESE ALLOYS, COBALTIRON-MANGANESE ALLOYS OR COBALT-IRON ALLOYS, HEATING THE RESULTING PARTICULATE MIXTURE IN AN ATMOSPHERE WHICH IS INERT TO IT AT A TEMPERATURE RANGING FROM ABOUT 850*C TO ABOUT 1,000*C DECOMPOSING SAID CALCIUM HYDRIDE AND EFFECTING REDUCTION OF SAID RARE EARTH METAL HALIDE TO PRODUCE THE RARE EARTH METAL, CONTINUING HEATING THE RESULTING MIXTURE IN AN ATMOSPHERE WHICH IS INERT TO IT AT A TEMPERATURE WHICH DIFFUSES THE RESULTING RARE EARTH METAL INTO SAID SOLID METAL GROUP MEMBER TO FORM THE RARE EARTH INTERMETALLIC COMPOUND, AND RECOVERING FROM THE RARE EARTH INTERMETALLIC COMPOUND-CONTAINING MIXTURE SAID RARE EARTH INTERMETALLIC COMPOUND.
Claim 2
Dependent Claim 155 words
A PROCESS FOR PREPARING A MAGNETIC MATERIAL COMPRISED OF A PARTICULATE RATE EARTH INTERMETALLIC COMPOUND COMPRISING PROVIDING A HALIDE OF A RATE EARTH METAL EXCEPT SAMARIUM, EUROPIUM AND YTTERBIUM, ADMIXING IN AT LEAST SUBSTANTIALLY STOICHIOMETRIC AMOUNTS PARTICLES OF SAID RARE EARTH METAL HALIDE, CALCIUM HYDRIDE AND A SOLID METAL SELECTED FROM THE GROUP CONSISTING OF COBALT, COBALT-MANGANESE ALLOYS, COBALTIRON-MANGANESE ALLOYS OR COBALT-IRON ALLOYS, HEATING THE RESULTING PARTICULATE MIXTURE IN AN ATMOSPHERE WHICH IS INERT TO IT AT A TEMPERATURE RANGING FROM ABOUT 850*C TO ABOUT 1,000*C DECOMPOSING SAID CALCIUM HYDRIDE AND EFFECTING REDUCTION OF SAID RARE EARTH METAL HALIDE TO PRODUCE THE RARE EARTH METAL, CONTINUING HEATING THE RESULTING MIXTURE IN AN ATMOSPHERE WHICH IS INERT TO IT AT A TEMPERATURE WHICH DIFFUSES THE RESULTING RARE EARTH METAL INTO SAID SOLID METAL GROUP MEMBER TO FORM THE RARE EARTH INTERMETALLIC COMPOUND, AND RECOVERING FROM THE RARE EARTH INTERMETALLIC COMPOUND-CONTAINING MIXTURE SAID RARE EARTH INTERMETALLIC COMPOUND.
Claim 3
Dependent Claim 50 words
A process according to claim 1 wherein calcium hydride is used in an amount in excess of stoichiometric and the resulting rare earth intermetallic compound-containing mixture is left in an oxidizing or moisture-containing atmosphere to allow the excess calcium precipitated therein to oxidize or hydrolyze causing said mixture to disintegrate.
Claim 4
Dependent Claim 21 words
A process according to claim 1 wherein said metal group member is cobalt and said rare earth halide is mischmetal chloride.
Claim 5
Dependent Claim 14 words
A process according to claim 1 wherein said calcium hydride is formed in situ.

References Cited (Backward Citations)

US3104166A Cited
US3684499A Cited
US3639181A Cited
US3748193A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-12-22 1979-06-23 1979-12-23 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-12-22 1983-06-23 1983-12-23 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-12-22 1987-06-23 1987-12-23 $7700.00 Window Closed / Lapsed

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