Patent US3919408A successfully refreshed from Google Patents.
US3919408A
Expired / Lapsed
US
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Alcohol-containing oral hygiene powders
Assignee: General Foods Corp
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Filing: 1974-03-04
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Granted: 1975-11-11
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Expires: 1994-03-04
Abstract
Abstract Flowable powders having up to 60% alcohol content are prepared by the sorption of the alcohol with bulked, low dextrose equivalent dextrins. The resulting products are stable when hermetically packaged and are particularly qualified as alcoholcontaining base materials for oral hygiene powder preparations.
Inventors
- 👤 William A Mitchell
- 👤 William C Seidel
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 20:37
CPC Classifications
A; A23; A23L; A23L13/00; A23L13/70; A23L13/72; A61; A61Q; A61Q11/00; A61K; A61K47/00; A61K47/30; A61K47/36; A61K8/00; A61K8/18; A61K8/30; A61K8/49; A61K8/4906; A61K8/4926; A61K8/72; A61K8/73; A61K8/732; A61K9/00; A61K9/14; A61K9/141; A61K9/146; C; C12; C12G; C12G3/00; C12G3/005
Claims Analysis
Total Claims: 13
Claim 1
Independent Claim
182 words
A METHOD OF PREPARING A FLOWABLE, DRY-TO-THE-TOUCH, ALCOHOL-CONTAINING MOUTHWASH POWDER WHICH COMPRISES: A. DISSOLVING IN WATER A DEXTRIN HAVING A DEXTROSE EQUIVALENT OF FROM ABOUT 5 TO ABOUT 15; B. EXPANDING THE DEXTRIN BY FORMING A FILM OF THE SOLUTION OF (A) AND DRYING SAID FILM; C. SUBDIVIDING THE DRIED FILM OF DEXTRIN TO YIELD PARTICULATES OF EXPANDED DEXTRIN HAVING A SIZE CORRESPONDING TO A 20-60 MESH SCREEN OPENING (U.S.S. SIEVE), A MOISTURE CONTENT RANGING FROM ABOUT 2 TO ABOUT 6% AND A BULK DENSITY RANGING FROM ABOUT 0.05 TO ABOUT 0.30 GRAMS/CUBIC CENTIMETER; D. CONTACTING THE EXPANDED DEXTRIN OF (C) WITH AN AQUEOUS SOLUTION OF ETHANOL SO AS TO CAUSE THE DEXTRIN TO SORB FROM ABOUT 30 TO ABOUT 60% ETHANOL BY WEIGHT OF THE RESULTING FLOWABLE ETHANOL-CONTAINING POWDER; AND E. BLENDING THE ALCOHOL DEXTRIN OF (D) WITH SMALL BUT EFFECTIVE AMOUNTS OF MOUTHWASH FLAVORING AND COLORING MATERIALS WHEREBY A FLOWABLE POWDERED MOUTHWASH MIXTURE IS PREPARED CONTAINING FROM ABOUT 30 TO ABOUT 60% ETHANOL, SAID MOUTHWASH BEING READILY SOLUBLE IN COLD WATER TO PRODUCE A MOUTHWASH SOLUTION FOR ORAL HYGIENE PURPOSES.
Claim 2
Independent Claim
182 words
A METHOD OF PREPARING A FLOWABLE, DRY-TO-THE-TOUCH, ALCOHOL-CONTAINING MOUTHWASH POWDER WHICH COMPRISES: A. DISSOLVING IN WATER A DEXTRIN HAVING A DEXTROSE EQUIVALENT OF FROM ABOUT 5 TO ABOUT 15; B. EXPANDING THE DEXTRIN BY FORMING A FILM OF THE SOLUTION OF (A) AND DRYING SAID FILM; C. SUBDIVIDING THE DRIED FILM OF DEXTRIN TO YIELD PARTICULATES OF EXPANDED DEXTRIN HAVING A SIZE CORRESPONDING TO A 20-60 MESH SCREEN OPENING (U.S.S. SIEVE), A MOISTURE CONTENT RANGING FROM ABOUT 2 TO ABOUT 6% AND A BULK DENSITY RANGING FROM ABOUT 0.05 TO ABOUT 0.30 GRAMS/CUBIC CENTIMETER; D. CONTACTING THE EXPANDED DEXTRIN OF (C) WITH AN AQUEOUS SOLUTION OF ETHANOL SO AS TO CAUSE THE DEXTRIN TO SORB FROM ABOUT 30 TO ABOUT 60% ETHANOL BY WEIGHT OF THE RESULTING FLOWABLE ETHANOL-CONTAINING POWDER; AND E. BLENDING THE ALCOHOL DEXTRIN OF (D) WITH SMALL BUT EFFECTIVE AMOUNTS OF MOUTHWASH FLAVORING AND COLORING MATERIALS WHEREBY A FLOWABLE POWDERED MOUTHWASH MIXTURE IS PREPARED CONTAINING FROM ABOUT 30 TO ABOUT 60% ETHANOL, SAID MOUTHWASH BEING READILY SOLUBLE IN COLD WATER TO PRODUCE A MOUTHWASH SOLUTION FOR ORAL HYGIENE PURPOSES.
Claim 3
Dependent Claim
24 words
The method of claim 1 wherein the 5-15 D.E. dextrin is expanded by forming a film of the solution and drum drying the film.
Claim 4
Dependent Claim
27 words
The method of claim 1 wherein the 5-15 D.E. dextrin is expanded by forming a film of the solution and drying the film in a spray drier.
Claim 5
Dependent Claim
26 words
The method of claim 1 wherein the expanded dextrin is contacted with an aqueous solution of ethanol which has been denatured with mouthwash alcohol denaturing materials.
Claim 6
Dependent Claim
56 words
The method of claim 1 wherein aqueous solution of the 5-15 D.E. dextrin is further characterized by combining, in addition to the dextrin, small but effective amounts in the range of 1-4% solids content by weight of the solution of sweetening agents selected from the group consisting of L-aspartyl-L-pheylalanine methyl ester, saccharine, cyclamate, and mixtures thereof.
Claim 7
Dependent Claim
53 words
The method of claim 1 wherein the dextrin having a dextrose equivalent of from about 5 to about 15 is further characterized by having more than 50% of the trimer, hexamer and heptamer ligomers by weight of its total oligomer (10 or less degree of polymerization) content and less than about 1% glucose.
Claim 8
Dependent Claim
23 words
The method of claim 1 further including the addition of small but effective amounts of mouthwash antibacterial agents to the mouthwash powdered mixture.
Claim 9
Dependent Claim
80 words
A dry-to-the-touch, alcohol-containing flowable mouthwash powder comprising; a. small but effective amounts of mouthwash flavoring and coloring materials, intimately blended with b. particulates of dry expanded dextrin, said particulates of dextrin having a dextrose equivalent of from about 5 to about 15, a moisture content ranging from about 2 to about 6%, a bulk density ranging from about 0.05 to about 0.30 grams/cubic centimeter, and from about 30 to about 60% by weight of added ethanol absorbed within said partiCulates.
Claim 10
Dependent Claim
80 words
A dry-to-the-touch, alcohol-containing flowable mouthwash powder comprising; a. small but effective amounts of mouthwash flavoring and coloring materials, intimately blended with b. particulates of dry expanded dextrin, said particulates of dextrin having a dextrose equivalent of from about 5 to about 15, a moisture content ranging from about 2 to about 6%, a bulk density ranging from about 0.05 to about 0.30 grams/cubic centimeter, and from about 30 to about 60% by weight of added ethanol absorbed within said partiCulates.
Claim 11
Dependent Claim
41 words
The product of claim 8 further characterized in that the dextrin has more than 50% of the trimer, hexamer and heptamer oligomers by weight of its total oligomer (10 or less degree of polymerization) content and less than about 1% glucose.
Claim 12
Dependent Claim
12 words
A mouthwash comprising an aqueous solution of the product of claim 8.
Claim 13
Dependent Claim
12 words
A mouthwash comprising an aqueous solution of the product of claim 9.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1978-11-10 | 1979-05-12 | 1979-11-11 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1982-11-10 | 1983-05-12 | 1983-11-11 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1986-11-10 | 1987-05-12 | 1987-11-11 | $7700.00 | Window Closed / Lapsed |