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US3909407A Expired / Lapsed US ⏱️ 0.0 years remaining

Treatment of wool scouring wastes

Assignee: George W Bollman and Co Inc
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Filing: 1974-09-30
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Granted: 1975-09-30
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Expires: 1994-09-30
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Abstract

Abstract A method of continuously treating wool scouring wastes in which the scouring liquor at an elevated temperature is acidified and treated with bentonite while continuously mixing, treating the acidulated liquor with lime and flocculating while continuously mixing, again at an elevated temperature, and finally the conditioned mixed liquor is transferred to a settling tank where the sludge is removed for further treatment and clear liquid is drawn off for discharge into a sewer system.

Inventors

  • 👤 Willis A Heisey

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 15:06
CPC Classifications
C; C02; C02F; C02F9/00; C02F1/00; C02F1/52; C02F1/5236; C11; C11B; C11B11/00; C11B11/005

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 185 words
A continuous process for treating wool scouring waste liquors having at least 20,000 ppm COD comprising, in combination: acidulating in a tank and maiNtaining in a pH range of 3.0-3.5 a continuously flowing, constantly agitated, scouring waste liquor heated to a temperature in the range of 160* to 200*F at a flow rate through the tank yielding an approximate retention time of 15 minutes in the tank; adding lime at a weight to volume concentration in the range of 0.5-1.25% and flocculating the continuously flowing, constantly agitated, heated acidulated waste liquor in a second tank forming a conditioned sludge at a flow rate through the tank yielding an approximate retention time of 15 minutes in a second tank; separating the conditioned sludge in a heated settling tank maintained at approximately 200*F to form a disposable supernatant liquor and a settled non drainable sludge; and centrifugally separating the settled non drainable sludge to form disposable liquid and solid constituents, where the temperature during the acidulating step and the weight to volume concentration of lime are selected from the ranges described to obtain a non drainable sludge.
Claim 2
Dependent Claim 185 words
A continuous process for treating wool scouring waste liquors having at least 20,000 ppm COD comprising, in combination: acidulating in a tank and maiNtaining in a pH range of 3.0-3.5 a continuously flowing, constantly agitated, scouring waste liquor heated to a temperature in the range of 160* to 200*F at a flow rate through the tank yielding an approximate retention time of 15 minutes in the tank; adding lime at a weight to volume concentration in the range of 0.5-1.25% and flocculating the continuously flowing, constantly agitated, heated acidulated waste liquor in a second tank forming a conditioned sludge at a flow rate through the tank yielding an approximate retention time of 15 minutes in a second tank; separating the conditioned sludge in a heated settling tank maintained at approximately 200*F to form a disposable supernatant liquor and a settled non drainable sludge; and centrifugally separating the settled non drainable sludge to form disposable liquid and solid constituents, where the temperature during the acidulating step and the weight to volume concentration of lime are selected from the ranges described to obtain a non drainable sludge.
Claim 3
Dependent Claim 31 words
A continuous process for treating wool scouring waste liquors as set forth in claim 1, wherein the waste liquor is maintained at a temperature of approximately 200*F during the flocculating step.
Claim 4
Dependent Claim 35 words
A continuous process for treating wool scouring waste liquors as set forth in claim 1, including the additional step of adding bentonite in a weight to volume concentration of approximately 0.3% during the acidulation step.
Claim 5
Dependent Claim 198 words
A CONTINUOUS PROCESS FOR TREATING WOOL SCOURING WASTE LIQUORS COMPRISING, IN COMBINATION: ADDING ACID MAINTAINING A PH RANGE OF 3.0-3.5 AND BENTONITE AT A RATE TO YIELD A WEIGHT TO VOLUME CONCERATION OF 0.3% TO CONTINUOUSLY FLOWING, CONSTANTLY AGITATED, WASTE LIQUOR IN A TANK AT A TEMPERATURE IN THE RANGE OF 190*-200*F AND AT A FLOW RATE THROUGH THE TANK YIELDING AN APPROXIMATE RETENTION TIME OF 15 MINUTES IN THE TANK ADDING LIME AT A RATE TO YIELD A WEIGHT TO VOLUME CONCENTRATION IN THE RANGE OF 1.0-2.0% AND FIOCCULATING THE CONTINUOUSLY FLOWING, CONSTANTLY AGITATED, ACIDULATED LIQUOR IN A SECOND TANK AT A TEMPERATURE IN THE RANGE OF 200*F AT A FLOW RATE THROUGH THE SECOND TANK YIELDING AN APPROXIMATE RETENTION TIME OF 15 MINUTES IN THE TANK FORMING A CONDITIONED SLUDGE, SEPARATING THE CONDITIONED SLUDGE IN A SETTLING TANK MAINTAINED AT APPROXIMATELY 200*F TO FORM A DISPOSABLE SUPERNATENT LIQUOR AND A SETTLED NON DRAINABLE SLUDGE, AND CENTRIFUGALLY SEPARATING THE SETTLED NON DRAINABLE SLUDGE TO FORM DISPOSABLE LIQUID AND SOLID CONSTITUENTS WHERE THE TEMPERATURE DURING THE ACIDULATING STEP AND THE WEIGHT TO VOLUME CONCENTRATION OF LIME ARE SELECTED FROM THE RANGES DESCRIBED TO OBTAIN A NON DRAINABLE SLUDGE.
Claim 6
Dependent Claim 198 words
A CONTINUOUS PROCESS FOR TREATING WOOL SCOURING WASTE LIQUORS COMPRISING, IN COMBINATION: ADDING ACID MAINTAINING A PH RANGE OF 3.0-3.5 AND BENTONITE AT A RATE TO YIELD A WEIGHT TO VOLUME CONCERATION OF 0.3% TO CONTINUOUSLY FLOWING, CONSTANTLY AGITATED, WASTE LIQUOR IN A TANK AT A TEMPERATURE IN THE RANGE OF 190*-200*F AND AT A FLOW RATE THROUGH THE TANK YIELDING AN APPROXIMATE RETENTION TIME OF 15 MINUTES IN THE TANK ADDING LIME AT A RATE TO YIELD A WEIGHT TO VOLUME CONCENTRATION IN THE RANGE OF 1.0-2.0% AND FIOCCULATING THE CONTINUOUSLY FLOWING, CONSTANTLY AGITATED, ACIDULATED LIQUOR IN A SECOND TANK AT A TEMPERATURE IN THE RANGE OF 200*F AT A FLOW RATE THROUGH THE SECOND TANK YIELDING AN APPROXIMATE RETENTION TIME OF 15 MINUTES IN THE TANK FORMING A CONDITIONED SLUDGE, SEPARATING THE CONDITIONED SLUDGE IN A SETTLING TANK MAINTAINED AT APPROXIMATELY 200*F TO FORM A DISPOSABLE SUPERNATENT LIQUOR AND A SETTLED NON DRAINABLE SLUDGE, AND CENTRIFUGALLY SEPARATING THE SETTLED NON DRAINABLE SLUDGE TO FORM DISPOSABLE LIQUID AND SOLID CONSTITUENTS WHERE THE TEMPERATURE DURING THE ACIDULATING STEP AND THE WEIGHT TO VOLUME CONCENTRATION OF LIME ARE SELECTED FROM THE RANGES DESCRIBED TO OBTAIN A NON DRAINABLE SLUDGE.

References Cited (Backward Citations)

US2429868A Cited
US2762681A Cited
US2903424A Cited
US3419493A Cited
US3677940A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-09-29 1979-03-31 1979-09-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-09-29 1983-03-31 1983-09-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-09-29 1987-03-31 1987-09-30 $7700.00 Window Closed / Lapsed

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