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US3900666A Expired / Lapsed US ⏱️ 0.0 years remaining

Flame retardant textiles by use of nitrogenous type resin and antimony oxide

Assignee: United States Department of Agriculture
•
Filing: 1974-06-04
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Granted: 1975-08-19
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Expires: 1994-06-04
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Abstract

Abstract Antimony oxide is employed as a flame retardant additive in aqueous solutions of N-methylol resins which are utilized in the treatment of blended textiles whose components are a cellulosic fiber and a halogen containing synthetic fiber. Durable press and/or weather and rot resistance can be imparted to the textile blend in addition to the flame retardance, said properties being dependent on the particular N-methylol resin employed.

Inventors

  • 👤 Mard Hubert H St
  • 👤 Jr Albert S Cooper
  • 👤 Carl Hamalainen

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 15:25
CPC Classifications
D; D06; D06M; D06M15/00; D06M15/19; D06M15/37; D06M15/39; D06M15/423; D06M11/00; D06M11/32; D06M11/36; D06M11/47; Y; Y10; Y10S; Y10S428/00; Y10S428/92; Y10S428/921; Y10T; Y10T428/00; Y10T428/31504; Y10T428/31855; Y10T428/31859; Y10T428/31862; Y10T428/31866; Y10T428/31942; Y10T428/31949; Y10T442/00; Y10T442/20; Y10T442/2631; Y10T442/2656; Y10T442/2762; Y10T442/277; Y10T442/2828; Y10T442/2844

Claims Analysis

Total Claims: 25
Claim 1
Independent Claim 59 words
A PROCESS FOR IMPARTING FLAME RETARDANCY TO A BLENDED COTTON AND HAOGEN-CONTAINING SYNTHETIC TEXTILE, THE PROCESS COMPRISING: A. IMPREGNATING A BLENDED FABRIC WHOSE COMPOSITION IS IN THE RANGE OF ABOUT FROM 85-15 PERCENT TO 15-85 PERCENT BY WEIGHT, RESPECTIVELY, OF COTTON AND A HALOGEN-CONTAINING SYNTHETIC TEXTILE, TO ABOUT FROM 60 TO 100 PRECENT WET PICKUP WITH A SOLUTION CONTAINING:
Claim 2
Dependent Claim 59 words
A PROCESS FOR IMPARTING FLAME RETARDANCY TO A BLENDED COTTON AND HAOGEN-CONTAINING SYNTHETIC TEXTILE, THE PROCESS COMPRISING: A. IMPREGNATING A BLENDED FABRIC WHOSE COMPOSITION IS IN THE RANGE OF ABOUT FROM 85-15 PERCENT TO 15-85 PERCENT BY WEIGHT, RESPECTIVELY, OF COTTON AND A HALOGEN-CONTAINING SYNTHETIC TEXTILE, TO ABOUT FROM 60 TO 100 PRECENT WET PICKUP WITH A SOLUTION CONTAINING:
Claim 3
Dependent Claim 30 words
ABOUT FROM 6 TO 20 PERCENT OF ACROSSLINKING AND/OR POLYMER-FORMING N-METHYLOL-TYPE RESIN SELECTED FROM THE GROUP CONSISTING OF TRIMETHYLOL MELAMINE, METHYLATED METHYLOL MELAMINE, DIMETHYLOL DIHYDROXY ETHYLENE UREA AND PROPYLENE UREA.
Claim 4
Dependent Claim 30 words
ABOUT FROM 6 TO 20 PERCENT OF ACROSSLINKING AND/OR POLYMER-FORMING N-METHYLOL-TYPE RESIN SELECTED FROM THE GROUP CONSISTING OF TRIMETHYLOL MELAMINE, METHYLATED METHYLOL MELAMINE, DIMETHYLOL DIHYDROXY ETHYLENE UREA AND PROPYLENE UREA.
Claim 5
Dependent Claim 47 words
ABOUT FROM 1 TO 8 PERCENT OF AN ACID TUYPE CATALYST SELECTED FROM THE GROUP CONSISTING OF A MIXTURE OF ZINC ACETATE AND ZINC NITRATE, A MIXTURE OF TARTARIC ACID AND AMMONIUM CHLORIDE, A MIXTURE OF CITRIC ACID AND MAGNESIUM CHLORIDE, AMMONIUM CHLORIDE, AND ZIRCONIUM ACETATE, AND
Claim 6
Dependent Claim 47 words
ABOUT FROM 1 TO 8 PERCENT OF AN ACID TUYPE CATALYST SELECTED FROM THE GROUP CONSISTING OF A MIXTURE OF ZINC ACETATE AND ZINC NITRATE, A MIXTURE OF TARTARIC ACID AND AMMONIUM CHLORIDE, A MIXTURE OF CITRIC ACID AND MAGNESIUM CHLORIDE, AMMONIUM CHLORIDE, AND ZIRCONIUM ACETATE, AND
Claim 7
Dependent Claim 47 words
about from 1 to 8 percent of an acid type catalyst selected from the group consisting of a mixture of zinc acetate and zinc nitrate, a mixture of tartaric acid and ammonium chloride, a mixture of citric acid and magnesium chloride, ammonium chloride, and zirconium acetate; and
Claim 8
Dependent Claim 47 words
about from 1 to 8 percent of an acid type catalyst selected from the group consisting of a mixture of zinc acetate and zinc nitrate, a mixture of tartaric acid and ammonium chloride, a mixture of citric acid and magnesium chloride, ammonium chloride, and zirconium acetate; and
Claim 9
Dependent Claim 15 words
The process of claim 1 wherein the crosslinking and/or polymer-forming N-methylol-type resin is trimethylol melamine.
Claim 10
Dependent Claim 16 words
The process of claim 1 wherein the crosslinking and/or polymer-forming N-methylol-type resin is dimethylol dihydroxy ethyleneurea.
Claim 11
Dependent Claim 37 words
about from 1 to 20 percent of antimony oxide as a flame retardant additive; and b. drying at about 2-4 minutes at about 185*F and curing the impregnated blended fabric for about 2-4 minutes at about 285*F.
Claim 12
Dependent Claim 37 words
about from 1 to 20 percent of antimony oxide as a flame retardant additive; and b. drying at about 2-4 minutes at about 185*F and curing the impregnated blended fabric for about 2-4 minutes at about 285*F.
Claim 13
Dependent Claim 36 words
ABOUT FROM 1 TO 20 PERCENT OF ANTIMONY OXIDE AS A FLAME RETARDANT ADDITIVE, AND B. DRYING AT ABOUT 2-4 MINUTESAT ABOUT 185*F AND CURING THE IMPREGNATED BLENDED FABRIC FOR ABOUT 2-4 MINUTES AT ABOUT 285*F.
Claim 14
Dependent Claim 36 words
ABOUT FROM 1 TO 20 PERCENT OF ANTIMONY OXIDE AS A FLAME RETARDANT ADDITIVE, AND B. DRYING AT ABOUT 2-4 MINUTESAT ABOUT 185*F AND CURING THE IMPREGNATED BLENDED FABRIC FOR ABOUT 2-4 MINUTES AT ABOUT 285*F.
Claim 15
Dependent Claim 22 words
The process of claim 1 wherein the crosslinking and/or polymer-forming resin is a mixture of methylolated methylol melamine and dimethylol propylene urea.
Claim 16
Dependent Claim 17 words
The process of claim 1 wherein the catalyst is a mixture of zinc acetate and zinc nitrate.
Claim 17
Dependent Claim 11 words
The process of claim 1 wherein the catalyst is zinc nitrate.
Claim 18
Dependent Claim 17 words
The process of claim 1 wherein the catalyst is a mixture of tartaric acid and ammonium chloride.
Claim 19
Dependent Claim 17 words
The process of claim 1 wherein the catalyst is a mixture of citric acid and magnesium chloride.
Claim 20
Dependent Claim 11 words
The process of claim 1 wherein the catalyst is ammonium chloride.
Claim 21
Dependent Claim 11 words
The process of claim 1 wherein the catalyst is zirconium acetate.
Claim 22
Dependent Claim 11 words
The process of claim 1 wherein the catalyst is magnesium chloride.
Claim 23
Dependent Claim 11 words
The flame-resisting blended fabric produced by the process of claim 2.
Claim 24
Dependent Claim 11 words
The flame-resisting blended fabric produced by the process of claim 3.
Claim 25
Dependent Claim 11 words
The flame-resisting blended fabric produced by the process of claim 4.

References Cited (Backward Citations)

US2299612A Cited
US3243391A Cited
US3219478A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-08-18 1979-02-17 1979-08-19 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-08-18 1983-02-17 1983-08-19 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-08-18 1987-02-17 1987-08-19 $7700.00 Window Closed / Lapsed

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