Claims Analysis
Total Claims: 19
Claim 1
Independent Claim
260 words
IN A METHOD OF FORMING A SURFACE DIFFUSION ALLOY BY APPLYING AT LEAST ONE APPLICATION METAL TO THE INNER WALL OF A HOLLOW METALLIC PART IN WHICH A CEMENT COMPRISING A POWDER OF AT LEAST ONE APPLICATION METAL, AN INERT DILUENT HAVING A HIGH HEAT OF FORMATION TO PREVENT COALESCENCE OR SINTERING OF THE PARTICLES OF THE APPLICATION METAL POWDER DURING FORMATION OF SAID SURFACE DIFFUSION ALLOY, AND A HALOGEN OR HALOGENATED COMPOUND FOR GENERATING VAPORS OF SAID APPLICATION METAL TO THE INNER WALL OF THE PART TO BE TREATED, IS INTRODUCED INTO THE CAVITY OF SAID HOLLOW PART IN IMMEDIATED PROXIMITY TO SAID WALL, AND IN WHICH THE CEMENT IS THEN HEATED TO GENERATE VAPORS OF THE APPLICATION METAL TO FORM A SURFACE DIFFUSION ALLOY OF THE APPLICATION METAL AND THE METALLIC PART AT THE INNER WALL OF SAID PART, THE IMPROVEMENT WHICH COMPRISES: PROVIDING IN SAID CEMENT A SURFACE ACTIVE AGENT SELECTED FROM THE GROUP CONSISTING OF OLEIC ACID, LINOLEIC ACID AND RICINOLEIC ACID IN AN AMOUNT SUFFICIENT TO CONFER THIXOTROPIC PPROPERTIES ON THE CEMENT SUCH THAT THE CEMENT IS TEMPORARILY LIQUEFIED WHEN SUBJECTED TO VIBRATION. SUBJECTING THE CEMENT WITHIN SAID CAVITY, PRIOR TO HEATING THE CEMENT TO VIBRATION TO TEMPORARILY LIQUEFY SAID CEMENT TO FACILITATE PENETRATION OF SAID CEMENT INTO REMOTE ZONES OF SAID CAVITY TO BRING SAID CEMENT INTO IMMEDIATE PROXIMITY TO SAID WALL, LEAVING THE CEMENT UNDISTURBED WITHIN THE CAVITY UNTIL IT RESUMES ITS INITIAL VISCOSITY, AND AFTER HEATING THE CEMENT TO FORM SAID SURFACE DIFFUSION ALLOY, REMOVING THE CEMENT FROM WITHIN THE HOLLOW PART.
Claim 2
Dependent Claim
260 words
IN A METHOD OF FORMING A SURFACE DIFFUSION ALLOY BY APPLYING AT LEAST ONE APPLICATION METAL TO THE INNER WALL OF A HOLLOW METALLIC PART IN WHICH A CEMENT COMPRISING A POWDER OF AT LEAST ONE APPLICATION METAL, AN INERT DILUENT HAVING A HIGH HEAT OF FORMATION TO PREVENT COALESCENCE OR SINTERING OF THE PARTICLES OF THE APPLICATION METAL POWDER DURING FORMATION OF SAID SURFACE DIFFUSION ALLOY, AND A HALOGEN OR HALOGENATED COMPOUND FOR GENERATING VAPORS OF SAID APPLICATION METAL TO THE INNER WALL OF THE PART TO BE TREATED, IS INTRODUCED INTO THE CAVITY OF SAID HOLLOW PART IN IMMEDIATED PROXIMITY TO SAID WALL, AND IN WHICH THE CEMENT IS THEN HEATED TO GENERATE VAPORS OF THE APPLICATION METAL TO FORM A SURFACE DIFFUSION ALLOY OF THE APPLICATION METAL AND THE METALLIC PART AT THE INNER WALL OF SAID PART, THE IMPROVEMENT WHICH COMPRISES: PROVIDING IN SAID CEMENT A SURFACE ACTIVE AGENT SELECTED FROM THE GROUP CONSISTING OF OLEIC ACID, LINOLEIC ACID AND RICINOLEIC ACID IN AN AMOUNT SUFFICIENT TO CONFER THIXOTROPIC PPROPERTIES ON THE CEMENT SUCH THAT THE CEMENT IS TEMPORARILY LIQUEFIED WHEN SUBJECTED TO VIBRATION. SUBJECTING THE CEMENT WITHIN SAID CAVITY, PRIOR TO HEATING THE CEMENT TO VIBRATION TO TEMPORARILY LIQUEFY SAID CEMENT TO FACILITATE PENETRATION OF SAID CEMENT INTO REMOTE ZONES OF SAID CAVITY TO BRING SAID CEMENT INTO IMMEDIATE PROXIMITY TO SAID WALL, LEAVING THE CEMENT UNDISTURBED WITHIN THE CAVITY UNTIL IT RESUMES ITS INITIAL VISCOSITY, AND AFTER HEATING THE CEMENT TO FORM SAID SURFACE DIFFUSION ALLOY, REMOVING THE CEMENT FROM WITHIN THE HOLLOW PART.
Claim 3
Dependent Claim
39 words
A method according to claim 1, wherein the treated hollow part, at least at the inner wall of its cavity, is constituted by at least one metal selected from the group consisting of iron, nickel, cobalt, tungsten and molybdenum.
Claim 4
Dependent Claim
33 words
A method according to claim 1, wherein at least the inner wall of the cavity of said part includes an additional metal selected from the group consisting of chromium, titanium, aluminum or zirconium.
Claim 5
Dependent Claim
29 words
A method according to claim 1, wherein the application metal is selected from the group consisting of chromium, aluminum, tantalum, tinanium, zirconium, vanadium, boron and alloys of these metals.
Claim 6
Dependent Claim
27 words
A method according to claim 1, wherein the surface active agent is present in a solution, the solvent thereof having a boiling point between 80* and 120*C.
Claim 7
Dependent Claim
18 words
A method according to claim 5, wherein the solvent is an aliphatic or aromatic hydrocarbon, or absolute alcohol.
Claim 8
Dependent Claim
29 words
A method according to claim 1, wherein the surface active agent is introduced into a mixing apparatus at the same operational stage as the other constituents of the cement.
Claim 9
Dependent Claim
20 words
A method according to claim 1, wherein introduction of the cement into the cavity is effected by simple gravity flow.
Claim 10
Dependent Claim
26 words
A method according to claim 1, wherein the introduction of the cement into the cavity of the treated part subjected to vibration is effected by injection.
Claim 11
Dependent Claim
29 words
A method according to claim 1, wherein the surface active agent is present in a solution and wherein the solvent is removed prior to forming said surface diffusion alloy.
Claim 12
Dependent Claim
16 words
A method according to claim 10, wherein the elimination of the solvent is effected by heating.
Claim 13
Dependent Claim
39 words
A method according to claim 11, wherein the heating is carried out in a first phase conducted at a temperature below the boiling point of the solution and a second phase conducted at a temperature above this boiling point.
Claim 14
Dependent Claim
25 words
A method according to claim 1, wherein the removal of the cement residue from the hollow part comprises introducing an aqueous or alcohol acid solution.
Claim 15
Dependent Claim
25 words
A method according to claim 1, wherein the application metal is one which forms a protective surface diffusion alloy on the wall of said part.
Claim 16
Dependent Claim
38 words
A method according to claim 1, wherein the outer wall of the part is provided with a surface diffusion alloy by heat treatment with a cement comprising said powder, said inert diluent, and said halogen or halogenated compound.
Claim 17
Dependent Claim
27 words
A method according to claim 15, wherein the cement used for the treatment of the outer wall is different from the cement used for the inner wall.
Claim 18
Dependent Claim
30 words
A method according to claim 15, wherein the cement used for the treatment of the outer wall is the same as that used for the treatment of the inner wall.
Claim 19
Dependent Claim
16 words
Hollow metallic part having a surface diffusion alloy formed by the method according to claim 1.