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US3886358A
Expired / Lapsed
US
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Specimen transfer container for ion microprobe mass analyzer
Assignee: United States Department of Energy
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Filing: 1974-05-23
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Granted: 1975-05-27
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Expires: 1994-05-23
Abstract
Abstract This invention is directed to a specimen holder for use with an ion microprobe mass analyzer. The specimen holder provides for the transfer of the specimen from an inert atmosphere to the analyzer without exposing the specimen to an atmosphere reactive therewith prior to analysis of the specimen.
Inventors
- 👤 John F Mclaughlin
- 👤 Stephen S Cristy
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-27 12:32
CPC Classifications
H; H01; H01J; H01J49/00; H01J49/02; H01J49/04; H01J49/0409; H01J37/00; H01J37/02; H01J37/20
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
227 words
A specimen holder for use with an ion microprobe mass analyzer to provide for the transfer of a specimen to be analyzed from a specimen-loading facility to a specimen-analyzing chamber exhaustable to a predetermined pressure in said analyzer without exposing the specimen to an atmosphere reactive with the specimen, comprising an open housing having a receptacle at one end thereof for receiving a specimen container through the opening, sealing means at said open end of the housing disposed about said receptacle, removable lid means adapted to be disposed over said receptacle at said one end thereof in a contacting relationship with said sealing means, a passageway projecting into said housing in registry with said receptacle for placing said receptacle in communication with a source of vacuum to a pressure corresponding to said predetermined pressure for evacuating said receptacle and pulling said lid means against said sealing means for enclosing said receptacle, and valve means in registry with said passageway for selectively opening and closing said passageway, with said lid means being affixed to said housing upon evacuation of said receptacle and closing of said passageway by said valve means, whereby when said holder is positioned within the analyzer chamber and when said chamber is at said predetermined pressure, the cover is released from said contacting relationship with said sealing means so that the specimen may be analyzed.
Claim 2
Dependent Claim
227 words
A specimen holder for use with an ion microprobe mass analyzer to provide for the transfer of a specimen to be analyzed from a specimen-loading facility to a specimen-analyzing chamber exhaustable to a predetermined pressure in said analyzer without exposing the specimen to an atmosphere reactive with the specimen, comprising an open housing having a receptacle at one end thereof for receiving a specimen container through the opening, sealing means at said open end of the housing disposed about said receptacle, removable lid means adapted to be disposed over said receptacle at said one end thereof in a contacting relationship with said sealing means, a passageway projecting into said housing in registry with said receptacle for placing said receptacle in communication with a source of vacuum to a pressure corresponding to said predetermined pressure for evacuating said receptacle and pulling said lid means against said sealing means for enclosing said receptacle, and valve means in registry with said passageway for selectively opening and closing said passageway, with said lid means being affixed to said housing upon evacuation of said receptacle and closing of said passageway by said valve means, whereby when said holder is positioned within the analyzer chamber and when said chamber is at said predetermined pressure, the cover is released from said contacting relationship with said sealing means so that the specimen may be analyzed.
Claim 3
Dependent Claim
70 words
The specimen holder claimed in claim 1, wherein said specimen container comprises a specimen-carrying block having a closed-end cavity therein for receiving the specimen, a plurality of apertures projecting through said block adjacent to said cavity, and wherein said block is disposed fully within said receptacle with said cavity opening towards said lid means and with said apertures projecting between said lid means and the innermost surface of said receptacle.
Claim 4
Dependent Claim
38 words
The specimen holder claimed in claim 2, wherein, in combination, lid clamping means are disposed within said specimen-analyzing chamber for receiving and securing said lid means to provide for selective displacement of said housing from said lid means.
Claim 5
Dependent Claim
70 words
The specimen holder claimed in claim 3, wherein said specimen-analyzing chamber has a rotatable disc disposed therein with said disc having a receptacle therein for receiving said specimen holder, said lid means has a flange projecting therefrom, said lid clamping means has a pivotable arm thereon having a slot therein for receiving said flange, and wherein clamping means project into said slot for securing said lid means to said arm.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1978-05-26 | 1978-11-25 | 1979-05-27 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1982-05-26 | 1982-11-25 | 1983-05-27 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1986-05-26 | 1986-11-25 | 1987-05-27 | $7700.00 | Window Closed / Lapsed |