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US3883311A Expired / Lapsed US ⏱️ 0.0 years remaining

Reaction crystallizer

Assignee: Chiyoda Corp
•
Filing: 1972-09-22
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Granted: 1975-05-13
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Expires: 1992-09-22
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Abstract

Abstract In a reaction crystallizer provided at the upper portion thereof with a suspension zone and at the lower portion thereof with a classification zone, the said suspension zone comprises an outer mother liquor chamber adapted to separate a crystal slurry into a dense slurry and a clear mother liquor by virtue of the difference in specific gravity, a means for circulating a part of the clear mother liquor in the said mother liquor chamber into the classification zone, an inner circulation chamber enclosed within the said mother liquor chamber, a reaction chamber enclosed within the said circulation chamber and adapted to receive therein reactants being introduced, and a means for introducing air upwardly into the reaction chamber so as to circulate the dense slurry produced in the reaction chamber convectively and suspend the same between the said reaction chamber and the circulation chamber. On the other hand, the classification zone comprises a crystal discharge passage and a means for introducing air into the suspension zone. The fine crystals among the crystals produced in the suspension zone and falling into the classification zone are circulated and retained in the reaction chamber cooperatively by the clear mother liquor and air introduced into the classification zone so that, the crystals therein grow in a fixed size. Thus, only coarse crystals fall against the ascending current of said clear mother liquor and are discharged from the crystal discharge passage.

Inventors

  • 👤 Toshio Kanai
  • 👤 Masaaki Noguchi
  • 👤 Hiroshi Yanagioka
  • 👤 Yosio Kogawa
  • 👤 Susumu Kondo

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 13:06
CPC Classifications
B; B01; B01J; B01J8/00; B01J8/18; B01J8/20; B01J8/22; B01J8/224; B01J8/226; B01D; B01D9/00; B01D9/0036; B01D9/005

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 265 words
A REACTION CRYSTALLIZER WHICH COMPRISES IN COMBINATION A CLOSED VERTICAL REACTION TANK HAVING A CYLINDRICAL CROSS SECTION AND AN UPPER BARREL HAVING THE LARGES DIAMETER, A MIDDLE BARREL HAVING A SMALLER DIAMETER THAN SAID UPPER BARREL AND A LOWER BARREL DEFINING A CLASSIFICATION ZONE HAING A SMALLER DIAMETER THAN SAID MIDDLE BARREL, A FIRST INNER CYLINDER SUSPENDED FROM THE TOP OF THE REATION TANK AND HAVING A DIAMETER SMALLER THAN THAT OF THE UPPER BARREL, SAID FIRST CYLINDER DEFINING AN ANNULAR MOTHER LIQUID CHAMBER WITH THE UPPER BARREL, A SECOND CYLINDER DEFINING A REACTION CHAMBER HAVING A DIAMETER SMALLER THAN THAT OF THE MIDDLE BARREL AND THE FIRST INNER CYLINDER SAID SECOND CYLINDER BEING DISPOSED FROM WITHIN THE FIRST INNER CYLINDER AND TO THE MIDDLE BARREL, SAID SECOND CYLINDER DEFINING AN ANNULAR CIRCULATION CHAMBER WITH THE INNER SURFACE OF THE SAID FIRST INNER CYLINDER, MEANS FOR INTRODUCING A FIRST REACTION TO THE SECOND CYLINDER, MEANS FOR INTRODUCING AIR TO AN OPEN BOTTOM PORTION OF THE SECOND CYLINDER, AND MEANS FOR INTRODUCING A SECOND REACTANT TO THE SECOND CYLINDER MEANS FOR INTRODUCING AIR TO THE LOWER BARREL, A CRYSTAL DISCHARGED PASSAGE DISPOSED AT THE LOWER PORTION OF THE LOWER BARREL, RECYCLE PIPE DISPOSED FOR PASSING MOTHER LIQUID FROM THE MOTHER LIQUOR CHAMBER TO THE LOWER BARREL DEFINING THE CLASSIFICATION ZONE, A DISCHARGE PASSAGE FOR OVERFLOW OF MOTHER LIQUOR DISPOSED NEAR THE UPPER PORTION OF THE UPPER BARREL, AND A GAS DISCHARGE DISPOSED ON TOP OF THE REACTION TANK, WHEREBY FINE CRYSTALS PRODUCED IN THE RREACTION TANK REMAIN SUSPENDED, WITH COARSE CRYSTALS PASSING TO THE CLASSIFICATION ZONE.
Claim 2
Dependent Claim 265 words
A REACTION CRYSTALLIZER WHICH COMPRISES IN COMBINATION A CLOSED VERTICAL REACTION TANK HAVING A CYLINDRICAL CROSS SECTION AND AN UPPER BARREL HAVING THE LARGES DIAMETER, A MIDDLE BARREL HAVING A SMALLER DIAMETER THAN SAID UPPER BARREL AND A LOWER BARREL DEFINING A CLASSIFICATION ZONE HAING A SMALLER DIAMETER THAN SAID MIDDLE BARREL, A FIRST INNER CYLINDER SUSPENDED FROM THE TOP OF THE REATION TANK AND HAVING A DIAMETER SMALLER THAN THAT OF THE UPPER BARREL, SAID FIRST CYLINDER DEFINING AN ANNULAR MOTHER LIQUID CHAMBER WITH THE UPPER BARREL, A SECOND CYLINDER DEFINING A REACTION CHAMBER HAVING A DIAMETER SMALLER THAN THAT OF THE MIDDLE BARREL AND THE FIRST INNER CYLINDER SAID SECOND CYLINDER BEING DISPOSED FROM WITHIN THE FIRST INNER CYLINDER AND TO THE MIDDLE BARREL, SAID SECOND CYLINDER DEFINING AN ANNULAR CIRCULATION CHAMBER WITH THE INNER SURFACE OF THE SAID FIRST INNER CYLINDER, MEANS FOR INTRODUCING A FIRST REACTION TO THE SECOND CYLINDER, MEANS FOR INTRODUCING AIR TO AN OPEN BOTTOM PORTION OF THE SECOND CYLINDER, AND MEANS FOR INTRODUCING A SECOND REACTANT TO THE SECOND CYLINDER MEANS FOR INTRODUCING AIR TO THE LOWER BARREL, A CRYSTAL DISCHARGED PASSAGE DISPOSED AT THE LOWER PORTION OF THE LOWER BARREL, RECYCLE PIPE DISPOSED FOR PASSING MOTHER LIQUID FROM THE MOTHER LIQUOR CHAMBER TO THE LOWER BARREL DEFINING THE CLASSIFICATION ZONE, A DISCHARGE PASSAGE FOR OVERFLOW OF MOTHER LIQUOR DISPOSED NEAR THE UPPER PORTION OF THE UPPER BARREL, AND A GAS DISCHARGE DISPOSED ON TOP OF THE REACTION TANK, WHEREBY FINE CRYSTALS PRODUCED IN THE RREACTION TANK REMAIN SUSPENDED, WITH COARSE CRYSTALS PASSING TO THE CLASSIFICATION ZONE.
Claim 3
Dependent Claim 32 words
The reaction crystallizer according to claim 1, wherein the means for introducing air to the bottom open portion of the second cylinder is disposed above the means for introducing the second reactant.
Claim 4
Dependent Claim 21 words
The reaction crystallizer according to claim 1, wherein the reactants are introduced countercurrently to the second cylinder defining the reaction chamber.
Claim 5
Dependent Claim 25 words
The reaction crystallizer according to claim 1, wherein the reactants are introduced to the open bottom portion of the second cylinder defining the reaction chamber.

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-05-12 1978-11-11 1979-05-13 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-05-12 1982-11-11 1983-05-13 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-05-12 1986-11-11 1987-05-13 $7700.00 Window Closed / Lapsed

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