Patent US3880974A successfully refreshed from Google Patents.
US3880974A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for biaxially producing oriented tubular polyethylene terephthalate films by simultaneous stretching
Assignee: Kohjin Holdings Co Ltd
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Filing: 1973-08-08
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Granted: 1975-04-29
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Expires: 1993-08-08
Abstract
Abstract An improved simultaneous biaxial stretching process for polyethylene terephthalate is provided by observing the following factors: the nonstretched film has a crystallinity of below 18%; the length of the stretching zone is 1 to 1.5 times the maximum expansion diameter; the film in the initial one-third of the stretching zone is kept at 83* - 108*C; and the temperature is smoothly and continuously lowered over the remaining two-thirds of the stretching zone so the film temperature at the stretching end point is at 70* - 78*C.
Inventors
- 👤 Ryohta Nohtomi
- 👤 Tuyoshi Shigeyoshi
- 👤 Masayoshi Sugiyama
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 01:46
CPC Classifications
B; B29; B29C; B29C55/00; B29C55/28; B29C48/00; B29C48/001; B29C48/0018; B29C48/0019; B29C48/03; B29C48/09; B29C48/10
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
174 words
A PROCESS FOR PRODUCING SIMULTANEOUSLY BIAXIALLY ORIENTED TUBULAR POLYETHYLENE TEREPHTHALATE FILMS BY SIMULTANEOUS STRETCHING WHICH COMPRISES EXTRUDING A MOLTEN POLYETHYLENE TEREPHTHALATE RESIN FROM AN ANNULAR DIE, INTRODUCING THE COOLED TUBULAR NON-STRETCHED FILM BETWEEN TWO PAIRS OF SPEED CONTROLLING DEVICES WHICH HAVE A DIFFERENT CIRCUMFERENTIAL SPEED, AND EXPANDING IN A STRETCHING ZONE BY APPLYING GAS PRESSURE INSIDE THE TUBULAR FILM WHILE HEATI*G, BY WHICH THE TUBULAR FILM IS SIMULTANEOUSLY BIAXIALLY STRETCHED 2.5 TO 4.0 TIMES IN BOTH DIRECTIONS, WHEREIN SAID PROCESS IS CHARACTERIZED BY: THE CRYSTALLINITY OF THE NON-STRETCHED FILM IS 3% TO 18%; THE LENGTH OF THE STRETCHING ZONE FROM THE STARTING POINT FOR STRETCHING THE FILM TO THE END POINT OF STRETCHING THEREOF IS KEPT IN THE RANGE OF 1.0-1.5 TIMES OF THE MAXIMUM EXPANSION DIAMETER OF THE STRETCHED FILM; THE FILM TEMPERATURE AT THE INITIAL ONE-THIRD OF THE STRETCHING ZONE IS KEPT AT 83*-108*C; THE FILM TEMPERATURE IS CONTINOUSLY DECREASED IN THE REMAIN: ING TWO-THIRDS OF SAID STRETCHING ZONE; AND THE FILM TEMPERATURE AT THE STRETCHING END POINT IS KEPT AT 70*-78*C.
Claim 2
Dependent Claim
174 words
A PROCESS FOR PRODUCING SIMULTANEOUSLY BIAXIALLY ORIENTED TUBULAR POLYETHYLENE TEREPHTHALATE FILMS BY SIMULTANEOUS STRETCHING WHICH COMPRISES EXTRUDING A MOLTEN POLYETHYLENE TEREPHTHALATE RESIN FROM AN ANNULAR DIE, INTRODUCING THE COOLED TUBULAR NON-STRETCHED FILM BETWEEN TWO PAIRS OF SPEED CONTROLLING DEVICES WHICH HAVE A DIFFERENT CIRCUMFERENTIAL SPEED, AND EXPANDING IN A STRETCHING ZONE BY APPLYING GAS PRESSURE INSIDE THE TUBULAR FILM WHILE HEATI*G, BY WHICH THE TUBULAR FILM IS SIMULTANEOUSLY BIAXIALLY STRETCHED 2.5 TO 4.0 TIMES IN BOTH DIRECTIONS, WHEREIN SAID PROCESS IS CHARACTERIZED BY: THE CRYSTALLINITY OF THE NON-STRETCHED FILM IS 3% TO 18%; THE LENGTH OF THE STRETCHING ZONE FROM THE STARTING POINT FOR STRETCHING THE FILM TO THE END POINT OF STRETCHING THEREOF IS KEPT IN THE RANGE OF 1.0-1.5 TIMES OF THE MAXIMUM EXPANSION DIAMETER OF THE STRETCHED FILM; THE FILM TEMPERATURE AT THE INITIAL ONE-THIRD OF THE STRETCHING ZONE IS KEPT AT 83*-108*C; THE FILM TEMPERATURE IS CONTINOUSLY DECREASED IN THE REMAIN: ING TWO-THIRDS OF SAID STRETCHING ZONE; AND THE FILM TEMPERATURE AT THE STRETCHING END POINT IS KEPT AT 70*-78*C.
Claim 3
Dependent Claim
23 words
A process as claimed in claim 1 wherein the intrinsic viscosity of said polyethylene terephthalate ( eta ) is from 0.55 to 1.10.
Claim 4
Dependent Claim
19 words
A process as claimed in claim 2 wherein said maximum expansion diameter is from 10 cm to 2 m.
Claim 5
Dependent Claim
28 words
A process as claimed in claim 1 wherein the stretching tension is smoothly and continuously changed during the stretching, the stretching tension sigma being defined by the formula:
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1978-04-28 | 1978-10-28 | 1979-04-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1982-04-28 | 1982-10-28 | 1983-04-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1986-04-28 | 1986-10-28 | 1987-04-29 | $7700.00 | Window Closed / Lapsed |