← Back to Patent Explorer
US3868469A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of dutching cocoa

Assignee: Individual
•
Filing: 1974-02-19
•
Granted: 1975-02-25
•
Expires: 1994-02-19
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract The dutching of cocoa to obtain a rich color is accomplished in a continuous fashion by grinding the pressed cake made from cocoa beans, converting the ground mass into a coarse, free-flowing powder, mixing the powder with the appropriate amounts of aqueous alkaline solution and desired additive, feeding this mixture into a combined cooker and pressurized extruder and then pelletizing the cooked composition. The pellets are formed by extruding the mass through appropriate dies and breaking off the rods to form pellets by interaction with a stationary plate. The preferable temperature range of the combined cooking-pressurizing step is 150*-230* F. and the preferred pressures are progressive to between 500 and 1,300 pounds per square inch adjacent the extruding die. The pellets are dried in a continuous fashion by a plurality of gas jet streams that lift and tumble the pellets continuously passing underneath on a vibrating conveyor. The drying is carried out in an inert atmosphere over a preferable time period of 2.5 to 3 minutes at temperatures preferably ranging from 350*-450* F. The initial moisture content of 33% is reduced to approximately 4%. The occurrence of favorable parameters in addition to color, such as taste, pH factor, water absorption and viscosity, low microbial flora, identifies the end product of the process of this invention.

Inventors

  • 👤 Manuel L Chalin

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-02 02:34
CPC Classifications
A; A23; A23G; A23G1/00; A23G1/04; A23G1/20; A23G1/201; A23G1/202; A23G1/02; A23G1/042; A23G1/047; A23G1/30; A23G1/56; A23G2210/00

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 498 words
THE METHOD OF CONTINUOUS DUTCHING AND DRYING OF COCOA SO AS TO ATTAIN A RICH COLOR AND OTHER FAVORABLE PARAMETERS IN THE END PRODUCT, COMPRISING THE STEPS OF: PULVERIZING A PRESS CAKE OR NIBS OF COCOA MATERIAL INTO A FREE-FLOWING POWDER STATE, FORMING AN AQUEOUS ALKALINE SOLUTION HAVING A CONCENTRATION OF ABOUT 3 TO 12 WEIGHT PERCENT WHEREIN THE ALKALINE SOLUTION IS FORMED FROM AMMONIA GAS OR A HYDROXIDE, OXIDE, CARBONATE OR BICARBONATE OF AN ALKALI METAL, AMMONIUM OR AN ALKALINE EARTH METAL OR MIXTURES THEREOF, COMBINING SAID AQUEOUS ALKALINE SOLUTION WITH SAID PULVERIZED MATERIAL AND ADDITIONAL WATER OF DILUTION TO FORM A PRODUCT MIXTURE IN THE FORM OF A DAMP MASS HAVING AN INITIAL MOSITURE CONTENT OF ABOUT 20 TO 35 PERCENT AND A MAXIMUM OF UP TO ABOUT 6 WEIGHT PERCENT ALKALINE EQUIVALENT TO POTASSIUM CARBONATE AND SUBJECTING THE RESULTANT PRODUCT MIXTURE TO THOROUGHT MIXING TO FORM A HOMOGENEOUS PRODUCT MIXTURE, COOKING THE PRODUCT MIXTURE AT A TEMPERATURE OF ABOUT 150*C-230*F. FOR A RESIDENCE PERIOD OF ABBOUT 2 1/2 TO 5 MINUTES WHILE CONTINUING MIXING AND WHILE PROGRESSIVELY INCREASING THE PRESSURE TO A FINAL STAGE OF PRESSURIZATION OF ABOUT 500-1,300 POUNDS PER SQUARE INCH TO FORM A HEATED AND PRESSURIZED MASS, WHEREIN COOKING IS PERFORMED BY FEEDING THE PRODUCT MIXTURE INTO A CHAMBER CONTAINING MEANS TO FORM THE PRODUCT MIXTURE INTO A WORKING MASS CORRESPONDING TO SAID WORKING MASS AS PROGRESSIVELY GREATER PRESSURE ON SAID WORKING MASS AS THE MIXTURE MOVES FROM THE ENTRANCE END OF THE CHAMBER TO THE EXIT END, CONTROLLING THE HEATING IN SAID CHAMBER TO RAISE THE TEMPERATURE OF THE PRODUCT MIXTURE TO COOKING TEMPERATURE, EXTRUDING THE RESULTANT HEATED AND PRESSURIZED MASS THROUGH DIE MEANS TO FORM A PRODUCT ROD, WHEREIN THE STEP OF EXTRUDING THE PRODUCT MASS IS CARRIED OUT AT THE EXIT END OF THE ELONGATED CHAMBER IMMEDIATELY AFTER PRESSURIZED COOKING OF THE PRODUCT MIXTURE BY PASSING THE PRODUCT MASS THROUGH AN EXTRUDING DIE HAVING AT LEAST ONE RESTRICTED OPENING TO FORM THE PRODUCT ROD, DIVIDING THE PRODUCT ROD INTO LENGTHS TO FORM PRODUCT PELLETS, SAID PELLETS AT THIS STAGE CONTAINING ABOUT 85-97 INTEGRALLY FORMED WITH THE BODY AS A PROJECTION THEREFROM AT PERCENT OF THE INITIAL MOISTURE CONTENT, AND DRYING SAID PRODUCT PELLETS ON A FLUIDIZED BED AS THE PELLETS CONTINUOUSLY MOVE ALONG SAID BED BY CONTACT WITH A HEATED INERT GAS AT A TEMPERATURE OF ABOUT 350D-450DF FOR 2.5 TO 3 MINUTES AND THEN RAPIDLY COOLING THE PELLETS WITH FILTERED AIR TO APPROXIMATELY AMBIENT TEMPERATURE, WHEREIN SAID PELLETS HAVE A MOISTURE CONTENT OF ABOUT 4 PERCENT; WHEREBY DUTCHING IS CARRIED OUT IN A CONTROLLED FASHION WITH INTERUPTIONS RIB INTEGRALLY FORMED ON ONE SURFACE OF THE BODY AND EXTENDING LENGTHWISE THEREOF, AND A GUIDE GROOVE FORMED IN THE INNER SURFACE OF THE CASING AND EXTENDING FROM THE FORWARD END THEREOF FOR RECEIVEDLY GUIDING THE RIB, SAID STOP BEING FORMED ON BOTH LATERAL SIDES OF THE RIB, AND PART OF THE GUIDE GROOVE BEING LATERALLY EXTENDED TO PROVIDE SAID RECESS.
Claim 2
Independent Claim 498 words
THE METHOD OF CONTINUOUS DUTCHING AND DRYING OF COCOA SO AS TO ATTAIN A RICH COLOR AND OTHER FAVORABLE PARAMETERS IN THE END PRODUCT, COMPRISING THE STEPS OF: PULVERIZING A PRESS CAKE OR NIBS OF COCOA MATERIAL INTO A FREE-FLOWING POWDER STATE, FORMING AN AQUEOUS ALKALINE SOLUTION HAVING A CONCENTRATION OF ABOUT 3 TO 12 WEIGHT PERCENT WHEREIN THE ALKALINE SOLUTION IS FORMED FROM AMMONIA GAS OR A HYDROXIDE, OXIDE, CARBONATE OR BICARBONATE OF AN ALKALI METAL, AMMONIUM OR AN ALKALINE EARTH METAL OR MIXTURES THEREOF, COMBINING SAID AQUEOUS ALKALINE SOLUTION WITH SAID PULVERIZED MATERIAL AND ADDITIONAL WATER OF DILUTION TO FORM A PRODUCT MIXTURE IN THE FORM OF A DAMP MASS HAVING AN INITIAL MOSITURE CONTENT OF ABOUT 20 TO 35 PERCENT AND A MAXIMUM OF UP TO ABOUT 6 WEIGHT PERCENT ALKALINE EQUIVALENT TO POTASSIUM CARBONATE AND SUBJECTING THE RESULTANT PRODUCT MIXTURE TO THOROUGHT MIXING TO FORM A HOMOGENEOUS PRODUCT MIXTURE, COOKING THE PRODUCT MIXTURE AT A TEMPERATURE OF ABOUT 150*C-230*F. FOR A RESIDENCE PERIOD OF ABBOUT 2 1/2 TO 5 MINUTES WHILE CONTINUING MIXING AND WHILE PROGRESSIVELY INCREASING THE PRESSURE TO A FINAL STAGE OF PRESSURIZATION OF ABOUT 500-1,300 POUNDS PER SQUARE INCH TO FORM A HEATED AND PRESSURIZED MASS, WHEREIN COOKING IS PERFORMED BY FEEDING THE PRODUCT MIXTURE INTO A CHAMBER CONTAINING MEANS TO FORM THE PRODUCT MIXTURE INTO A WORKING MASS CORRESPONDING TO SAID WORKING MASS AS PROGRESSIVELY GREATER PRESSURE ON SAID WORKING MASS AS THE MIXTURE MOVES FROM THE ENTRANCE END OF THE CHAMBER TO THE EXIT END, CONTROLLING THE HEATING IN SAID CHAMBER TO RAISE THE TEMPERATURE OF THE PRODUCT MIXTURE TO COOKING TEMPERATURE, EXTRUDING THE RESULTANT HEATED AND PRESSURIZED MASS THROUGH DIE MEANS TO FORM A PRODUCT ROD, WHEREIN THE STEP OF EXTRUDING THE PRODUCT MASS IS CARRIED OUT AT THE EXIT END OF THE ELONGATED CHAMBER IMMEDIATELY AFTER PRESSURIZED COOKING OF THE PRODUCT MIXTURE BY PASSING THE PRODUCT MASS THROUGH AN EXTRUDING DIE HAVING AT LEAST ONE RESTRICTED OPENING TO FORM THE PRODUCT ROD, DIVIDING THE PRODUCT ROD INTO LENGTHS TO FORM PRODUCT PELLETS, SAID PELLETS AT THIS STAGE CONTAINING ABOUT 85-97 INTEGRALLY FORMED WITH THE BODY AS A PROJECTION THEREFROM AT PERCENT OF THE INITIAL MOISTURE CONTENT, AND DRYING SAID PRODUCT PELLETS ON A FLUIDIZED BED AS THE PELLETS CONTINUOUSLY MOVE ALONG SAID BED BY CONTACT WITH A HEATED INERT GAS AT A TEMPERATURE OF ABOUT 350D-450DF FOR 2.5 TO 3 MINUTES AND THEN RAPIDLY COOLING THE PELLETS WITH FILTERED AIR TO APPROXIMATELY AMBIENT TEMPERATURE, WHEREIN SAID PELLETS HAVE A MOISTURE CONTENT OF ABOUT 4 PERCENT; WHEREBY DUTCHING IS CARRIED OUT IN A CONTROLLED FASHION WITH INTERUPTIONS RIB INTEGRALLY FORMED ON ONE SURFACE OF THE BODY AND EXTENDING LENGTHWISE THEREOF, AND A GUIDE GROOVE FORMED IN THE INNER SURFACE OF THE CASING AND EXTENDING FROM THE FORWARD END THEREOF FOR RECEIVEDLY GUIDING THE RIB, SAID STOP BEING FORMED ON BOTH LATERAL SIDES OF THE RIB, AND PART OF THE GUIDE GROOVE BEING LATERALLY EXTENDED TO PROVIDE SAID RECESS.
Claim 3
Dependent Claim 24 words
The method according to claim 1 wherein the extruding die has an opening ranging from a diameter of about 0.100 to about 0.150 inch.
Claim 4
Dependent Claim 51 words
The method of continuous dutching of cocoa of claim 2 wherein the temperature during the cooking step is maintained in the range of approximately 180* to 212* F. and the pressure is maintained in the final steps of pressurization in the range between about 700 to 1,100 pounds per square inch.
Claim 5
Dependent Claim 38 words
The method of continuous dutching of cocoa of claim 3 wherein the combining step of the aqueous alkaline solution with the pulverized material is carried out to give a product mixture of about 27-33 percent total moisture content.
Claim 6
Dependent Claim 25 words
The method of continuous dutching of cocoa as defined in claim 4 wherein the fat content of the cocoa material is between 10% and 16%.
Claim 7
Dependent Claim 29 words
The method according to claim 5 wherein the pellets are cooled to approximately ambient temperature within a period of about 2.5 to 3 minutes by contacting with filtered air.
Claim 8
Dependent Claim 54 words
The method of continuous dutching of cocoa as required in claim 6 wherein the step of dividing the product rod is performed by moving the product rod from the die means directly into the path of a stationary plate that bends the rod and causes breaking into lengths of approximately one-quarter to 1 inch.
Claim 9
Dependent Claim 58 words
The method of continuous dutching of cocoa as defined in claim 7 wherein the drying step is performed by injecting a plurality of fluid jet streams downwardly onto a continuously moving bed of product pellets, whereby the pellets are lifted and tumbled by the jet streams impinging against the support for the bed of pellets and turning upward.
Claim 10
Dependent Claim 28 words
The method of continuous dutching of cocoa defined in claim 8 wherein the jet streams and the surrounding space where the pellets are dried is an inert gas.
Claim 11
Dependent Claim 67 words
The method of continuous dutching of cocoa as defined in claim 9 wherein the alkaline solution contains sodium carbonate as the alkali, the initial moisture content is about 33%, the temperature within the cooker-extruder is about 190* F., the final pressure is about 900 psig., the residence time within the cooker-extruder is about 4 1/2 minutes and the diameter of the die opening is about one-eighth inch.

References Cited (Backward Citations)

US3056677A Cited
US3544328A Cited
US3754928A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-02-24 1978-08-26 1979-02-25 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-02-24 1982-08-26 1983-02-25 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-02-24 1986-08-26 1987-02-25 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag