Patent US3856831A successfully refreshed from Google Patents.
US3856831A
Expired / Lapsed
US
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Process for preparing hard butter
Assignee: Fuji Oil Co Ltd (fka Fuji Oil Holdings Inc)
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Filing: 1973-07-12
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Granted: 1974-12-24
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Expires: 1993-07-12
Abstract
Abstract Hard butters which are particularly suitable for use as cocoa butter substitutes and which can be used in the manufacture of confectioneries without tempering are prepared by hydrogenating a fat or oil having an iodine value within the range of 60 to 78 and a total content of linoleic and linolenic acids of less than 17 weight percent with a nickel catalyst containing 6 to 21 parts by weight sulfur per 100 parts nickel.
Inventors
- 👤 T Tateishi
- 👤 K Murase
- 👤 Y Iwanaga
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-05 09:15
CPC Classifications
C; C11; C11C; C11C3/00; C11C3/12; C11C3/123
Claims Analysis
Total Claims: 15
Claim 1
Independent Claim
77 words
A PROCESS FOR PREPARING A HARD BUTTER, WHICH IS SUITABLE FOR USE AS A COCOA BUTTER SUBSTITUTE IN THE MANUFACTURE OF CONFECTIONERIES WITHOUT TEMPERING, COMPRISING HYDROGENATING A FAT OR OIL HAVING AN IODINE VALUE WITHIN THE RANGE OF 60 TO 78 AND A TOTAL LINOLEIC ACID AND LINOLENIC ACID CONTENT OF LESS THAN 17 WEIGHT %, BASED ON THE TOTAL WEIGHT OF THE OIL OR FAT AND CALCULATED AS THE FATTY ACID; WITH A NICKEL CATALYST CONTAINING
Claim 2
Dependent Claim
77 words
A PROCESS FOR PREPARING A HARD BUTTER, WHICH IS SUITABLE FOR USE AS A COCOA BUTTER SUBSTITUTE IN THE MANUFACTURE OF CONFECTIONERIES WITHOUT TEMPERING, COMPRISING HYDROGENATING A FAT OR OIL HAVING AN IODINE VALUE WITHIN THE RANGE OF 60 TO 78 AND A TOTAL LINOLEIC ACID AND LINOLENIC ACID CONTENT OF LESS THAN 17 WEIGHT %, BASED ON THE TOTAL WEIGHT OF THE OIL OR FAT AND CALCULATED AS THE FATTY ACID; WITH A NICKEL CATALYST CONTAINING
Claim 3
Dependent Claim
23 words
A process according to claim 1 wherein the iodine value of said fat or oil is within the range of 65 to 73.
Claim 4
Dependent Claim
29 words
A process according to claim 1 wherein said hydrogenation is continued until the per hour rate of decrease in the iodine value of the reaction product is about 1.
Claim 5
Dependent Claim
40 words
A process according to claim 1 wherein said fat or oil includes combined C16 fatty acids in an amount within the range of 25 to 50 weight %, based on the total combined fatty acids or said oil or fat.
Claim 6
Dependent Claim
16 words
A process according to claim 4 wherein said fat or oil is a palm oil fraction.
Claim 7
Dependent Claim
33 words
A process according to claim 4 wherein said fat or oil is prepared by an interesterification between palm oil or a palm oil fraction and soy bean oil or hydrogenated soy bean oil.
Claim 8
Dependent Claim
20 words
A process according to claim 1 further including solvent fractionating the resultant hydrogenated product to obtain a medium melting portion.
Claim 9
Dependent Claim
32 words
A process according to claim 7 wherein said fractionation is carried out in two steps, first cooling the solution to 15* to 25*C. and then cooling the solution to 5* to -10*C.
Claim 10
Dependent Claim
34 words
A process according to claim 1 wherein said catalYst is prepared by subjecting a reduced hydrogenation catalyst to an atmosphere containing hydrogen sulfide for a sufficient time to add the desired sulfur content thereto.
Claim 11
Dependent Claim
38 words
A process according to claim 1 wherein said catalyst is prepared by contacting a reduced nickel catalyst with a mixed gas stream containing hydrogen and hydrogen sulfide for a sufficient time to add the desired sulfur content thereto.
Claim 12
Dependent Claim
10 words
A hard butter prepared by the process of claim 1.
Claim 13
Dependent Claim
10 words
A hard butter prepared by the process of claim 7.
Claim 14
Dependent Claim
35 words
The process according to claim 1 wherein the amount of catalyst employed in within the range of about 0.1 to about 3 wt. %, based on the total weight of the starting fat or oil.
Claim 15
Dependent Claim
24 words
A process according to claim 13 wherein the hydrogenation is carried out at a temperature in the range of about 160* to about 220*C.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1977-12-23 | 1978-06-24 | 1978-12-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1981-12-23 | 1982-06-24 | 1982-12-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1985-12-23 | 1986-06-24 | 1986-12-24 | $7700.00 | Window Closed / Lapsed |