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US3855393A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing low thermal conductivity high strength silica foam

Assignee: Owens Corning Canada Inc
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Filing: 1971-12-09
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Granted: 1974-12-17
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Expires: 1991-12-09
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Abstract

Abstract This specification discloses an improvement in the manufacture of silica foam involving the use of a fluoride type insolubilizer. This invention introduces the additional step of removing the fluoride reaction product from the cured foam by the use of a leaching agent having the ability to form water soluble or water dispersible fluoride compounds or complexes which exhibit a reduced affinity for the silica foam structure. The resulting product is a low thermal conductivity, high strength, non-toxic and incombustible silica foam.

Inventors

  • 👤 R Rao

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 04:47
CPC Classifications
C; C04; C04B; C04B41/00; C04B41/009; C01; C01F; C01F7/00; C01F7/48; C01F7/50; C01F7/54; C04B41/53; C04B41/60; C04B41/72; F; F16; F16L; F16L59/00; F16L59/04

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 172 words
IN A PROCESS FOR THE PREPARATION OF INORGANIC SILICA FOAM WHEREIN AN AQUEOUS ALKALI METAL SILICATE CHASEN FROM SODIUM NOT POTASSIUM SILICATES IS FORMED AND SAID FOAM IS CURED IN THE PRESENCE OF AN ALKALI METAL OR ALKALINE EARTH METAL SILICOFLUORIDE ISOLUBILIZER, RESULTING IN A RIGID FOAMED STRUCTURE HAVING CELL WALLS FORMED OF SILICA, AND CONTAINING INTERSTITIAL ALKALI METAL FLUORIDE REACTION PRODUCT, AND TREATING SAID CURED FOAM FOR THE REMOVAL OF ALKALI METAL FLUORIDE, THE IMPROVEMENT WHICH COMPRISES PREVENTING DEGRADATION AND WEAKENING OF THE STRENGTH AND INSULATION PROPERTIES OF THE FOAMED MASS BY CARRYING OUT SAID LEACHING STEP PRIOR TO THE OCCURANCE OF SUBSTANTIAL DAMAGING CRYSTAL GROWTH OF ALKALI METAL FLUORIDE IN THE WET FOAMED MASS, AND BY LEACHING THE CURED, WET FOAM WITH AN AQUEOUS SOLUTION OR COLLIDAL AQUEOUS SUSPENSION OF AN ACID OR ACIDIC SALT LEACHING AGENT, SAID LEACHING AGENT BEING NON-REACTIVE WITH RESPECT TO SILICA, SAID LEACHING AGENT HAVING THE ABILITY TO FORM WATER SOLUBLE OR WATER DISPERSIBLE FLUORIDE COMPOUNDS OR COMPLEXES HAVING REDUCED AFFINITY FOR THE SILICA STRUCTURE.
Claim 2
Dependent Claim 172 words
IN A PROCESS FOR THE PREPARATION OF INORGANIC SILICA FOAM WHEREIN AN AQUEOUS ALKALI METAL SILICATE CHASEN FROM SODIUM NOT POTASSIUM SILICATES IS FORMED AND SAID FOAM IS CURED IN THE PRESENCE OF AN ALKALI METAL OR ALKALINE EARTH METAL SILICOFLUORIDE ISOLUBILIZER, RESULTING IN A RIGID FOAMED STRUCTURE HAVING CELL WALLS FORMED OF SILICA, AND CONTAINING INTERSTITIAL ALKALI METAL FLUORIDE REACTION PRODUCT, AND TREATING SAID CURED FOAM FOR THE REMOVAL OF ALKALI METAL FLUORIDE, THE IMPROVEMENT WHICH COMPRISES PREVENTING DEGRADATION AND WEAKENING OF THE STRENGTH AND INSULATION PROPERTIES OF THE FOAMED MASS BY CARRYING OUT SAID LEACHING STEP PRIOR TO THE OCCURANCE OF SUBSTANTIAL DAMAGING CRYSTAL GROWTH OF ALKALI METAL FLUORIDE IN THE WET FOAMED MASS, AND BY LEACHING THE CURED, WET FOAM WITH AN AQUEOUS SOLUTION OR COLLIDAL AQUEOUS SUSPENSION OF AN ACID OR ACIDIC SALT LEACHING AGENT, SAID LEACHING AGENT BEING NON-REACTIVE WITH RESPECT TO SILICA, SAID LEACHING AGENT HAVING THE ABILITY TO FORM WATER SOLUBLE OR WATER DISPERSIBLE FLUORIDE COMPOUNDS OR COMPLEXES HAVING REDUCED AFFINITY FOR THE SILICA STRUCTURE.
Claim 3
Dependent Claim 14 words
A method as in claim 1, wherein the alkali metal silicate is sodium silicate.
Claim 4
Dependent Claim 65 words
A method as in claim 1 wherein the leaching agent is an acid or acidic salt derived from the following cations and anions: cations: ammonium, aluminum, zinc, magnesium, calcium, zirconium, titanium, molybdenum, iron, lithium barium and H ; anions: carbonates, bicarbonates, chlorides, nitrates, nitrites, oxychlorides, borates, metaborates, orthoborates, bisulfates, sulfates, bisulfites, sulfites, phosphates, zincates, stannates, aluminates, chromates, dichromates, titanates, zirconates, manganates, molybdates, acetates, and formates.
Claim 5
Dependent Claim 31 words
A method as in claim 3 wherein the leaching agent is chosen from ammonium sulfate, aluminum sulfate, calcium chloride, aluminum chloride, dilute sulfuric acid, and dilute hydrochloric acid, in aqueous solution.

References Cited (Backward Citations)

US2768063A Cited
US3136645A Cited
US3573228A Cited
US3411879A Cited
US3563699A Cited
US3741898A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-12-16 1978-06-17 1978-12-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-12-16 1982-06-17 1982-12-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-12-16 1986-06-17 1986-12-17 $7700.00 Window Closed / Lapsed

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