Patent US3855393A successfully refreshed from Google Patents.
US3855393A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for producing low thermal conductivity high strength silica foam
Assignee: Owens Corning Canada Inc
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Filing: 1971-12-09
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Granted: 1974-12-17
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Expires: 1991-12-09
Abstract
Abstract This specification discloses an improvement in the manufacture of silica foam involving the use of a fluoride type insolubilizer. This invention introduces the additional step of removing the fluoride reaction product from the cured foam by the use of a leaching agent having the ability to form water soluble or water dispersible fluoride compounds or complexes which exhibit a reduced affinity for the silica foam structure. The resulting product is a low thermal conductivity, high strength, non-toxic and incombustible silica foam.
Inventors
- 👤 R Rao
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 04:47
CPC Classifications
C; C04; C04B; C04B41/00; C04B41/009; C01; C01F; C01F7/00; C01F7/48; C01F7/50; C01F7/54; C04B41/53; C04B41/60; C04B41/72; F; F16; F16L; F16L59/00; F16L59/04
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
172 words
IN A PROCESS FOR THE PREPARATION OF INORGANIC SILICA FOAM WHEREIN AN AQUEOUS ALKALI METAL SILICATE CHASEN FROM SODIUM NOT POTASSIUM SILICATES IS FORMED AND SAID FOAM IS CURED IN THE PRESENCE OF AN ALKALI METAL OR ALKALINE EARTH METAL SILICOFLUORIDE ISOLUBILIZER, RESULTING IN A RIGID FOAMED STRUCTURE HAVING CELL WALLS FORMED OF SILICA, AND CONTAINING INTERSTITIAL ALKALI METAL FLUORIDE REACTION PRODUCT, AND TREATING SAID CURED FOAM FOR THE REMOVAL OF ALKALI METAL FLUORIDE, THE IMPROVEMENT WHICH COMPRISES PREVENTING DEGRADATION AND WEAKENING OF THE STRENGTH AND INSULATION PROPERTIES OF THE FOAMED MASS BY CARRYING OUT SAID LEACHING STEP PRIOR TO THE OCCURANCE OF SUBSTANTIAL DAMAGING CRYSTAL GROWTH OF ALKALI METAL FLUORIDE IN THE WET FOAMED MASS, AND BY LEACHING THE CURED, WET FOAM WITH AN AQUEOUS SOLUTION OR COLLIDAL AQUEOUS SUSPENSION OF AN ACID OR ACIDIC SALT LEACHING AGENT, SAID LEACHING AGENT BEING NON-REACTIVE WITH RESPECT TO SILICA, SAID LEACHING AGENT HAVING THE ABILITY TO FORM WATER SOLUBLE OR WATER DISPERSIBLE FLUORIDE COMPOUNDS OR COMPLEXES HAVING REDUCED AFFINITY FOR THE SILICA STRUCTURE.
Claim 2
Dependent Claim
172 words
IN A PROCESS FOR THE PREPARATION OF INORGANIC SILICA FOAM WHEREIN AN AQUEOUS ALKALI METAL SILICATE CHASEN FROM SODIUM NOT POTASSIUM SILICATES IS FORMED AND SAID FOAM IS CURED IN THE PRESENCE OF AN ALKALI METAL OR ALKALINE EARTH METAL SILICOFLUORIDE ISOLUBILIZER, RESULTING IN A RIGID FOAMED STRUCTURE HAVING CELL WALLS FORMED OF SILICA, AND CONTAINING INTERSTITIAL ALKALI METAL FLUORIDE REACTION PRODUCT, AND TREATING SAID CURED FOAM FOR THE REMOVAL OF ALKALI METAL FLUORIDE, THE IMPROVEMENT WHICH COMPRISES PREVENTING DEGRADATION AND WEAKENING OF THE STRENGTH AND INSULATION PROPERTIES OF THE FOAMED MASS BY CARRYING OUT SAID LEACHING STEP PRIOR TO THE OCCURANCE OF SUBSTANTIAL DAMAGING CRYSTAL GROWTH OF ALKALI METAL FLUORIDE IN THE WET FOAMED MASS, AND BY LEACHING THE CURED, WET FOAM WITH AN AQUEOUS SOLUTION OR COLLIDAL AQUEOUS SUSPENSION OF AN ACID OR ACIDIC SALT LEACHING AGENT, SAID LEACHING AGENT BEING NON-REACTIVE WITH RESPECT TO SILICA, SAID LEACHING AGENT HAVING THE ABILITY TO FORM WATER SOLUBLE OR WATER DISPERSIBLE FLUORIDE COMPOUNDS OR COMPLEXES HAVING REDUCED AFFINITY FOR THE SILICA STRUCTURE.
Claim 3
Dependent Claim
14 words
A method as in claim 1, wherein the alkali metal silicate is sodium silicate.
Claim 4
Dependent Claim
65 words
A method as in claim 1 wherein the leaching agent is an acid or acidic salt derived from the following cations and anions: cations: ammonium, aluminum, zinc, magnesium, calcium, zirconium, titanium, molybdenum, iron, lithium barium and H ; anions: carbonates, bicarbonates, chlorides, nitrates, nitrites, oxychlorides, borates, metaborates, orthoborates, bisulfates, sulfates, bisulfites, sulfites, phosphates, zincates, stannates, aluminates, chromates, dichromates, titanates, zirconates, manganates, molybdates, acetates, and formates.
Claim 5
Dependent Claim
31 words
A method as in claim 3 wherein the leaching agent is chosen from ammonium sulfate, aluminum sulfate, calcium chloride, aluminum chloride, dilute sulfuric acid, and dilute hydrochloric acid, in aqueous solution.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1977-12-16 | 1978-06-17 | 1978-12-17 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1981-12-16 | 1982-06-17 | 1982-12-17 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1985-12-16 | 1986-06-17 | 1986-12-17 | $7700.00 | Window Closed / Lapsed |