Patent US3852401A successfully refreshed from Google Patents.
US3852401A
Expired / Lapsed
US
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Method for producing artificial fibers containing microcapsules
Assignee: Japan Exlan Co Ltd
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Filing: 1972-06-27
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Granted: 1974-12-03
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Expires: 1992-06-27
Abstract
Abstract Microcapsules containing a fiber modifier are introduced into the fibers by forming the microcapsules directly in the polymer spinning solution and extruding the resultant spinning solution in the usual manner.
Inventors
- 👤 H Suzuki
- 👤 T Ichimaru
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 03:04
CPC Classifications
B; B01; B01J; B01J13/00; B01J13/02; B01J13/025; D; D01; D01F; D01F1/00; D01F1/02; D01F1/10; D01F6/00; D01F6/02; D01F6/18; D01F6/28; D01F6/38; Y; Y10; Y10T; Y10T428/00; Y10T428/29; Y10T428/2982; Y10T428/2984; Y10T428/2985; Y10T428/2987; Y10T428/2989
Claims Analysis
Total Claims: 15
Claim 1
Independent Claim
154 words
IN A METHOD FOR PRODUCING ARTIFICIAL FIBERS CONTAINING MICROCAPSULES OF A FIBER MODIFIER SELECTED FROM THE GROUP CONSISTING OF SANITARY PROCESSING AGENTS, FLAME RESISTANT AGENTS, LUMINOUS SUBSTANCES, DEODORANTS, SOFTENING AGENTS, PERFUMES, ANTISTATIC AGENTS, ANTIOXIDANTS AND U.V. ABSORBERS, BY EXTRUDING A SPINNING SOLUTION CONTAINING THE MICROCAPSULES IN A FINELY DISPERSED STATE, A FIBER FORMING POLYMER SELECTED FROM THE GROUP CONSISTING OF POLYAMIDES, POLYESTERS, POLYVINYL CHLORIDE, POLYVINYL ALCOHOL, POLYACRYLONITRILE, COPOLYMERS OF ACRYLONITRILE WITH ONE OR MORE OTHER VINYL MONOMERS AND CELLULOSE ACETATE, AND A SOLVENT FOR THE POLYMER, THE IMPROVEMENT WHEREIN THE SPINNING SOLUTION CONTAINING THE MICROCAPSULES IS PREPARED BY FINELY DISPERSING IN THE SPINNING SOLUTION THE FIBER MODIFIER WHICH IS INCOMPATIBLE WITH THE SPINNING SOLUTION AND A FILM-FORMING SUBSTANCE SOLUBLE IN THE SPINNING SOLUTION OR FIBER MODIFIER, AND FORMING A FILM INSOLUBLE IN THE SPINNING SOLUTION ON THE SURFACE OF THE DISPERSED PARTICLES OF THE FIBER MODIFIER TO FORM MICROCAPSULES ENCLOSING THE FIBER MODIFIER THEREIN.
Claim 2
Dependent Claim
154 words
IN A METHOD FOR PRODUCING ARTIFICIAL FIBERS CONTAINING MICROCAPSULES OF A FIBER MODIFIER SELECTED FROM THE GROUP CONSISTING OF SANITARY PROCESSING AGENTS, FLAME RESISTANT AGENTS, LUMINOUS SUBSTANCES, DEODORANTS, SOFTENING AGENTS, PERFUMES, ANTISTATIC AGENTS, ANTIOXIDANTS AND U.V. ABSORBERS, BY EXTRUDING A SPINNING SOLUTION CONTAINING THE MICROCAPSULES IN A FINELY DISPERSED STATE, A FIBER FORMING POLYMER SELECTED FROM THE GROUP CONSISTING OF POLYAMIDES, POLYESTERS, POLYVINYL CHLORIDE, POLYVINYL ALCOHOL, POLYACRYLONITRILE, COPOLYMERS OF ACRYLONITRILE WITH ONE OR MORE OTHER VINYL MONOMERS AND CELLULOSE ACETATE, AND A SOLVENT FOR THE POLYMER, THE IMPROVEMENT WHEREIN THE SPINNING SOLUTION CONTAINING THE MICROCAPSULES IS PREPARED BY FINELY DISPERSING IN THE SPINNING SOLUTION THE FIBER MODIFIER WHICH IS INCOMPATIBLE WITH THE SPINNING SOLUTION AND A FILM-FORMING SUBSTANCE SOLUBLE IN THE SPINNING SOLUTION OR FIBER MODIFIER, AND FORMING A FILM INSOLUBLE IN THE SPINNING SOLUTION ON THE SURFACE OF THE DISPERSED PARTICLES OF THE FIBER MODIFIER TO FORM MICROCAPSULES ENCLOSING THE FIBER MODIFIER THEREIN.
Claim 3
Dependent Claim
36 words
A method according to claim 1 wherein the microcapsules enclosing the fiber modifier are produced by a microencapsulation method selected from the group consisting of in situ polymerization, interfacial polymerization, phase separation and intra-liquid drying process.
Claim 4
Dependent Claim
23 words
A method according to claim 1 wherein 0.5 to 40 percent by weight of said fiber-forming polymer is contained in the spinning solution.
Claim 5
Dependent Claim
19 words
A method according to claim 1 wherein the microcapsules are of a size of 0.5 to 30 Mu .
Claim 6
Dependent Claim
16 words
A method according to claim 1 wherein said fiber-forming polymer is an acrylonitrile polymer or copolymer.
Claim 7
Dependent Claim
13 words
A method according to claim 1 wherein said fiber-forming polymer is cellulose acetate.
Claim 8
Dependent Claim
28 words
A method according to claim 1 wherein said fiber modifier is finely dispersed in the spinning solution with a particle diameter of not more than 30 Mu .
Claim 9
Dependent Claim
13 words
A method according to claim 1 wherein said coagulating medium is a liquid.
Claim 10
Dependent Claim
13 words
A method according to claim 1 wherein said coagulating medium is a gas.
Claim 11
Dependent Claim
17 words
A method according to claim 1 wherein said film-forming substance is a polyvinyl alcohol or melamine-formaldehyde precondensate.
Claim 12
Dependent Claim
43 words
A method according to claim 1 wherein the fiber-forming polymer is an acrylonitrile polymer or copolymer and the solvent is selected from the group consisting of dimethyl formamide, dimethyl acetamide, ethylene carbonate, dimethyl sulfoxide, concentrated aqueous solutions of inorganic salts and nitric acid.
Claim 13
Dependent Claim
26 words
A method according to claim 1 wherein the spinning solution is composed of an acrylonitrile polymer or copolymer and a concentrated aqueous solution of a thiocyanate.
Claim 14
Dependent Claim
27 words
A method according to claim 1 wherein the amount of the fiber modifier in the fibers is not more than 40 percent by weight of the fibers.
Claim 15
Dependent Claim
31 words
A method according to claim 1 wherein 2 to 200 percent by weight of the film-forming substance, based on the weight of the fiber modifier, is added to the spinning solution.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1977-12-02 | 1978-06-03 | 1978-12-03 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1981-12-02 | 1982-06-03 | 1982-12-03 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1985-12-02 | 1986-06-03 | 1986-12-03 | $7700.00 | Window Closed / Lapsed |