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Dense silicon carbide ceramic and method of making same

Assignee: General Electric Co
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Filing: 1972-11-27
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Granted: 1974-12-03
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Expires: 1992-11-27
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Abstract

Abstract A dense silicon carbide ceramic is disclosed which is composed of a silicon carbide matrix filled with a boron carbide-silicon carbide composition. The silicon carbide ceramic is prepared by performing a porous silicon carbide body, infiltrating the pores of the body with a boron carbide-silicon carbide melt at a sufficient temperature, and directionally cooling the filled body to advance the solidification front through the body whereby a dense substantially nonporous ceramic is formed.

Inventors

  • 👤 S Prochazka

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 03:23
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/515; C04B35/56; C04B35/565

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 75 words
A SILICON CARBIDE CERAMIC BODY COMPRISING A SILICON CARBIDE MATRIC FILLED WITH A COMPOSITION CONSISTING ESSENTIALLY IN WEIGHT PERCENT OF 55-70 PERCENT OF BORON CARBIDE, 30-45 PERCENT OF SILICON CARBIDE AND, BASED ON THE TOTAL WEIGHT OF THEP COMPOSITION, AN AMOUNT UP TO 10 PERCENT BY WEIGHT AND AT LEAST SUFFICIENT O LOWER THE TEMPERATURE OF LIQUID FORMATION OF SAID COMPSITION, OF A MEMBER SELECTED FROM THE GROUP CONSISTING OF SILICON METAL AND ALUMINUM CARBIDE.
Claim 2
Dependent Claim 75 words
A SILICON CARBIDE CERAMIC BODY COMPRISING A SILICON CARBIDE MATRIC FILLED WITH A COMPOSITION CONSISTING ESSENTIALLY IN WEIGHT PERCENT OF 55-70 PERCENT OF BORON CARBIDE, 30-45 PERCENT OF SILICON CARBIDE AND, BASED ON THE TOTAL WEIGHT OF THEP COMPOSITION, AN AMOUNT UP TO 10 PERCENT BY WEIGHT AND AT LEAST SUFFICIENT O LOWER THE TEMPERATURE OF LIQUID FORMATION OF SAID COMPSITION, OF A MEMBER SELECTED FROM THE GROUP CONSISTING OF SILICON METAL AND ALUMINUM CARBIDE.
Claim 3
Dependent Claim 15 words
The body of claim 1, wherein said matrix comprises at least 70 percent by volume.
Claim 4
Independent Claim 138 words
A method of making a dense silicon carbide ceramic comprising the steps of a. preforming a porous silicon carbide body having a density of at least 70 percent, b. placing a composition consisting essentially in weight percent of 55-70 of boron carbide and 30-45 percent of silicon carbide in contact with the preformed porous body, c. firing the body in an inert atmosphere at a sufficient temperature whereby the composition infiltrates the voids of the preformed porous body, and d. directionally cooling the composite body under a thermal gradient extending across the body from the point at which the infiltrating composition is placed in contact with the body to a point remote from the contact point, with the contact point being at a higher temperature than the remote point to form a dense substantially nonporous silicon carbide ceramic.
Claim 5
Independent Claim 138 words
A method of making a dense silicon carbide ceramic comprising the steps of a. preforming a porous silicon carbide body having a density of at least 70 percent, b. placing a composition consisting essentially in weight percent of 55-70 of boron carbide and 30-45 percent of silicon carbide in contact with the preformed porous body, c. firing the body in an inert atmosphere at a sufficient temperature whereby the composition infiltrates the voids of the preformed porous body, and d. directionally cooling the composite body under a thermal gradient extending across the body from the point at which the infiltrating composition is placed in contact with the body to a point remote from the contact point, with the contact point being at a higher temperature than the remote point to form a dense substantially nonporous silicon carbide ceramic.
Claim 6
Dependent Claim 21 words
The method of claim 3, wherein said preformed porous silicon carbide body is prepared by pressing a particulate silicon carbide mixture.
Claim 7
Dependent Claim 16 words
The method of claim 3, wherein said preformed silicon carbide body is prepared by slip casting.
Claim 8
Dependent Claim 26 words
The method of claim 3, wherein said composition consists essentially of 70 percent by weight of boron carbide and 30 percent by weight of silicon carbide.
Claim 9
Dependent Claim 30 words
The method of claim 3, wherein said composition additionally contains up to 10 percent by weight of an additive selected from the group consisting of silicon metal and aluminum carbide.
Claim 10
Dependent Claim 20 words
ThE method of claim 3, wherein said inert atmosphere is argon and the infiltration is performed under a subatmospheric pressure.
Claim 11
Dependent Claim 18 words
The method of claim 3, wherein said thermal gradient is in the range of 5*-50* C. per centimeter.

References Cited (Backward Citations)

US2108794A Cited
US2637091A Cited
US3275722A Cited
US3649342A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-12-02 1978-06-03 1978-12-03 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-12-02 1982-06-03 1982-12-03 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-12-02 1986-06-03 1986-12-03 $7700.00 Window Closed / Lapsed

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