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US3850591A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for preparation of high pressure apparatus reaction vessel construction

Assignee: General Electric Co
•
Filing: 1971-07-01
•
Granted: 1974-11-26
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Expires: 1991-07-01
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Abstract

Abstract An improved reaction vessel construction for the compaction of a mass of dense, strong particles e.g. diamond is disclosed. This improved construction embodies a mechanically unstable structural system to prevent the formation of pressure-supporting geometries within or encircling the mass.

Inventors

  • 👤 R Wentorf

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 20:12
CPC Classifications
B; B01; B01J; B01J3/00; B01J3/06; B01J3/065; B01J3/062; B01J2203/00; B01J2203/06; B01J2203/0605; B01J2203/062; B01J2203/0645; B01J2203/065; B01J2203/0655; B01J2203/066; B01J2203/0675; B01J2203/0685

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 260 words
IN A PROCESS FOR THE PEPARATION OF A REACTION VESSEL TO BE INTRODUCED INTO A HIGH PRESSURE, HIGH TEMPERATURE APPARATUS FOR THE CONDUCT OF HIGH PRESSURE, HIGH TEMEPRATURE COMPACTION OF CRYSTALLINE MATERIAL SELECTED FROM THE GROUP CONSISTING OF DIAMOND CUBIC BORON NITRIDE AND MIXTURES THEREOF DURING WHICH PREPARAION SAID CRYSTALLINE MATERIAL TOGETHER WITH CATALYST METAL, TO ENABLE THE CONVERSION OF THE HEXAGONAL FORM 0F SAID CRYSTALLINE MATERIAL TO THE CUBIC FORM THEREOF, ARE PLACED WITHIN A PROTECTIVE METAL ENCLOSURE AND SAID PROTECTIVE METAL ENCLOSURE IN TURN IS ASSEMBLED WITHIN A SERIES OF INTERFITTING INNER AND OUTER ELEMENTS, THE OUTER ELEMENT OF SAID REACTION VESSEL BEING IN THE SHAPED OF A HOLLOW WALL AND BEING MADE FROM ELECTRICALLY NON-CONDUCTIVE, THERMALLY INSULATING MATERIAL MEANS BEING LOCATED ADJACENT SAID OUTER ELEMENT OF CONDUCTING ELECTRICAL CURRENT INTO AND OUT OF SAID REACTION VESSEL FOR HEATING SAME, THE IMPROVEMENT IN SAID PREPARATION COMPRISING, A. FORMING SAID OUTER ELEMENT FROM A DEFORMABLE PRESSURETRANSMITING MATERIAL SELECTED FROM THE GROUP CONSISTING OF SALT AND TALC AND B. ARRANGING A SINGLE MASS OF SAID CRYSTALLINE MATERIAL IN THE FORM OF A VOLUME HAVING A PLURALITY OF MAJOR SURFACES AND A SINGLE CONCENTRATION OF SAID CATALYST METAL WITHIN SAID PROTECTIVE METAL ENCLOSURE, SAID SINGLE CONCENTRATION OF METAL BEING CONTIGUOUS WITH ONLY ONE MAJOR SURFACE OF SAID MASS, WHEREBY DURING THE CONDUCT OF THE COMPACTION PROCESS AT A TEMPERATURE RENDERING MOLTEN SAID CONCENTRATION OF CATALYST METAL, THE COMPACTION FRONT WALL ADVANCE THROUGH SAID MASS OF CRYSTALLINE MATERIAL IN A SINGLE GENERAL DIRECTION DUE TO THE MECHANICAL INSTABILITY OF THE COMPACTION SYSTEM.
Claim 2
Dependent Claim 260 words
IN A PROCESS FOR THE PEPARATION OF A REACTION VESSEL TO BE INTRODUCED INTO A HIGH PRESSURE, HIGH TEMPERATURE APPARATUS FOR THE CONDUCT OF HIGH PRESSURE, HIGH TEMEPRATURE COMPACTION OF CRYSTALLINE MATERIAL SELECTED FROM THE GROUP CONSISTING OF DIAMOND CUBIC BORON NITRIDE AND MIXTURES THEREOF DURING WHICH PREPARAION SAID CRYSTALLINE MATERIAL TOGETHER WITH CATALYST METAL, TO ENABLE THE CONVERSION OF THE HEXAGONAL FORM 0F SAID CRYSTALLINE MATERIAL TO THE CUBIC FORM THEREOF, ARE PLACED WITHIN A PROTECTIVE METAL ENCLOSURE AND SAID PROTECTIVE METAL ENCLOSURE IN TURN IS ASSEMBLED WITHIN A SERIES OF INTERFITTING INNER AND OUTER ELEMENTS, THE OUTER ELEMENT OF SAID REACTION VESSEL BEING IN THE SHAPED OF A HOLLOW WALL AND BEING MADE FROM ELECTRICALLY NON-CONDUCTIVE, THERMALLY INSULATING MATERIAL MEANS BEING LOCATED ADJACENT SAID OUTER ELEMENT OF CONDUCTING ELECTRICAL CURRENT INTO AND OUT OF SAID REACTION VESSEL FOR HEATING SAME, THE IMPROVEMENT IN SAID PREPARATION COMPRISING, A. FORMING SAID OUTER ELEMENT FROM A DEFORMABLE PRESSURETRANSMITING MATERIAL SELECTED FROM THE GROUP CONSISTING OF SALT AND TALC AND B. ARRANGING A SINGLE MASS OF SAID CRYSTALLINE MATERIAL IN THE FORM OF A VOLUME HAVING A PLURALITY OF MAJOR SURFACES AND A SINGLE CONCENTRATION OF SAID CATALYST METAL WITHIN SAID PROTECTIVE METAL ENCLOSURE, SAID SINGLE CONCENTRATION OF METAL BEING CONTIGUOUS WITH ONLY ONE MAJOR SURFACE OF SAID MASS, WHEREBY DURING THE CONDUCT OF THE COMPACTION PROCESS AT A TEMPERATURE RENDERING MOLTEN SAID CONCENTRATION OF CATALYST METAL, THE COMPACTION FRONT WALL ADVANCE THROUGH SAID MASS OF CRYSTALLINE MATERIAL IN A SINGLE GENERAL DIRECTION DUE TO THE MECHANICAL INSTABILITY OF THE COMPACTION SYSTEM.
Claim 3
Dependent Claim 31 words
The improvement as recited in claim 1 wherein the concentration of catalyst metal ranges from about 5 to 10 percent by volume of the material enclosed within the protective metal enclosure.
Claim 4
Dependent Claim 34 words
The improvement as recited in claim 1 wherein the crystalline material is disposed in a disc shaped volume and the catalyst metal is in the form of a disc shape of considerably reduced thicknEss.
Claim 5
Dependent Claim 52 words
The improvement as recited in claim 1 wherein the crystalline material is disposed in an annular volume and the catalyst metal is in the shape of a hollow cylinder disposed within said mass of crystalline material and the core of the hollow cylinder is occupied by a solid cylinder of sodium chloride.

References Cited (Backward Citations)

US2703750A Cited
US2992900A Cited
US3310501A Cited
US3423177A Cited
US3574580A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-11-25 1978-05-27 1978-11-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-11-25 1982-05-27 1982-11-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-11-25 1986-05-27 1986-11-26 $7700.00 Window Closed / Lapsed

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