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US3846323A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for making a permanent magnet material

Assignee: Robert Bosch GmbH
•
Filing: 1972-08-25
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Granted: 1974-11-05
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Expires: 1992-08-25
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Abstract

Abstract A permanent magnet material comprises a ferrite of the elements barium, strontium or lead or a combination of these elements. The ferrite has a lattice structure of a strong uniaxial magnetic anisotropy and includes in its crystal structure a substitution element selected from the group consisting of Sb, As and P which has at least two valences of which the lowermost is 3 and which forms ions at both valences which have a radius substantially equal to or smaller than the radius of the Fe3-ions of the ferrite which ions are unable to form a ferromagnetic coupling and which are substituted in their trivalent form for at least part of said Fe3 ions in at least one sublattice of said lattice structure. The material is made by sintering a finely ground mixture of the oxides or oxide furnishing compounds, then heat-treating the sintered product in such a manner that it releases part of its oxygen and that the ions are being converted in the lattice structure of the ferrite into their trivalent form; then comminuting the product to single domain grain size and finally tempering it in a nonoxidising atmosphere.

Inventors

  • 👤 F Esper
  • 👤 G Kaiser

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 17:24
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/01; C04B35/26; C04B35/2683

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 260 words
A PROCESS OF MAKING A PERMANENT MAGNET MATERIAL, COMPRISING THE STEPS OF FORMING A PARTICULATE MIXTURE INCLUDING A SUBSTANCE SELECTED FROM THE GROUP CONSISTING OF THE OXIDES AND OXIDE FURNISHING COMPOUNDS OF FE, A SUBSTANCE SELECTED FROM THE GROUP CONSISTING OF THE OXIDES AND OXIDES FURNIDHING COMPOUNDS OF BA, SR AND PB, AND A SUBSTANCE SELECTED FROM THE GROUP CONSISTING OF THE OXIDES AND OXIDES FURNISHING COMPOUNDS OF SB, AS AND P;SINTERING SAID MIXTURE IN AIR SO AS TO EFFECT REACTION OF SAID SUBSTANCES AND FORM A FIRST PRODUCT OF THE FORMULA MO. (FE203)6 WHEREIN FET3 IONS IN SAID SB, AS AND P ARE REPLACED BY THE IONS OF AT LEAST ONE OF SAID SB, AS AND P TO SUCH AN EXTENT AS TO CAUSE A LOWERING OF THE TEMPERATURE COEFFICIENT OF THE REVERSIBLE TEMPERATURE CHANGE OF THE MAGNETIC SATURATION MOMENT FROM THAT OF MO.(FE2O3)6 WHEREIN MO REPLACEMENT OF THE FE3 IONS IS EFFECTED, SAID BA, SR AND PB; HEAT AS AND P HAVING A VALENCE IN EXCESS OF T3, AND SAID M OF SAID MO. (FE203)6 BEING AT LEAST ONE OF SAID BA, SR AND PB; HEAT TREATING SAID FIRST PRODUCT WITHIN A TEMPERATURE RANGE OF 1,200* TO 1,350*C SO AS TO CAUSE EVOLUTION OF PART OF THE OXYGEN OF SAID PRODUCT AND SO AS TO CONVERT SAID IONS OF SB, AS AND P TO THEIR TRIVALENT STATE THEREBY FORMING A SECOND PRODUCT; COMMINUTING SAID SECOND PRRODUCT TO SINGLE DOMAIN SIZE; AND TEMPERING THE COMMINUTED SECOND PRODUCT IN A NON-OXIDIZING ATOMPHERE WITHIN A TEMPERATURE RANGE OF 750* TO 1,200*C.
Claim 2
Dependent Claim 260 words
A PROCESS OF MAKING A PERMANENT MAGNET MATERIAL, COMPRISING THE STEPS OF FORMING A PARTICULATE MIXTURE INCLUDING A SUBSTANCE SELECTED FROM THE GROUP CONSISTING OF THE OXIDES AND OXIDE FURNISHING COMPOUNDS OF FE, A SUBSTANCE SELECTED FROM THE GROUP CONSISTING OF THE OXIDES AND OXIDES FURNIDHING COMPOUNDS OF BA, SR AND PB, AND A SUBSTANCE SELECTED FROM THE GROUP CONSISTING OF THE OXIDES AND OXIDES FURNISHING COMPOUNDS OF SB, AS AND P;SINTERING SAID MIXTURE IN AIR SO AS TO EFFECT REACTION OF SAID SUBSTANCES AND FORM A FIRST PRODUCT OF THE FORMULA MO. (FE203)6 WHEREIN FET3 IONS IN SAID SB, AS AND P ARE REPLACED BY THE IONS OF AT LEAST ONE OF SAID SB, AS AND P TO SUCH AN EXTENT AS TO CAUSE A LOWERING OF THE TEMPERATURE COEFFICIENT OF THE REVERSIBLE TEMPERATURE CHANGE OF THE MAGNETIC SATURATION MOMENT FROM THAT OF MO.(FE2O3)6 WHEREIN MO REPLACEMENT OF THE FE3 IONS IS EFFECTED, SAID BA, SR AND PB; HEAT AS AND P HAVING A VALENCE IN EXCESS OF T3, AND SAID M OF SAID MO. (FE203)6 BEING AT LEAST ONE OF SAID BA, SR AND PB; HEAT TREATING SAID FIRST PRODUCT WITHIN A TEMPERATURE RANGE OF 1,200* TO 1,350*C SO AS TO CAUSE EVOLUTION OF PART OF THE OXYGEN OF SAID PRODUCT AND SO AS TO CONVERT SAID IONS OF SB, AS AND P TO THEIR TRIVALENT STATE THEREBY FORMING A SECOND PRODUCT; COMMINUTING SAID SECOND PRRODUCT TO SINGLE DOMAIN SIZE; AND TEMPERING THE COMMINUTED SECOND PRODUCT IN A NON-OXIDIZING ATOMPHERE WITHIN A TEMPERATURE RANGE OF 750* TO 1,200*C.
Claim 3
Dependent Claim 27 words
A process as defined in claim 1, wherein at least 0.5 Fe 3 ions are replaced by said Sb, As and P per molecular unit of MO.(Fe2O3)6.
Claim 4
Dependent Claim 21 words
A process as defined in claim 1, wherein approximately 1 atom of said oxygen is evolved per replaced Fe 3 ion.
Claim 5
Dependent Claim 37 words
A process as defined in claim 1; further comprising the step of press forming the comminuted second product into a shaped body prior to said tempering step; and wherein said tempering step comprises sintering said shaped body.
Claim 6
Dependent Claim 22 words
A process as defined in claim 1, wherein said sintering step is carried out at a temperature between substantially 1,100* and 1,350*C.

References Cited (Backward Citations)

US2900344A Cited
US2837483A Cited
US3563899A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-11-04 1978-05-06 1978-11-05 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-11-04 1982-05-06 1982-11-05 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-11-04 1986-05-06 1986-11-05 $7700.00 Window Closed / Lapsed

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