Patent US3843592A successfully refreshed from Google Patents.
← Back to Patent Explorer
US3843592A Expired / Lapsed US ⏱️ 0.0 years remaining

Fire resistant polychloroprene adhesive

Assignee: PEACE INDUSTRIES Ltd 1100 HICKS RD ROLLING MEADOWS IL A CORP OF
•
Filing: 1973-05-07
•
Granted: 1974-10-22
•
Expires: 1993-05-07
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract A novel self-curing polychloroprene base adhesive composition is provided which exhibits unexpectedly superior resistance to fire and high temperature conditions, shows reduced staining properties, exhibits good shelf life and is especially useful in the building construction field in lieu of traditional fasteners such as nails, screws and the like. The composition contains polychloroprene elastomer, asbestos, a combination of heat advancing oil soluble phenolic resins, non-staining antioxidants and fillers. The novel properties of this composition are achieved by a process which includes forming a solvent solution of the phenolic resin which is admixed with magnesium or cadmium oxide. This mixture is held for a period of time for prereaction, preferably at least two weeks, or more, although shorter times will suffice. A separate admixture of neoprene, magnesium or cadmium oxide, zinc oxide, antioxidants and asbestos is formed and is thoroughly admixed in the dry state below 140*F. The two admixtures are blended for a period of about eight hours or more to provide a high viscosity composition and solvents are added to the mixed composition to reduce the viscosity to from about 23,000 to about 90,000 centipoises.

Inventors

  • 👤 G Perkins

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 13:06
CPC Classifications
C; C09; C09J; C09J111/00; C08; C08K; C08K5/00; C08K5/36; C08K5/39; C08L; C08L11/00; C08L61/00; C08L61/04; C08K3/00; C08K3/18; C08K3/20; C08K3/22; C08K3/34; C08K3/346; C08K7/00; C08K7/02; C08K7/04; C08K7/10; C08K7/12; C08L2666/00; C08L2666/02; C08L2666/14; C08L2666/16

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 194 words
A PROCESS FOR PREPARING A FIRE RESISTANT ADHESIVE COMPOSITION COMPRISING ON A WEIGHT PERCENT BASIS: FROM 20 TO 80 PERCENT POLYCHLOROPRENE; FROM 15 TO 50 PERCENT HEAT ADVANCING, OIL SOLUBLE PHENOLIC RESIN OF WHICH AT LEAST 20 PERCENT IS A RESIN WHICH IS THERMALLY STABLE AT 500*F. AND ABOVE; FROM 1 TO 50 PERCENT ASBESTOS; FROM 2 TO 20 PERCENT OF AN OXIDE SELECTED FROM THE GROUP CONSISTING OF MAGNESIUM AND CADMIUM OXIDE; FROM 0 TO 50 PERCENT FILLERS; AND FROM 0.1 TO 2 PERCENT EACH OF A DIALKYL THIODIPROPIONATE AND A NICKEL DIBUTYL DITHIOCARBAMATE ANTIOXIDANT, SAID PROCESS COMPRISING: A. FORMING A MIXTURE OF THE PHENOLIC RESIN AND A PORTION OF THE MAGNESIUM OR CADMIUM OXIDE IN AN ORGANIC SOLVENT, ADMIXING THE SAME UNTIL DISPERSION IS COMPLETE, AND PERMITTING THE ADMIXTURE TO PRE-REACT; B. BLENDING THE POLYCHLOROPRENE ELASTOMER WITH THE REMAINDER OF THE MAGNESIUM OR CADMIUM OXIDES, THE ANTIOXIDANTS, ZINC OXIDE AND ASBESTOS FIBER IN A HIGH SHEAR MIXING APPARATUS AND THEN DISSOLVING THE BLEND IN AN ORGANIC SOLVENT; AND C. BLENDING THE COMPOSITIONS OBTAINED FROM STEPS A AND B AT A TEMPERATURE BELOW ABOUT 140*F. FOR A PERIOD OF AT LEAST 8 HOURS.
Claim 2
Dependent Claim 194 words
A PROCESS FOR PREPARING A FIRE RESISTANT ADHESIVE COMPOSITION COMPRISING ON A WEIGHT PERCENT BASIS: FROM 20 TO 80 PERCENT POLYCHLOROPRENE; FROM 15 TO 50 PERCENT HEAT ADVANCING, OIL SOLUBLE PHENOLIC RESIN OF WHICH AT LEAST 20 PERCENT IS A RESIN WHICH IS THERMALLY STABLE AT 500*F. AND ABOVE; FROM 1 TO 50 PERCENT ASBESTOS; FROM 2 TO 20 PERCENT OF AN OXIDE SELECTED FROM THE GROUP CONSISTING OF MAGNESIUM AND CADMIUM OXIDE; FROM 0 TO 50 PERCENT FILLERS; AND FROM 0.1 TO 2 PERCENT EACH OF A DIALKYL THIODIPROPIONATE AND A NICKEL DIBUTYL DITHIOCARBAMATE ANTIOXIDANT, SAID PROCESS COMPRISING: A. FORMING A MIXTURE OF THE PHENOLIC RESIN AND A PORTION OF THE MAGNESIUM OR CADMIUM OXIDE IN AN ORGANIC SOLVENT, ADMIXING THE SAME UNTIL DISPERSION IS COMPLETE, AND PERMITTING THE ADMIXTURE TO PRE-REACT; B. BLENDING THE POLYCHLOROPRENE ELASTOMER WITH THE REMAINDER OF THE MAGNESIUM OR CADMIUM OXIDES, THE ANTIOXIDANTS, ZINC OXIDE AND ASBESTOS FIBER IN A HIGH SHEAR MIXING APPARATUS AND THEN DISSOLVING THE BLEND IN AN ORGANIC SOLVENT; AND C. BLENDING THE COMPOSITIONS OBTAINED FROM STEPS A AND B AT A TEMPERATURE BELOW ABOUT 140*F. FOR A PERIOD OF AT LEAST 8 HOURS.
Claim 3
Dependent Claim 25 words
A process according to claim 1 wherein the polychloroprene is employed in an amount of from 45 to 65 percent by weight of said composition.
Claim 4
Dependent Claim 25 words
A process according to claim 1 wherein the oxide is magnesium oxide and is employed in amounts of from 2 to 10 percent by weight.
Claim 5
Dependent Claim 30 words
A process according to claim 1 wherein the oxide employed is an admixture of magnesium and cadmium oxide in an aggregate amount of from 2 to 10 percent by weight.
Claim 6
Dependent Claim 31 words
A process according to claim 1 wherein from 30 to 100 percent of the phenolic resin employed is a high cure rate resin having thermal stability at temperatures above about 500*F.
Claim 7
Dependent Claim 27 words
A process according to claim 1 wherein the composition produced by Step C is admixed with solvents to a viscosity of from 23,000 to about 90,000 centipoises.
Claim 8
Dependent Claim 29 words
A process according to claim 1 wherein the antioxidants are dilauryl thiodipropionate and nickel dibutyl dithiocarbamate, each employed in an amount of from 0.1 to 2 percent by weight.
Claim 9
Dependent Claim 18 words
A process according to claim 1 wherein Step C is carried out at a temperature below about 120*F.
Claim 10
Dependent Claim 23 words
A process according to claim 1 wherein the composition of Step A is pre-reacted for a period of up to about 2 weeks.

References Cited (Backward Citations)

No citation records indexed.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-10-21 1978-04-22 1978-10-22 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-10-21 1982-04-22 1982-10-22 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-10-21 1986-04-22 1986-10-22 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag