Production of 4-endotricyclo(5,2,1,02,6-endo)decylamine
Abstract
Abstract 1. A PROCESS FOR THE PRODUCTION OF STERICALLY UNIFORM 4-ENDOTRICYCLO(5,2,10**2,6-ENDO)-DECYLAMINE WHICH COMPRISES: ELECTROCHEMICALLY REDUCING A COMPOUND OF THE FORMULA 2-(X-NH-)-PERHYDRO-4,7-METHANOINDENE WHEREIN X IS HYDROGEN, HYDROXY OR -OCOR IN WHICH R IS LOWER ALKYL OF 1 TO 4 CARBON ATOMS, SAID REDUCTION BEING CARRIED OUT IN A LIQUID SOLVENT SELECTED FROM THE GROUP CONSISTING OF AN ORGANIC SOLVENT AND AN AQUEOUS ORGANIC SOLVENT REACTION MEDIUM AT A MERCURY, LEAD OR AMALGAM ELECTRODE AT A CURRENT DENSITY OF ABOUT 1 TO 20 AMPS/DM.2 AT A TEMPERATURE OF FROM -20*C. TO 40*C. AND A PH OF ABOUT 5 OR LESS; AND SEPARATING THE SUBSTANTIALLY STERICALLY UNIFORM AMINE PRODUCT FROM THE REACTION MEDIUM.
Inventors
- 👤 B Giese
- 👤 P Jaeger
- 👤 H Koenig
- 👤 K Brenner
Bibliographic Details
Claims Analysis
Total Claims: 2References Cited (Backward Citations)
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