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US3839205A Expired / Lapsed US ⏱️ 0.0 years remaining

Chromatographic element and method for producing the same

Assignee: Shionogi and Co Ltd
•
Filing: 1972-09-07
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Granted: 1974-10-01
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Expires: 1992-09-07
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Abstract

Abstract A chromatographic element composed of a thin rod of refractory and chemically-stable materials covered with a porous sintered layer of finely divided or powdered glass containing fine particles of a chromatographically-active inorganic adsorbent within the porous structure of powdered glass is made by coating said thin rod with a slurry including said powdered glass and absorbent and baking said coated thin rod at a temperature at which the glass begins to melt until the glass becomes sticky and the particles thereof adhere to one another and to the thin rod support. The element has an excellent chromatographic activity even after repeated adsorptions, intense heatings by means of, for instance a hydrogen flame and regenerations by means of, for example, corrosive reagents. It can be handled easily in the same manner as conventional glass implements.

Inventors

  • 👤 T Okumura
  • 👤 T Kadono

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 03:25
CPC Classifications
G; G01; G01N; G01N30/00; G01N30/90; G01N30/92; G01N30/93; G01N30/02; G01N30/50; G01N30/52; G01N2030/524; G01N2030/528

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 73 words
A CHROMATOGRAPHIC ELEMENT FOR USE IN STICK CHROMATOGRAPHY OR ROD THIN-LAYER CHROMATOGRAPHY WHICH CONSISTS ESSENTIALLY OF A THIN ROD OF REFRACTORY AND CHEMICALLY STABLE MATERIALS AND A POROUS SINTERED LAYER OF FINELY DIVIDED OR POWDERED GLASS CONTAINING FINE PARTICLES OF A CHROMATOGRAPHICALLY ACTIVE INORGANIC ADSORBENT WITHIN THE POROUS STRUCTURE OF POWDERED GLASS, THE PARTICLES OF SAID SINTERED LAYER BEING ADHRED TO ONE ANOTHER, TO THE ADSORBENT PARTICLES AND TO THE THIN ROD SUPPORT.
Claim 2
Dependent Claim 73 words
A CHROMATOGRAPHIC ELEMENT FOR USE IN STICK CHROMATOGRAPHY OR ROD THIN-LAYER CHROMATOGRAPHY WHICH CONSISTS ESSENTIALLY OF A THIN ROD OF REFRACTORY AND CHEMICALLY STABLE MATERIALS AND A POROUS SINTERED LAYER OF FINELY DIVIDED OR POWDERED GLASS CONTAINING FINE PARTICLES OF A CHROMATOGRAPHICALLY ACTIVE INORGANIC ADSORBENT WITHIN THE POROUS STRUCTURE OF POWDERED GLASS, THE PARTICLES OF SAID SINTERED LAYER BEING ADHRED TO ONE ANOTHER, TO THE ADSORBENT PARTICLES AND TO THE THIN ROD SUPPORT.
Claim 3
Dependent Claim 37 words
A chromatographic element is claimed in claim 1, wherein said finely divided or powdered glass is selected from the group consisting of soda-lime glass, borosilicate glass, lead silicate glass, high silicate glass, crystallized glass and mixtures thereof.
Claim 4
Dependent Claim 31 words
A chromatographic element as claimed in claim 1, wherein said adsorbent is selected from the group consisting of silica gel, alumina, diatomaceous earth, magnesium silicate, porous glass powder and mixtures thereof.
Claim 5
Dependent Claim 53 words
A chromatographic element as claimed in claim 1, wherein said thin rod of refractory and chemically-stable materials is a rod or tubular body of a material selected from the group consisting of quartz, high silicate glass, borosilicate glass, ceramic materials, titanium, tantalum, stainless steel, platinum, aluminum, copper, iron and alloys of said metals.

References Cited (Backward Citations)

US3005514A Cited
US3418152A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-09-30 1978-04-01 1978-10-01 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-09-30 1982-04-01 1982-10-01 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-09-30 1986-04-01 1986-10-01 $7700.00 Window Closed / Lapsed

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