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US3795451A Expired / Lapsed US ⏱️ 0.0 years remaining

Rotor for fast analyzer of rotary cuvette type

Assignee: United States Atomic Energy Commission
•
Filing: 1973-04-24
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Granted: 1974-03-05
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Expires: 1993-04-24
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Abstract

Abstract An improved rotor characterized by efficient premixing of sample and reactant liquids prior to their being discharged into a sample analysis cuvette is provided. Inner and outer concentric circular arrays of static loading cavities are disposed within the rotor on a one-to-one basis centripetal to an array of sample analysis cuvettes. The centrifugal walls of cavities in the inner array of loading cavities each slope downwardly and outwardly to a capillary-sized passage having a bubble trap. Liquid communication is provided by the capillary-sized passages between those cavities and respective cavities in the outer array of loading cavities upon rotation of the rotor while intercontact of the liquids in the respective cavities is prevented under static loading conditions. The centrifugal walls of cavities in the outer array of loading cavities each slope upwardly and outwardly to a cuvette loading passageway at an angle approaching the vertical in order to retain liquids in those cavities at preselected low rotor rotational speeds sufficient to cause liquid to flow through the capillary-sized passage and to discharge liquids through the cuvette loading passageways at preselected higher speeds.

Inventors

  • 👤 J Mailen

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 13:41
CPC Classifications
B; B04; B04B; B04B5/00; B04B5/04; B04B5/0407; B01; B01F; B01F25/00; B01F25/10; B01F25/104; B01F35/00; B01F35/71; B01F35/717; B01F35/71725; G; G01; G01N; G01N21/00; G01N21/01; G01N21/03; G01N21/07; B01F33/00; B01F33/30

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 240 words
An improved rotor for a fast analyzer of the rotary cuvette type characterized by efficient premixing of sample and reactant liquids prior to their being discharged into sample analysis cuvettes for photometric analysis, the improved rotor comprising a generally disk-shaped member defining: a. a circular array of sample analysis cuvettes for accepting mixtures of liquid samples and reactants, said disk-shaped member having transparent walls above and below said sample analysis cuvettes; b. an inner array of static loading cavities equal in number and disposed centripetal to said sample analysis cuvettes, the centrifugal walls of said cavities in said inner array of cavities extending downwardly and outwardly; c. an outer array of static loading cavities equal in number and disposed radially intermediate said sample analysis cuvettes and said cavities in said inner array of static loading cavities, the centrifugal walls of said cavities in said outer array of cavities extending upwardly and outwardly with a steep inclination selected to retain liquids in said cavities at preselected low rotor rotational speeds; d. capillary-sized passages extending between respective cavities in said inner and outer arrays of cavities, said passages being sized to prevent flow between said cavities under static conditions while permitting flow from cavities in said inner array of cavities to cavities in said outer array of cavities at preselected low rotational speeds; and e. connecting passages extending between respective cavities in said outer array of cavities and said sample analysis cuvettes.
Claim 2
Dependent Claim 240 words
An improved rotor for a fast analyzer of the rotary cuvette type characterized by efficient premixing of sample and reactant liquids prior to their being discharged into sample analysis cuvettes for photometric analysis, the improved rotor comprising a generally disk-shaped member defining: a. a circular array of sample analysis cuvettes for accepting mixtures of liquid samples and reactants, said disk-shaped member having transparent walls above and below said sample analysis cuvettes; b. an inner array of static loading cavities equal in number and disposed centripetal to said sample analysis cuvettes, the centrifugal walls of said cavities in said inner array of cavities extending downwardly and outwardly; c. an outer array of static loading cavities equal in number and disposed radially intermediate said sample analysis cuvettes and said cavities in said inner array of static loading cavities, the centrifugal walls of said cavities in said outer array of cavities extending upwardly and outwardly with a steep inclination selected to retain liquids in said cavities at preselected low rotor rotational speeds; d. capillary-sized passages extending between respective cavities in said inner and outer arrays of cavities, said passages being sized to prevent flow between said cavities under static conditions while permitting flow from cavities in said inner array of cavities to cavities in said outer array of cavities at preselected low rotational speeds; and e. connecting passages extending between respective cavities in said outer array of cavities and said sample analysis cuvettes.
Claim 3
Dependent Claim 21 words
The improved rotor of claim 1 further including a bubble trap disposed intermediate the ends of each of said capillary-sized passages.
Claim 4
Dependent Claim 37 words
The improved rotor of claim 1 wherein cavities in said outer array of loading cavities are generally round in horizontal cross section and wherein said capillary-sized passages intersect said cavities in said outer array of cavities tangentially.
Claim 5
Dependent Claim 27 words
The improved rotor of claim 3 wherein said sample analysis cuvettes are generally round in horizontal cross section and wherein said connecting passages intersect said cuvettes tangentially.
Claim 6
Dependent Claim 27 words
The improved rotor of claim 1 wherein said capillary-sized passages extend between the lower ends of respective cavities in said inner and outer arrays of loading cavities.
Claim 7
Dependent Claim 24 words
The improved rotor of claim 5 wherein said capillary-sized passages intersect with the centrifugal walls of said cavities in said inner array of cavities.
Claim 8
Dependent Claim 29 words
The improved rotor of claim 1 wherein said connecting passages extend between the upper ends of respective cavities in said outer array of cavities and said sample analysis cuvettes.
Claim 9
Dependent Claim 24 words
The improved rotor of claim 7 wherein said connecting passages intersect with the centrifugal walls of said cavities in said outer array of cavities.

References Cited (Backward Citations)

US3555284A Cited
US3547547A Cited
US3669551A Cited
US3744974A Cited
US3744975A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-03-04 1977-09-03 1978-03-05 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-03-04 1981-09-03 1982-03-05 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-03-04 1985-09-03 1986-03-05 $7700.00 Window Closed / Lapsed

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