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US3793408A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for the purification of bis (2-ethyl-hexyl) phosphoric acid

Assignee: United States Atomic Energy Commission
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Filing: 1972-01-28
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Granted: 1974-02-19
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Expires: 1992-01-28
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Abstract

Abstract FOREIGN PRODUCTS INCLUDING THE NEUTRAL ORGANOPHOSPHOROUS COMPOUNDS AND THE IRON SALTS NORMALLY PRESENT IN COMMERICAL BIS(2-ETHYL-HEXYL)PHOSPHORIC ACID (HDEHP), AND THE RADIOLYTIC DEGRADATION PRODUCTS OF HDEHP ON EXPOSURE HDEHP TO BETA AND GAMMA IRADIATION ARE REMOVED FRO HDEHP CONTAINING ONE OR MOR OF SUCH PRODUCTS BY CONTACTING THE SAID FOREIGN PRODUCT SCONTAINING HDEHP WITH A MACRORETICULAR ANION EXCHANGE RESIN IN BASE FORM WHEREBY THE DEHP- ION OF HDEHP EXCHANGES WITH THE ANION OF THE RESIN AND IS THUS ADSORBED ON THE RESIN AND THE SAID FOREIGN PRODUCTS ARE NOT ADSORBED AND WILL PASS THROUGH A BED OF PARTICLES OF THE RESIN. THE ADSORBED DEHP- ION IS THEN ELUTED FROM THE RESIN AND ACIDIFIED TO FORM AND RECOVER THE PURIFIED HDEHP.

Inventors

  • 👤 W Schulz

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 23:02
CPC Classifications
C; C07; C07F; C07F9/00; C07F9/02; C07F9/025; B; B01; B01J; B01J41/00; B01J41/04; B01J41/07; C07F9/06; C07F9/08; C07F9/09; C07F9/11

Claims Analysis

Total Claims: 0
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References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-02-18 1977-08-20 1978-02-19 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-02-18 1981-08-20 1982-02-19 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-02-18 1985-08-20 1986-02-19 $7700.00 Window Closed / Lapsed

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