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Method for determining thermo-physical properties of specimens

Assignee: National Aeronautics and Space Administration
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Filing: 1972-08-18
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Granted: 1974-02-05
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Expires: 1992-08-18
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Abstract

Abstract The square root of the product of thermophysical properties Rho , c and k, where Rho is density, c is specific heat and k is thermal conductivity, is determined directly on a test specimen such as a wind tunnel model. The test specimen and a reference specimen of known specific heat are positioned a given distance from a heat source. The specimens are provided with a coating, such as a phase change coating, to visually indicate that a given temperature has been reached as well as to ensure that both specimens have the same absorbtivity and thus receive the same heat rate. A shutter interposed between the heat source and the specimens is opened and a motion picture camera is actuated to provide a time record of the heating step. The temperature of the reference specimen is recorded as a function of time. The heat rate to which both the test and reference specimens have been subjected is determined from the temperature time response of the reference specimen by the conventional thin-skin calorimeter equation. This heat rate is then used to determine square root Rho ck of the test specimen from the transient one dimensional heat conduction equation for a semi-infinite solid subjected to a step heat input at a constant heat rate. A model, such as a wind tunnel model, can be tested directly thus eliminating the costly and inaccurate method of making test models solely for the purpose of determining square root Rho ck.

Inventors

  • 👤 R Jones

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 23:47
CPC Classifications
G; G01; G01N; G01N25/00; G01N25/18

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 183 words
A method of determining the value of the square root of the product of thermophysical properties square root Rho ck of a material comprising the steps of: providing a test specimen of a material to be tested; providing a reference specimen of a material having a known specific heat, thickness and density; subjecting a surface of the test and reference specimens of known initial temperature simultaneously to a heat source located a given distance from the test and reference specimens, said surfaces having the same absorptivity such that the test and reference specimens are subjected to the same heat rate; determining the time required to heat the reference specimen to a given temperature; determining the time required to heat the test specimen to said given temperature; measuring the temperature of said reference specimen as a function of time to determine the rate of change of temperature thereof with time; determining the heat rate to which the test and reference specimens were subjected; and determining from said heat rate the value of the product of thermophysical properties square root Rho ck for said specimen.
Claim 2
Independent Claim 183 words
A method of determining the value of the square root of the product of thermophysical properties square root Rho ck of a material comprising the steps of: providing a test specimen of a material to be tested; providing a reference specimen of a material having a known specific heat, thickness and density; subjecting a surface of the test and reference specimens of known initial temperature simultaneously to a heat source located a given distance from the test and reference specimens, said surfaces having the same absorptivity such that the test and reference specimens are subjected to the same heat rate; determining the time required to heat the reference specimen to a given temperature; determining the time required to heat the test specimen to said given temperature; measuring the temperature of said reference specimen as a function of time to determine the rate of change of temperature thereof with time; determining the heat rate to which the test and reference specimens were subjected; and determining from said heat rate the value of the product of thermophysical properties square root Rho ck for said specimen.
Claim 3
Dependent Claim 27 words
A method according to claim 1 wherein the test and reference specimens are each provided with means for visually indicating that said given temperature has been reached.
Claim 4
Dependent Claim 26 words
A method according to claim 2 wherein the time required to heat the reference and test specimens to said given temperature is determined by visual observation.
Claim 5
Dependent Claim 41 words
A method according to claim 2 wherein the time required to heat the reference and test specimens to said given temperature is determined by providing a motion picture record of the heating step and by analysis of the developed photographic record.
Claim 6
Dependent Claim 16 words
A method according to claim 2 wherein said visual indicating means comprises a phase change coating.
Claim 7
Dependent Claim 56 words
A method according to claim 1 wherein said heat rate is determined from the equation: Q Rho c l dT/dt wherein Q heat rate, Rho density of the reference specimen, c specific heat of the reference specimen, l thickness of the reference specimen; and dT/dt rate of change of temperature of the reference specimen with time.
Claim 8
Dependent Claim 64 words
A method according to claim 1 wherein the value of Square Root Rho ck is determined from the following equation: Square Root Rho ck Q/Tg - Ti . (2/ Square Root pi ) . Square Root t where Q the heat rate Tg the given temperature Ti the initial temperature of the specimens, t time required for test specimen to reach the given temperature.
Claim 9
Dependent Claim 15 words
A method according to claim 1 wherein said heat source comprises a radient heat source.
Claim 10
Dependent Claim 37 words
A method according to claim 1 wherein the temperature of said heat source is sufficiently higher than said given temperature that the change in temperature of the specimens has a negligible effect on the imposed heat rate.

References Cited (Backward Citations)

US3114836A Cited
US3165915A Cited
US3279239A Cited
US3433052A Cited
US3566669A Cited
US3570302A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-02-04 1977-08-06 1978-02-05 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-02-04 1981-08-06 1982-02-05 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-02-04 1985-08-06 1986-02-05 $7700.00 Window Closed / Lapsed

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