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Method for treating reverse osmosis membranes

Assignee: Eastman Technology Inc
•
Filing: 1971-06-14
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Granted: 1973-11-13
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Expires: 1991-06-14
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Abstract

Abstract A single phase temperature independent imbibing solution for cellulose ester or ether reverse osmosis membranes consists essentially of (a) 30-60 percent grycerin; (b) 25-55 percent water; (c) 3-10 percent nonionic first surface active agent such as a polythylene glycol ether of C11-C15 linear alcohol; and (d) 0.1-5 percent of a second surface active agent which is either anionic (eg. the dioctyl ester of sodium sulfosuccinic acid, or the sodium sulfate derivative of 7 ethyl-2 methyl -4-undecanol), or cationic (eg. C8-C18 alkyl dimethyl benzyl ammonium chloride). In the method, a cellulose ester or ether reverse osmosis membrane in a water-wet condition is immersed in the novel imbibing solution, and then is removed and dried under ambient conditions, or by exposing it to heated air.

Inventors

  • 👤 B Brown
  • 👤 E Ray

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 12:46
CPC Classifications
B; B01; B01D; B01D67/00; B01D67/0081; B01D67/0095

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 24 words
In a method in accordance with claim 1, said imbibing solution wherein said anionic surface active agent is dioctyl ester of sodium sulfosuccinic acid.
Claim 2
Dependent Claim 23 words
In a method in accordance with claim 1, said imbibing solution wherein said anionic surface active agent is sodium sulfate derivative of 7-ethyl-2-methyl-4-undecanol.
Claim 3
Dependent Claim 239 words
In a method for treating a cellulose ester or ether reverse osmosis membrane comprising immersing such a membrane in a water-wet condition in an imbibing solution, and then removing and drying said membrane, the improvement wherein said imbibing solution is a single phase temperature independent imbibing solution which remains homogeneous at imbibing temperatures without coacervation and without causing substantial loss of desalination parameters by said membrane, said solution consisting essentially of: about 30 to 60 percent of glycerin; about 25 to 55 percent of water; about 3 to 10 percent of a nonionic first surface active agent; and about 0.1 to 5 percent of a second surface active agent selected from the group consisting of anionic and cationic surface active agents, all percentages being by weight, said nonionic surface active agent being (a) a product formed by condensing one or more alkylene oxides of two to four carbon atoms alone or with other alkylene oxides with a relatively hydrophobic compound selected from a fatty alcohol, fatty acid, sterol, fatty glyceride, fatty amide, fatty mercaptan or tall oil fatty acids, or (b) a product formed by condensing one or more lower alkyl alcohol amines with a fatty acid; said anionic surface active agent being selected from sulfates and sulfonated alkyl, aryl, alkyl-aryl hydrocarbons and alkali-metal salts thereof; and said cationic surface active agent being an alkyl dimethyl benzyl ammonium chloride wherein said alkyl group has eight to 18 carbon atoms.
Claim 4
Dependent Claim 40 words
In a method in accordance with claim 4, an imbibing solution wherein said second surface active agent is an alkyl dimethyl benzyl ammonium chloride wherein said alkyl group has 8 to 18 carbon atoms, as a cationic surface active agent.
Claim 5
Dependent Claim 31 words
In a method in accordance with claim 4, an imbibing solution wherein said second surface active agent is the dioctyl ester of sodium sulfosuccinic acid, as an anionic surface active agent.
Claim 6
Dependent Claim 32 words
In a method in accordance with claim 4, an imbibing solution wherein said second surface active agent is the sodium sulfate derivative of 7 ethyl-2 methyl-4-undecanol, as an anionic surface active agent.
Claim 7
Dependent Claim 78 words
In a method in accordance with claim 4, an imbibing solution wherein said nonionic surface active agent is a polyethylene glycol ether of C11-C15 linear alcohol; wherein said anionic surface active agent is selected from the group consisting of the dioctyl ester of sodium sulfosuccinic acid and the sodium sulfate derivative of 7 ethyl-2 methyl-4-undecanol; and said cationic surface active agent is an alkyl dimethyl benzyl ammonium chloride wherein said alkyl group has eight to 18 carbon atoms.

References Cited (Backward Citations)

US3567809A Cited
US3646179A Cited
US3592672A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-11-12 1977-05-14 1977-11-13 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-11-12 1981-05-14 1981-11-13 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-11-12 1985-05-14 1985-11-13 $7700.00 Window Closed / Lapsed

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