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US3755158A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for capturing metal ions

Assignee: Ajinomoto Co Inc
•
Filing: 1971-08-04
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Granted: 1973-08-28
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Expires: 1991-08-04
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Abstract

Abstract Cations of metals other than the alkali metals may be precipitated practically completely from their aqueous solutions at a pH of 4 or higher by N-acylamino acids whose acyl group is alkanoyl or alkenoyl having seven to 25 carbon atoms, the acylamino group being connected with the carboxyl group by divalent alkylene having one to five carbon atoms. The voluminous precipitates include even more of the metal ions originally present and settle faster in the presence of small amounts of polyhydric alcohols, polyethers, alkali metal silicates, or alkali metal borates. Water polluted with heavy metals can be made potable by this method.

Inventors

  • 👤 S Inazuka
  • 👤 M Takehara
  • 👤 R Yoshida

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 21:36
CPC Classifications
C; C02; C02F; C02F1/00; C02F1/52; C02F1/54; C02F1/5236; C02F1/5272

Claims Analysis

Total Claims: 13
Claim 1
Independent Claim 20 words
A method as set forth in claim 1, wherein said amount is 0.01 to 10 stoichiometric equivalents of said cations.
Claim 2
Dependent Claim 17 words
the acyl radical of said N-acylamino acid being alkanoyl or alkenoyl having 7 to 25 carbon atom,
Claim 3
Dependent Claim 35 words
the acylamino group of said N-acylamino acid being connected with a carboxyl group of said N-acylamino acid by divalent alkylene having one to five carbon atoms; and b. separating the precipitated cations from said medium.
Claim 4
Dependent Claim 20 words
A method as set forth in claim 1, wherein said amount is 1.0 to 4.0 stoichiometric equivalents of said cations.
Claim 5
Dependent Claim 19 words
A method as set forth in claim 3, wherein said alkanoyl or alkenoyl has 11 to 21 carbon atoms.
Claim 6
Dependent Claim 85 words
A method as set forth in claim 1, wherein an amount of at least one capturing assistant effective for enhancing the settling velocity of the precipitated cations in said medium and for reducing the concentration of residual cations in said medium after said precipitating is dispersed in said medium, said capturing assistant being an organic compound having two or more alcoholic hydroxyl groups, an organic compound having a polyoxyethylene radical including more than two ether linkages, an alkali metal silicate, or an alkali metal borate.
Claim 7
Dependent Claim 29 words
A method as set forth in claim 5, wherein the amount of said capturing assistant is between 10 7 and 10 percent of the weight of said N-acylamino acid.
Claim 8
Dependent Claim 26 words
A method as set forth in claim 6, wherein the amount of said capturing assistant is between 10 5 and 10 1 percent of said weight.
Claim 9
Dependent Claim 16 words
A method as set forth in claim 6, wherein said capturing assistant is a polyhydric alcohol.
Claim 10
Dependent Claim 15 words
A method as set forth in claim 6, wherein said capturing assistant is a saccharide.
Claim 11
Dependent Claim 16 words
A method as set forth in claim 6, wherein said capturing assistant is a polyalkylene glycol.
Claim 12
Dependent Claim 21 words
A method as set forth in claim 6, wherein said capturing assistant is an alkali metal silicate or alkali metal borate.
Claim 13
Dependent Claim 21 words
A method as set forth in claim 1, wherein the pH of said medium is lower than 8 after said dissolving.

References Cited (Backward Citations)

US3041374A Cited
US3337555A Cited
US3412180A Cited
US3437451A Cited
US3467684A Cited
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US3634230A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-08-27 1977-02-26 1977-08-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-08-27 1981-02-26 1981-08-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-08-27 1985-02-26 1985-08-28 $7700.00 Window Closed / Lapsed

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