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US3754990A Expired / Lapsed US ⏱️ 0.0 years remaining

Cleaning of ferrous metal surfaces

Assignee: Dow Chemical Co
•
Filing: 1971-02-22
•
Granted: 1973-08-28
•
Expires: 1991-02-22
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Abstract

Abstract The invention is based on the discovery that upon adding a polyamine having intralinear amino groups to an aqueous alkaline solution of an ammoniated or aminated polycarboxylic acid chelating agent, a new and improved metal cleaning solution is provided. Upon bringing such cleaning solution into contact with a ferrous metal surface having hardness and/or iron oxide scale, and copper, thereon and the solution being maintained at a temperature above about 155*C. for a time sufficient to dissolve all the hardness and iron oxides, the copper is dissolved and neither precipitates from solution nor deposits on the ferrous metal surface.

Inventors

  • 👤 F Teumac
  • 👤 J Scruggs

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 21:41
CPC Classifications
C; C11; C11D; C11D3/00; C11D3/16; C11D3/26; C11D3/33; C11D3/37; C11D3/3703; C11D3/3723; C11D7/00; C11D7/22; C11D7/32; C11D7/3209; C11D7/3245; C23; C23G; C23G1/00; C23G1/14; C23G1/19; C11D2111/00; C11D2111/10; C11D2111/14; C11D2111/16

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 47 words
The improvement as in claim 1 in which the aqueous cleaning solution is initially heated to a temperature in the range of above about 155* and up to 190*C, and then the temperature is reduced to about 110* to 150*C for the balance of the cleaning period.
Claim 2
Dependent Claim 67 words
The improvement as in claim 1 in which the cleaning solution contains from 0.1 to 5 per cent by weight of polyalkylenepolyamine, the cleaning solution is activated by heating to a temperature in the range of above about 155* and up to 190*C and thereafter the cleaning solution is maintained in contact with the ferrous metal surface at a temperature in the range of 110* to 150*C.
Claim 3
Dependent Claim 35 words
The improvement as in claim 1 in which the total amount of polyalkylenepolyamine added to the aqueous solution is about 2.8 parts by weight per part of copper impurity present in the system being cleaned.

References Cited (Backward Citations)

US2396938A Cited
GB821094A Cited
US2959555A Cited
US3003970A Cited
US3251778A Cited
US3262791A Cited
US3067070A Cited
US3308065A Cited
US3440170A Cited
US3438901A Cited
US3490741A Cited
US3447965A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-08-27 1977-02-26 1977-08-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-08-27 1981-02-26 1981-08-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-08-27 1985-02-26 1985-08-28 $7700.00 Window Closed / Lapsed

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