Patent US2191361A successfully refreshed from Google Patents.
Patent US3723594A successfully refreshed from Google Patents.
US3723594A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Rare earth removal from americium oxide
Assignee: United States Atomic Energy Commission
•
Filing: 1972-05-18
•
Granted: 1973-03-27
•
Expires: 1992-05-18
Abstract
Abstract Americium oxide materials having rare earths as impurities may have these removed by oxidizing the americium to the hexavalent state, precipitating and removing rare earth values using hydrofluoric acid, reducing the americium to the trivalent state, thereafter precipitating and removing americium oxalate using oxalic acid, and calcining the americium oxalate to americium oxide.
Inventors
- 👤 S Proctor
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-06 14:02
CPC Classifications
C; C01; C01G; C01G56/00; C01G56/007; C01G56/009
Claims Analysis
Total Claims: 2
Claim 1
Independent Claim
17 words
The method of claim 1 including recycling said fourth solution filtrate through the method of claim 1.
Claim 2
Dependent Claim
115 words
The method of claim 1 including recovering trapped americium in the rare earth precipitates comprising the further steps of dissolving said rare earth precipitates containing said trapped americium in nitric acid, adding sufficient oxalic acid to the solution containing said dissolved rare earth precipitates and said americium to thereby effect reaction with said oxalic acid and form americium oxalate, filtering to remove said americium oxalate, washing said americium oxalate with water, heating said americium oxalate to about 600* C for about 4 hours calcining said americium oxalate to americium oxide, and thereafter reprocessing said calcined americium oxide through the recited the process steps of the method of claim 1 in one or more additional stages.
References Cited (Backward Citations)
US3551119A
Cited
US3554867A
Cited
US2577097A
Cited
US2681923A
Cited
US3445201A
Cited
US3463619A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1976-03-26 | 1976-09-25 | 1977-03-27 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1980-03-26 | 1980-09-25 | 1981-03-27 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1984-03-26 | 1984-09-25 | 1985-03-27 | $7700.00 | Window Closed / Lapsed |