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US3723594A Expired / Lapsed US ⏱️ 0.0 years remaining

Rare earth removal from americium oxide

Assignee: United States Atomic Energy Commission
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Filing: 1972-05-18
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Granted: 1973-03-27
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Expires: 1992-05-18
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Abstract

Abstract Americium oxide materials having rare earths as impurities may have these removed by oxidizing the americium to the hexavalent state, precipitating and removing rare earth values using hydrofluoric acid, reducing the americium to the trivalent state, thereafter precipitating and removing americium oxalate using oxalic acid, and calcining the americium oxalate to americium oxide.

Inventors

  • 👤 S Proctor

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 14:02
CPC Classifications
C; C01; C01G; C01G56/00; C01G56/007; C01G56/009

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 17 words
The method of claim 1 including recycling said fourth solution filtrate through the method of claim 1.
Claim 2
Dependent Claim 115 words
The method of claim 1 including recovering trapped americium in the rare earth precipitates comprising the further steps of dissolving said rare earth precipitates containing said trapped americium in nitric acid, adding sufficient oxalic acid to the solution containing said dissolved rare earth precipitates and said americium to thereby effect reaction with said oxalic acid and form americium oxalate, filtering to remove said americium oxalate, washing said americium oxalate with water, heating said americium oxalate to about 600* C for about 4 hours calcining said americium oxalate to americium oxide, and thereafter reprocessing said calcined americium oxide through the recited the process steps of the method of claim 1 in one or more additional stages.

References Cited (Backward Citations)

US3551119A Cited
US3554867A Cited
US2577097A Cited
US2681923A Cited
US3445201A Cited
US3463619A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-03-26 1976-09-25 1977-03-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-03-26 1980-09-25 1981-03-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-03-26 1984-09-25 1985-03-27 $7700.00 Window Closed / Lapsed

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