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US3720041A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for drying methyl chloride in a polymer plant

Assignee: Individual
•
Filing: 1971-12-08
•
Granted: 1973-03-13
•
Expires: 1991-12-08
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Abstract

Abstract A process for drying methyl chloride in a butyl rubber process using glycol is improved by presaturating the glycol with liquid methyl chloride thereby avoiding temperature increases during presaturation. Need for a glycol-methyl chloride cooler is thereby eliminated. Since the absorber operates at a lower temperature, drying of the methyl chloride stream is more complete.

Inventors

  • 👤 E Upchurch
  • 👤 J Alvarez

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 20:34
CPC Classifications
B; B01; B01D; B01D53/00; B01D53/26; C; C08; C08F; C08F10/00

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 78 words
In a process for preparing butyl rubber, wherein the diluent stream is fried by contacting said diluent stream with a glycol in an absorption tower, the improvement which comprises: a. presaturating the glycol stream with liquid methyl chloride; b. storing the presaturated glycol in a presaturation vessel; and c. maintaining a constant pressure differential between the absorption tower and the presaturation vessel, said prEsaturation vessel being at about 1 to about 10 psi higher than said absorption tower.
Claim 2
Dependent Claim 78 words
In a process for preparing butyl rubber, wherein the diluent stream is fried by contacting said diluent stream with a glycol in an absorption tower, the improvement which comprises: a. presaturating the glycol stream with liquid methyl chloride; b. storing the presaturated glycol in a presaturation vessel; and c. maintaining a constant pressure differential between the absorption tower and the presaturation vessel, said prEsaturation vessel being at about 1 to about 10 psi higher than said absorption tower.
Claim 3
Dependent Claim 17 words
The process of claim 1 wherein the absorption tower pressure is about 25 to about 75 psig.
Claim 4
Dependent Claim 23 words
The process of claim 1 wherein the pressure differential between the absorption tower and presaturation vessel is about 2 to about 6 psi.
Claim 5
Dependent Claim 13 words
The process of claim 3 wherein the pressure differential is about 5 psi.
Claim 6
Dependent Claim 16 words
The process of claim 1 wherein the glycol is triethylene glycol, diethylene glycol or ethylene glycol.
Claim 7
Dependent Claim 11 words
The process of claim 5 wherein the glycol is triethylene glycol.
Claim 8
Dependent Claim 20 words
The process of claim 1 wherein the glycol stream comprises about 10 to about 30 wt. percent of an alkanolamine.

References Cited (Backward Citations)

US3005808A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-03-12 1976-09-11 1977-03-13 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-03-12 1980-09-11 1981-03-13 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-03-12 1984-09-11 1985-03-13 $7700.00 Window Closed / Lapsed

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