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US3719329A Expired / Lapsed US ⏱️ 0.0 years remaining

Ultradisintegration and agglomeration of minerals such as mica, products therefrom and apparatus therefor

Assignee: Individual
•
Filing: 1970-08-05
•
Granted: 1973-03-06
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Expires: 1990-08-05
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Abstract

Abstract Frangible or cleavable solids, such as mica, are disintegrated in oriented, high-velocity streams of a fluid medium so as to produce thin smooth-surfaced particles or flakes having a high specific surface area and a high ratio of length to thickness. The resulting particles or flakes are useful as agglomerants, fillers or pigments or can be agglomerated to form paper-like webs or solid discs or articles of other predetermined configurations, with or without added binder, either in selfsupporting form or adhered to a substrate. Various methods and apparatus for such disintegration are disclosed.

Inventors

  • 👤 J Ruzicka

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 18:58
CPC Classifications
B; B02; B02C; B02C19/00; B02C19/06; B28; B28D; B28D1/00; B28D1/32; B28D1/322

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 156 words
A process for disintegrating mica into thin particles which comprises: heating insufficiently fine pieces of mica to a temperature at which its water of hydration is released; injecting a hot gaseous medium as a multiplicity of swirling, non-radial, converging, flat, high velocity streams from a multiplicity of slit-shaped orifices into a lower portion of an upwardly extending disintegration zone of substantially circular cross section, said multiplicity of orifices being distributed in said disintegratiOn zone in part around its periphery to converge non-radially inward and in part around its central axis to converge non-radially outward, and exposing said mica pieces to said swirling gas streams in said lower portion at an operating temperature at which the water of hydration of said mica is released until said pieces become split into particles of different sizes and relatively fine particles having the desired fineness escape from said disintegration zone while relatively coarse particles remain therein to be split further.
Claim 2
Dependent Claim 156 words
A process for disintegrating mica into thin particles which comprises: heating insufficiently fine pieces of mica to a temperature at which its water of hydration is released; injecting a hot gaseous medium as a multiplicity of swirling, non-radial, converging, flat, high velocity streams from a multiplicity of slit-shaped orifices into a lower portion of an upwardly extending disintegration zone of substantially circular cross section, said multiplicity of orifices being distributed in said disintegratiOn zone in part around its periphery to converge non-radially inward and in part around its central axis to converge non-radially outward, and exposing said mica pieces to said swirling gas streams in said lower portion at an operating temperature at which the water of hydration of said mica is released until said pieces become split into particles of different sizes and relatively fine particles having the desired fineness escape from said disintegration zone while relatively coarse particles remain therein to be split further.
Claim 3
Dependent Claim 49 words
A process according to claim 1 wherein pieces of relatively coarse mica feed are introduced into the lower portion of said disintegration zone in the vicinity of its main vertical axis and wherein product particles of desired fineness are withdrawn from an upper peripheral portion of said disintegration zone.
Claim 4
Dependent Claim 40 words
A process according to claim 1 wherein pieces of insufficiently fine mica are introduced into said disintegration zone in a non-central portion thereof and product particles of desired fineness are withdrawn from a central portion in a lower part thereof.
Claim 5
Independent Claim 152 words
An apparatus for disintegrating solids suspended in a fluid medium which comprises: an upwardly extending shell of generally circular cross section providing a disintegration chamber in the lower portion thereof and an elutriation chamber thereabove; a first plurality of high velocity nozzle means having substantially vertically elongated orifices disposed within said disintegration chamber around its periphery and oriented for jetting non-radially converging streams of fluid medium in a generally inward direction into said disintegration chamber; a second plurality of nozzle means having substantially vertically elongated orifices disposed within said disintegration chamber around its main vertical axis and oriented for jetting non-radially converging streams of fluid medium in a generally outward direction into said disintegration chamber; means for feeding fluid medium to said nozzle means; means for introducing insufficiently fine pieces of frangible mineral into said disintegration chamber; and means for removing fine product particles from an upper portion of said elutriation chamber.
Claim 6
Independent Claim 152 words
An apparatus for disintegrating solids suspended in a fluid medium which comprises: an upwardly extending shell of generally circular cross section providing a disintegration chamber in the lower portion thereof and an elutriation chamber thereabove; a first plurality of high velocity nozzle means having substantially vertically elongated orifices disposed within said disintegration chamber around its periphery and oriented for jetting non-radially converging streams of fluid medium in a generally inward direction into said disintegration chamber; a second plurality of nozzle means having substantially vertically elongated orifices disposed within said disintegration chamber around its main vertical axis and oriented for jetting non-radially converging streams of fluid medium in a generally outward direction into said disintegration chamber; means for feeding fluid medium to said nozzle means; means for introducing insufficiently fine pieces of frangible mineral into said disintegration chamber; and means for removing fine product particles from an upper portion of said elutriation chamber.
Claim 7
Dependent Claim 30 words
An apparatus according to claim 4 wherein said mineral introducing means comprises a means for introducing a preselected gas thereinto so as to minimize entry of the surrounding atmosphere thereinto.
Claim 8
Dependent Claim 35 words
An apparatus according to claim 5 wherein said shell has the shape of an inverted truncated cone and wherein the means for removing fine product particles therefrom is located in an upper peripheral portion thereof.
Claim 9
Dependent Claim 22 words
An apparatus according to claim 4 which further comprises a high frequency vibrating means to create high frequency vibrations within said shell.
Claim 10
Dependent Claim 22 words
A process according to claim 1 wherein said gas is an inert gas and said operating temperature is above about 800* C.

References Cited (Backward Citations)

US2032827A Cited
US2325080A Cited
US2590220A Cited
US2588945A Cited
US2612889A Cited
US2704635A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1976-03-05 1976-09-04 1977-03-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1980-03-05 1980-09-04 1981-03-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1984-03-05 1984-09-04 1985-03-06 $7700.00 Window Closed / Lapsed

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