Synthesis of aluminum hydride and tertiary amine adducts thereof
Abstract
Abstract A PROCESS IS PROVIDED FOR THE STEPWISE PREPARATION OF ALUMINUM HYDRIDE AND ITS TERTIARY AMINE ADDUCTS BY (1) SYNTHESIZING THE TRIMETHYLAMINE-ALANE ADDUCT FROM ALUMINUM, HYDROGEN AND TRIMETHYLAMINE IN THE PRESENCE OF A GROUP I-A OR GROUP II-A METAL CATALYST, (2) TRANSAMINATING THE TRIMETHYLAMINE-ALANE ADDUCT WITH ANOTHER TERTIARY AMINE TO FORM ANOTHER TERTRIARY AMINE-ALANE ADDUCT, AND (3) THERMALLY DECOMPOSING THE TERTIARY AMINE-ALANE ADDUCT IN THE PRESENCE OF A GROUP I-A OR GROUP II-A METAL HYDRIDE OR ORGANOMETALLIC COMPOUND CATALYST TO FORM ALANE AND THE TERTIARY AMINE. A PROCESS IS ALSO PROVIDED FOR SYNTHESIZING RELATIVELY STABLE TERTIARY AMINE-ALANE ADDUCTS FROM ALUMINUM, HYDROGEN AND THE CORRESPONDING TERTIARY AMINE IN THE PRESENCE OF A GROUP I-A OR GROUP II-A METAL CATALYST.
Inventors
- 👤 Jawad H Murib
- 👤 David Horvitz
Bibliographic Details
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