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US3634591A Expired / Lapsed US ⏱️ 0.0 years remaining

Furnace assembly for thermal analysis use

Assignee: Dow Chemical Co
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Filing: 1969-07-09
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Granted: 1972-01-11
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Expires: 1989-07-09
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Abstract

Abstract This invention relates to a heating furnace assembly which is adapted to be coupled to and become a part of a mass spectrometer adjacent to the ion source (usually) within the instrument. The furnace is a radiant heating device utilizing a helical coil and reflective surface and is adapted to be controlled by means of temperature sensing means disposed within a separate thermal analysis cell which is adapted to be disposed within the furnace.

Inventors

  • 👤 Horst G Langer

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 08:49
CPC Classifications
F; F27; F27D; F27D11/00; F27D11/02; H; H01; H01J; H01J49/00; H01J49/02; H01J49/10; H01J49/14

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 248 words
A furnace and sample insertion assembly for use under highvacuum conditions, comprising tubular means, an annular element having a central bore and which is at least as large as the inner diameter of said tubular means, said annular element being disposed perpendicularly with respect to the longitudinal axis of said tubular means and secured thereto, an array of rodlike support elements disposed perpendicularly with respect to said annular element and secured adjacent to the outer periphery of said annular element, a disc, said disc being disposed above said annular element and coupled to said support elements, a heater winding, said heater winding being disposed around said support elements between said annular element and said disc, a hollow cylindrically shaped heat reflector, said heat reflector surrounding said support elements between said annular element and said disc, a tubular element, the longitudinal axis of said tubular element being aligned perpendicularly with respect to a flanged mounting plate, said flanged plate extending transversely from said tubular element intermediate the ends thereof, said flanged plate being hermetically sealed to said tubular element, said tubular element having a valve therein on the side of said flanged plate remote from said heater winding, said tubular element having an inner diameter which is slightly larger than the diameter of a thermal analysis cell assembly adapted to be inserted therethrough and into the space within said heater winding, means for sealing said tubular element to said cell assembly, and lead means for energizing said heater winding.
Claim 2
Dependent Claim 248 words
A furnace and sample insertion assembly for use under highvacuum conditions, comprising tubular means, an annular element having a central bore and which is at least as large as the inner diameter of said tubular means, said annular element being disposed perpendicularly with respect to the longitudinal axis of said tubular means and secured thereto, an array of rodlike support elements disposed perpendicularly with respect to said annular element and secured adjacent to the outer periphery of said annular element, a disc, said disc being disposed above said annular element and coupled to said support elements, a heater winding, said heater winding being disposed around said support elements between said annular element and said disc, a hollow cylindrically shaped heat reflector, said heat reflector surrounding said support elements between said annular element and said disc, a tubular element, the longitudinal axis of said tubular element being aligned perpendicularly with respect to a flanged mounting plate, said flanged plate extending transversely from said tubular element intermediate the ends thereof, said flanged plate being hermetically sealed to said tubular element, said tubular element having a valve therein on the side of said flanged plate remote from said heater winding, said tubular element having an inner diameter which is slightly larger than the diameter of a thermal analysis cell assembly adapted to be inserted therethrough and into the space within said heater winding, means for sealing said tubular element to said cell assembly, and lead means for energizing said heater winding.
Claim 3
Dependent Claim 23 words
An assembly in accordance with claim 1 wherein said means for sealing the tubular element to said cell assembly comprises a compression seal.
Claim 4
Dependent Claim 28 words
An assembly in accordance with claim 1, wherein said reflector element is supported on a tubular sleeve which is mechanically coupled to at least one of said discs.
Claim 5
Dependent Claim 17 words
An assembly in accordance with claim 1, wherein said support elements are made of a vitreous material.
Claim 6
Dependent Claim 20 words
An assembly in accordance with claim 1, wherein said flanged plate is adapted to be coupled to a mass spectrometer.

References Cited (Backward Citations)

US3431451A Cited
US3414661A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-01-10 1975-07-12 1976-01-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-01-10 1979-07-12 1980-01-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-01-10 1983-07-12 1984-01-11 $7700.00 Window Closed / Lapsed

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