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US3634149A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of manufacturing aluminium nitride crystals for semiconductor devices

Assignee: US Philips Corp
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Filing: 1967-10-25
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Granted: 1972-01-11
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Expires: 1987-10-25
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Abstract

Abstract A method of forming aluminum nitride single crystals of large area and silicon carbide-aluminum nitride heterojunctions using a modified Lely method. Aluminum nitride is introduced, as a vapor phase, into a furnace containing a plate-shaped monocrystal of silicon carbide at a temperature between 1800* and 2300* C. At those temperatures, aluminum nitride recrystallizes and condenses to deposit epitaxially on the silicon carbide. If the silicon carbide is of one conductivity type, the aluminum nitride can be suitably doped to be of the opposite conductivity type whereby a heterojunction is formed.

Inventors

  • 👤 Wilhelmus Francisc Knippenberg
  • 👤 Gerrit Verspui

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 19:54
CPC Classifications
C; C01; C01B; C01B21/00; C01B21/06; C01B21/072; C30; C30B; C30B25/00; C30B25/02; C30B29/00; C30B29/10; C30B29/38; Y; Y10; Y10S; Y10S117/00; Y10S117/915; Y10S148/00; Y10S148/065; Y10S148/072; Y10S148/113; Y10S148/148

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 40 words
A method as set forth in claim 1 wherein the silicon carbide monocrystal is provided by growing in the same chamber by recrystallization and condensation within a space bounded by silicon carbide and at a temperature of approximately 2,500* C.
Claim 2
Dependent Claim 25 words
A method as set forth in claim 1 for the growth of aluminum nitride crystals wherein the temperature is between 1,800* and 2, 100* C.
Claim 3
Dependent Claim 29 words
A method as set forth in claim 1 for the growth of mixed crystals of silicon carbide and aluminum nitride wherein the temperature is between 2,100* and 2,300* C.
Claim 4
Dependent Claim 24 words
A method as set forth in claim 1 wherein the gas atmosphere includes an inert gas-containing acceptor or donor impurities for the aluminum nitride.
Claim 5
Dependent Claim 21 words
A method as set forth in claim 1 wherein the silicon carbide crystal is separated from the aluminum nitride epitaxial layer.

References Cited (Backward Citations)

US3102828A Cited
US3224913A Cited
US3129125A Cited
US3228756A Cited
US3210624A Cited
US3275415A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-01-10 1975-07-12 1976-01-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-01-10 1979-07-12 1980-01-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-01-10 1983-07-12 1984-01-11 $7700.00 Window Closed / Lapsed

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